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1. 发明专利

JP2009256332A New polycarboxylic acid having fluorene skeleton, and method for producing the same 有权
标题翻译：具有荧光素的新型聚碳酸酯及其制造方法
公开(公告)号：JP2009256332A
公开(公告)日：2009-11-05
申请号：JP2009066862
申请日：2009-03-18
申请人： Osaka Gas Co Ltd , 大阪瓦斯株式会社
发明人： YAMADA MASAHIRO , MIYAUCHI SHINSUKE , NAGASHIMA TAICHI , MURASE HIROAKI , KAWASAKI SHINICHI , KITAJIMA SATSUKI , HANASAKA FUMIHIRO , SHIBAHARA TETSUYA , SATO MASAHIRO
IPC分类号： C07C59/72 , C07C51/367
摘要： PROBLEM TO BE SOLVED: To provide a polycarboxylic acid having a new fluorene skeleton, excellent in heat resistance etc. SOLUTION: This polycarboxylic acid is expressed by formula (1) [wherein, ring Z is a fused polycyclic aromatic hydrocarbon ring such as a naphthalene ring or the like; R 1 is cyano, a halogen atom or an alkyl; R 2 is a hydrocarbon group, an alkoxy, an aryloxy or the like; R 3 is an aliphatic hydrocarbon such as methylene or the like; (k) is an integer of 0 to 4; (m) is an integer of ≥0; and (n) is an integer of ≥1]. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供具有新的芴骨架的多元羧酸，耐热性优异等。解决方案：该多元羧酸由式（1）表示[其中，环Z是稠合多环芳族烃环等萘环等; R 1是氰基，卤素原子或烷基; R 2是烃基，烷氧基，芳氧基等; R 3是脂族烃，例如亚甲基等; （k）为0〜4的整数，（m）为≥0的整数; 和（n）为≥1的整数]。版权所有（C）2010，JPO＆INPIT

2. 发明专利

JP2009256333A New polycarboxylic acid having fluorene skeleton, and method for producing the same 有权
标题翻译：具有荧光素的新型聚碳酸酯及其制造方法
公开(公告)号：JP2009256333A
公开(公告)日：2009-11-05
申请号：JP2009066863
申请日：2009-03-18
申请人： Osaka Gas Co Ltd , 大阪瓦斯株式会社
发明人： YAMADA MASAHIRO , MIYAUCHI SHINSUKE , NAGASHIMA TAICHI , MURASE HIROAKI , KAWASAKI SHINICHI , KITAJIMA SATSUKI , HANASAKA FUMIHIRO , SHIBAHARA TETSUYA , SATO MASAHIRO
IPC分类号： C07C65/21 , C07C51/367
摘要： PROBLEM TO BE SOLVED: To provide a polycarboxylic acid having a new fluorene skeleton, excellent in heat resistance etc. SOLUTION: This polycarboxylic acid is expressed by formula (1) [wherein, ring Z is a fused polycyclic aromatic hydrocarbon ring; R 1 , R 2 are each an alkyl or the like; R 3 is an aliphatic hydrocarbon group; R 4 is an aromatic hydrocarbon group; (k) is an integer of 0 to 4; (m) is an integer of ≥0; and (n) is an integer of ≥1]. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供具有新的芴骨架的多元羧酸，耐热性优异等。解决方案：该多元羧酸由式（1）表示[其中，环Z是稠合多环芳族烃环; R 1 ，R 2 各自为烷基等; R 3是脂族烃基; R 4 是芳族烃基; （k）为0〜4的整数，（m）为≥0的整数; 和（n）为≥1的整数]。版权所有（C）2010，JPO＆INPIT

3. 发明专利

JP2014159400A Method for producing bromine-containing fluorene compound 审中-公开
标题翻译：生产含有荧光素的氟化合物的方法
公开(公告)号：JP2014159400A
公开(公告)日：2014-09-04
申请号：JP2013246484
申请日：2013-11-28
申请人： Osaka Gas Co Ltd , 大阪瓦斯株式会社
发明人： YAMADA MASAHIRO , MIYAUCHI SHINSUKE , NAGASHIMA TAICHI , MURASE HIROAKI , KAWASAKI SHINICHI , SHIBAHARA TETSUYA , KITAJIMA SATSUKI , HANASAKA FUMIHIRO , SATO MASAHIRO
IPC分类号： C07C39/42
摘要： PROBLEM TO BE SOLVED: To provide a specific fluorene skeleton-containing compound having a hydroxy group and a bromine atom, which can be produced in a high yield, inexpensively, and industrially advantageously.SOLUTION: Provided is a bromine-containing fluorene compound such as 9,9-bis(hydroxybromoaryl)fluorene represented by formula (2D), wherein Ris a cyano group, a halogen atom or an alkyl group; Ris an alkylene group; Ris a substituent such as an alkyl group or an aryl group; k is an integer of 0-4, m is an integer of 0 or more, and p1 is an integer of 0-3.
摘要翻译：要解决的问题：提供具有羟基和溴原子的特定含芴骨架化合物，其可以高产率，低成本和工业上有利地制备。溶液：提供含溴的芴化合物，例如由式（2D）表示的9,9-双（羟基溴芳基）芴，其中R是氰基，卤素原子或烷基; R为亚烷基; R是取代基，例如烷基或芳基; k为0〜4的整数，m为0以上的整数，p1为0〜3的整数。

