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    • 2. 发明授权
    • Process of making alkyl sulfate granulates
    • 制备烷基硫酸盐颗粒的方法
    • US06455488B1
    • 2002-09-24
    • US09700309
    • 2001-01-12
    • Georg AssmannOlaf BlochwitzAndreas SyldathDitmar Kischkel
    • Georg AssmannOlaf BlochwitzAndreas SyldathDitmar Kischkel
    • C11D1700
    • C11D1/146A61K8/0225A61K8/463A61Q5/02A61Q19/10B01J2/16C07C303/44C07C305/06
    • A process for making substantially odorless granules of alkyl sulfates corresponding to formula (I): R-O-SO3X (I) wherein R is an alkyl group containing from 6 to 18 carbon atoms, and X is selected from the group consisting of an alkali metal, an alkaline earth metal, ammonium, an alkyl ammonium, and alkanolammonium, and a glucammonium ion, the process involving: (a) providing a water-containing paste of alkyl sulfates having a content of unsulfonated components of greater than 0.3% by weight; and (b) simultaneously granulating and drying, in a fluidized bed, the water-containing paste of alkyl sulfates to form substantially odorless granules of alkyl sulfates, and wherein the substantially odorles granules thus formed have less than 0.2% by weight, based on the weight of active substance, of unsulfonated components present therein.
    • 对应于式(I)的基本无臭的烷基硫酸盐颗粒的方法:RO-SO 3 X(I)其中R是含有6至18个碳原子的烷基,X选自碱金属, 碱土金属,铵,烷基铵和链烷醇铵和葡萄糖铵离子,所述方法包括:(a)提供含有大于0.3重量%的未磺化组分含量的烷基硫酸盐的含水浆料; 和(b)在流化床中同时造粒和干燥烷基硫酸盐的含水浆料,以形成基本上无气味的烷基硫酸盐颗粒,并且其中由此形成的基本上气味的颗粒的含量小于0.2重量%,基于 活性物质,其中存在的未磺化组分的重量。