4. 发明专利

JP2013103153A Porous substance, siloxane removing agent, and filter using the same 有权
标题翻译：多孔物质，硅酮去除剂和使用其的过滤器
公开(公告)号：JP2013103153A
公开(公告)日：2013-05-30
申请号：JP2011247151
申请日：2011-11-11
申请人： Osaka Gas Co Ltd , 大阪瓦斯株式会社
发明人： NIWA ATSUSHI , SOJO DAISAKU , KITAJIMA SATSUKI , ONAKA JUNKO , NAKAYAMA TOSHIRO , NAKAJIMA TAKASHI , ONISHI HISAO , NONAKA ATSUSHI
IPC分类号： B01J20/22 , B01D53/02 , G01N1/22
摘要： PROBLEM TO BE SOLVED: To provide a porous substance useful for efficiently adsorbing siloxanes to remove them, a siloxane removing agent or (adsorbent) constituted of the porous substance, and a filter useful for removing siloxanes (or a gas sensor equipped with the filter).SOLUTION: The porous substance is constituted by adding and applying a sulfonic group modified metal oxide sol to a porous material and the sulfonic group modified metal oxide sol modified by a functional group preferably represented by formula (1) HOS(=O)-R-Si(CH)(-O-)[wherein R is 1-10C alkylene group (wherein a urethane bond or a urea bond may be contained in this alkylene chain) and n is 0 or 1] is added and applied to the porous material.
摘要翻译：要解决的问题：为了提供用于有效吸附硅氧烷以除去它们的多孔物质，由多孔物质构成的硅氧烷除去剂或（吸附剂）和可用于除去硅氧烷的过滤器（或配备有过滤器）。解决方案：多孔物质通过向多孔材料中加入并施加磺酸基改性金属氧化物溶胶而构成，并且通过优选由式（1）表示的官能团改性的磺酸基改性的金属氧化物溶胶HOS（= O）（SB <= POS =“POST”> 3 ）< - SB POS =“POST”> n ）其中R为1-10C亚烷基（其中该亚烷基链中可含有氨基甲酸酯键或脲键），n为0或1]为添加并应用于多孔材料。版权所有（C）2013，JPO＆INPIT

5. 发明专利

JP2009256293A Silicon compound having fluorene skeleton 有权
标题翻译：含有氟橡胶的硅化合物
公开(公告)号：JP2009256293A
公开(公告)日：2009-11-05
申请号：JP2008121538
申请日：2008-05-07
申请人： Osaka Gas Co Ltd , 大阪瓦斯株式会社
发明人： YAMADA MASAHIRO , MIYAUCHI SHINSUKE , NAGASHIMA TAICHI , KAWASAKI SHINICHI , KITAJIMA SATSUKI , HANASAKA FUMIHIRO , SHIBAHARA TETSUYA , SATO MASAHIRO
IPC分类号： C07F7/18
摘要： PROBLEM TO BE SOLVED: To provide a new silicon compound having a fluorene skeleton which has excellent properties such as a high refractive index, and high transparency. SOLUTION: The new silicon compound is represented by the formula (wherein ring Z is a benzene ring or the like; X is a connecting group; R 1 is a cyano group or the like; R 2 is an alkyl group or the like; R 3 is an alkylene group; R 4 , R 5 , and R 6 are each hydrogen or the like; k is an integer of 0-4; m is an integer of not less than 0; n is an integer of not less than 0; p1 is an integer of not less than 1; and p2 is an integer of not less than 0). COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供具有优异性能如高折射率和高透明度的芴骨架的新的硅化合物。解决方案：新的硅化合物由式（其中环Z是苯环等）表示; X是连接基团; R 1是氰基等; R 2 是烷基等; R 3是亚烷基; R 4是，R 5，和R 6各自为氢等; k为0-4的整数; m为不小于0的整数; n为不小于0的整数; p1为整数不小于1; p2是不小于0的整数）。版权所有（C）2010，JPO＆INPIT

6. 发明专利

JP2013103154A Porous substance, siloxane removing agent, and filter using the same 有权
标题翻译：多孔物质，硅酮去除剂和使用其的过滤器
公开(公告)号：JP2013103154A
公开(公告)日：2013-05-30
申请号：JP2011247205
申请日：2011-11-11
申请人： Osaka Gas Co Ltd , 大阪瓦斯株式会社
发明人： NIWA ATSUSHI , SOJO DAISAKU , KITAJIMA SATSUKI , ONAKA JUNKO , NAKAYAMA TOSHIRO , NAKAJIMA TAKASHI , ONISHI HISAO , NONAKA ATSUSHI
IPC分类号： B01J20/22 , B01D53/02 , G01N1/22
摘要： PROBLEM TO BE SOLVED: To provide a porous substance useful for efficiently adsorbing siloxanes to remove them, a siloxane removing agent or (adsorbent) constituted of the porous substance, and a filter useful for removing siloxanes (or a gas sensor equipped with the filter).SOLUTION: The porous material is constituted by adding and applying a sulfonic group modified metal oxide sol to a porous material and adsorbing siloxanes on the porous material. The sulfonic group modified metal oxide sol modified by a functional group preferably represented by formula (1) HOS(=O)-R-Si(CH)(-O-)[wherein R is a 1-10C alkylene group (wherein a urethane bond or a urea bond may be contained in the alkylene chain) and n is 0 or 1] is added and applied to the porous material.
摘要翻译：要解决的问题：为了提供用于有效吸附硅氧烷以除去它们的多孔物质，由多孔物质构成的硅氧烷除去剂或（吸附剂）和可用于除去硅氧烷的过滤器（或配备有过滤器）。解决方案：多孔材料通过向多孔材料中添加并施加磺酸基改性的金属氧化物溶胶并在多孔材料上吸附硅氧烷而构成。通过优选由式（1）表示的官能团改性的磺酸基改性金属氧化物溶胶HOS（= O） 2 -S-Si（CH ） n （ - O - ） 3-n 其中R是1-10C亚烷基（其中亚烷基链中可以包含氨基甲酸酯键或脲键），并且n为0或1]并加入到多孔材料中。版权所有（C）2013，JPO＆INPIT

7. 发明专利

JP2011105887A Fluorene polyester oligomer and method for producing the same 有权
标题翻译：氟聚合物低聚物及其制备方法
公开(公告)号：JP2011105887A
公开(公告)日：2011-06-02
申请号：JP2009264325
申请日：2009-11-19
申请人： Osaka Gas Co Ltd , 大阪瓦斯株式会社
发明人： YAMADA MASAHIRO , MIYAUCHI SHINSUKE , NAGASHIMA TAICHI , MURASE HIROAKI , KAWASAKI SHINICHI , SHIBAHARA TETSUYA , KITAJIMA SATSUKI , SATO MASAHIRO
IPC分类号： C08G63/199
摘要： PROBLEM TO BE SOLVED: To provide a fluorene polyester oligomer and to provide a high yield and easy method for producing the same.
SOLUTION: The fluorene polyester oligomer can be produced by adding a base to a reaction system in which an excess mole of one component to the other component of a diol having a fluorene skeleton (e.g. 9, 9-bis(aryl) fluorene skeleton) and a dicarboxylic acid dihalide is put to perform condensation reaction of both components. Weight-average molecular weight of the fluorene polyester oligomer produced by this method may be
摘要翻译：待解决的问题：提供芴聚酯低聚物并提供高产率和易于制备的方法。解决方案：芴聚酯低聚物可以通过向其中过量摩尔的一种组分与具有芴骨架的二醇的另一种组分（例如9,9-双（芳基）芴）的反应体系骨架）和二羧酸二卤化物进行两种组分的缩合反应。通过该方法制备的芴聚酯低聚物的重均分子量可以<5,000，以聚苯乙烯换算为例如表示。凝胶渗透色谱法。版权所有（C）2011，JPO＆INPIT

8. 发明专利

JP2009256334A Method for producing bromine-containing fluorene compound 有权
标题翻译：生产含有荧光素的氟化合物的方法
公开(公告)号：JP2009256334A
公开(公告)日：2009-11-05
申请号：JP2009066864
申请日：2009-03-18
申请人： Osaka Gas Co Ltd , 大阪瓦斯株式会社
发明人： YAMADA MASAHIRO , MIYAUCHI SHINSUKE , NAGASHIMA TAICHI , MURASE HIROAKI , KAWASAKI SHINICHI , SHIBAHARA TETSUYA , KITAJIMA SATSUKI , HANASAKA FUMIHIRO , SATO MASAHIRO
IPC分类号： C07C37/62 , C07C39/42
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a specific fluorene skeleton-containing compound having a hydroxy group and a bromine atom in a high yield, inexpensively and also industrially advantageously.
SOLUTION: This method for producing a bromine-containing fluorene compound is provided by reacting a fluorene compound expressed by formula (1) [wherein, ring Z is an aromatic hydrocarbon ring; R
1 is an alkyl or the like; R
2 is an alkylene or the like; R
3 is a substituting group such as an alkyl, an aryl or the like; and (k), (m), (n) and (p) are each an integer] with bromine.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：提供一种以高产率，低成本且在工业上有利地制备具有羟基和溴原子的特定含芴骨架化合物的方法。解决方案：通过使式（1）表示的芴化合物[其中，环Z是芳族烃环; R 1是烷基等; R 2是亚烷基等; R 3是取代基，例如烷基，芳基等; 和（k），（m），（n）和（p）各自为整数]。版权所有（C）2010，JPO＆INPIT

9. 发明专利

JP2009227603A Method of manufacturing polycarboxylic acid having fluorene skeleton 有权
标题翻译：制造具有荧光素的聚碳酸的方法
公开(公告)号：JP2009227603A
公开(公告)日：2009-10-08
申请号：JP2008073965
申请日：2008-03-21
申请人： Osaka Gas Co Ltd , 大阪瓦斯株式会社
发明人： YAMADA MASAHIRO , MIYAUCHI SHINSUKE , NAGASHIMA TAICHI , MURASE HIROAKI , KAWASAKI SHINICHI , KITAJIMA SATSUKI , HANASAKA FUMIHIRO , SHIBAHARA TETSUYA , SATO MASAHIRO
IPC分类号： C07C51/367 , C07C59/72
摘要： PROBLEM TO BE SOLVED: To provide a method for simply and efficiently manufacturing a polycarboxylic acid having a fluorene skeleton [for example, 9,9-bis(carboxy 1-4C alkoxyphenyl)fluorene and the like]. SOLUTION: The manufacturing method comprises reacting a compound represented by formula (2) with a carboxylic acid represented by formula (3) or a derivative thereof (for example, an ester, or an alkali or alkaline earth metal salt) in the presence of a basic compound. COPYRIGHT: (C)2010,JPO&INPIT

10. 发明专利

JP2011042596A New heterocycle-containing compound having fluorene skeleton and method for producing the same 有权
标题翻译：具有荧光素的新的含有异氰酸酯的化合物及其生产方法
公开(公告)号：JP2011042596A
公开(公告)日：2011-03-03
申请号：JP2009190444
申请日：2009-08-19
申请人： Osaka Gas Co Ltd , 大阪瓦斯株式会社
发明人： YAMADA MASAHIRO , MIYAUCHI SHINSUKE , NAGASHIMA TAICHI , MURASE HIROAKI , KAWASAKI SHINICHI , SHIBAHARA TETSUYA , KITAJIMA SATSUKI , HANASAKA FUMIHIRO , SATO MASAHIRO
IPC分类号： C07D213/73 , C07D213/80 , C07D307/68 , C07D333/40
摘要： PROBLEM TO BE SOLVED: To provide a new heterocycle-containing compound having a fluorene skeleton and usable as a raw material or the like for a resin excelling in heat resistance or the like. SOLUTION: The heterocycle-containing compound is represented by formula (1) (wherein, ring Ar is an aromatic hydrocarbon ring; ring Het is a heterocycle; R 1 is cyano or the like; R 2 and R 3 are each hydrocarbon or the like; A 1 is alkylene; A 2 is a direct bond or aliphatic hydrocarbon; X is a reactive group, a derivative thereof or a precursor thereof; k is an integer of 0-4; m, p and q are each an integer of ≥0; and n is an integer of ≥1). COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供具有芴骨架的新的含杂环化合物，并且可用作耐热性等优异的树脂的原料等。解决方案：含杂环化合物由式（1）表示（其中环Ar为芳族烃环;环Het为杂环; R 1为氰基等; R 2 和R 3 分别为烃类等; A SP SP 1为亚烷基; A 2 为直接键或脂族烃; X为反应性基团，其衍生物或其前体; k为0-4的整数; m，p和q各自为≥0的整数; n为≥1的整数）。版权所有（C）2011，JPO＆INPIT

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