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1. 发明申请

US20050084706A1 Method of selective region vapor phase aluminizing 有权
标题翻译：选择性区域气相镀铝的方法
公开(公告)号：US20050084706A1
公开(公告)日：2005-04-21
申请号：US10685637
申请日：2003-10-15
申请人： Nripendra Das , Joseph Rigney , Jeffrey Pfaendtner , Matthew Saylor
发明人： Nripendra Das , Joseph Rigney , Jeffrey Pfaendtner , Matthew Saylor
IPC分类号： C23C10/02 , C23C10/06 , C23C10/14 , B32B15/10
CPC分类号： C23C10/06 , C23C10/02 , C23C10/14 , Y02T50/67 , Y10T428/12736
摘要： The present invention is process for forming diffusion aluminide coatings on an uncoated surface of a substrate, without interdiffusing a sufficient amount of aluminum into a coating layer to adversely affect the coating growth potential and mechanical properties of said coating layer. A metal substrate is provided comprising an external surface and an internal passage therein defined by an internal surface, at least a portion of the external surface of the substrate being coated with a coating layer selected from the group consisting of β-NiAl-base, MCrAlX, a line-of-sight diffusion aluminide, a non-line-of-sight diffusion aluminide, a pack diffusion aluminide, and a slurry diffusion aluminide on said substrate. The external surface of the substrate is cleaned. The metal substrate is subjected to a aluminum vapor phase deposition process performed using a fluorine-containing activator selected from the group consisting of AlF3, CrF3, NH4F, and combinations thereof, at a rate in the range of about 0.036 mols of fluorine per ft3/hr of transport gas to about 0.18 mols of fluorine per ft3/hr of transport gas, at a temperature in the range of about 1350° F. (730° C.) to about 1925° F. (1050° C.), using a transport gas selected from the group consisting of argon, nitrogen, hydrogen, and combinations thereof, the transport gas being provided at a flow rate in the range of about 20 ft3/hr to about 120 ft3/hr for a period of time in the range of about 2 hours to about 10 hours. The substrate is then cooled. The present invention is also a superalloy article coated with a diffusion aluminide layer using the diffusion aluminide coating process of the present invention.
摘要翻译：本发明是在基材的未涂覆表面上形成扩散铝化物涂层的方法，而不会将足够量的铝相互扩散到涂层中，从而不利地影响涂层生长电位和所述涂层的机械性能。提供了一种金属基底，其包括由内表面限定的外表面和内部通道，所述基底的外表面的至少一部分被涂覆有选自β-NiAl基，MCrAlX ，视线扩散铝化物，非视线扩散铝化物，包层扩散铝化物和在所述衬底上的浆料扩散铝化物。清洁基板的外表面。对金属基板进行铝蒸气相沉积工艺，该方法使用选自AlF 3 N 3，CrF 3 N，NH 4的含氟活化剂 F和它们的组合，以约0.036摩尔氟/ ft 3 /小时的运输气体至约0.18摩尔氟/ ft 3的范围内的速率，在约1350°F（730℃）至约1925°F（1050℃）的温度范围内使用选自以下的输送气体：氩气，氮气，氢气及其组合，输送气体的流速为约20ft 3 / hr至约120ft 3 / hr 一段时间在约2小时至约10小时的范围内。然后将衬底冷却。本发明也是使用本发明的扩散铝化物涂覆方法涂覆有扩散铝化物层的超级合金制品。

2. 发明申请

US20050069650A1 NICKEL ALUMINIDE COATING AND COATING SYSTEMS FORMED THEREWITH 审中-公开
标题翻译：镍基铝涂料和涂料系统
公开(公告)号：US20050069650A1
公开(公告)日：2005-03-31
申请号：US10904325
申请日：2004-11-04
申请人： Ramgopal Darolia , Joseph Rigney , William Walston , Jeffrey Pfaendtner , Brett Boutwell , Irene Spitsberg , James Ruud
发明人： Ramgopal Darolia , Joseph Rigney , William Walston , Jeffrey Pfaendtner , Brett Boutwell , Irene Spitsberg , James Ruud
IPC分类号： C23C4/02 , C23C4/12 , C23C14/06 , C23C28/00 , H05H1/26
CPC分类号： C23C28/321 , C23C4/02 , C23C4/12 , C23C14/06 , C23C28/3215 , C23C28/324 , C23C28/345 , C23C28/3455 , Y10T428/12576 , Y10T428/12611 , Y10T428/12618 , Y10T428/12736 , Y10T428/12771 , Y10T428/12806 , Y10T428/12944 , Y10T428/252
摘要： A beta-phase NiAl overlay coating containing a dispersion of ceramic particles and a process for depositing the overlay coating. If the coating is used to adhere a thermal barrier coating (TBC), the TBC exhibits improved spallation resistance as a result of the dispersion of ceramic particles having a dispersion-strengthening effect on the overlay coating. The overlay coating contains at least one reactive element and is deposited so that the some of the reactive element deposits as the ceramic particles dispersed in the overlay coating.
摘要翻译：含有陶瓷颗粒分散体的β相NiAl覆盖涂层和沉积覆盖层的方法。如果涂层用于粘附热障涂层（TBC），则由于在覆盖涂层上具有分散强化作用的陶瓷颗粒的分散，TBC显示出改进的抗剥落性。覆盖层包含至少一个反应性元件并沉积成使得一部分反应性元素沉积为陶瓷颗粒分散在覆盖层中。

3. 发明申请

US20050019491A1 BETA-PHASE NICKEL ALUMINIDE OVERLAY COATING AND PROCESS THEREFOR 审中-公开
标题翻译： BETA相镍合金镀层及其工艺
公开(公告)号：US20050019491A1
公开(公告)日：2005-01-27
申请号：US10711584
申请日：2004-09-27
申请人： Irene Spitsberg , Joseph Rigney , Ramgopal Darolia , Elissa Lee , Jeffrey Pfaendtner
发明人： Irene Spitsberg , Joseph Rigney , Ramgopal Darolia , Elissa Lee , Jeffrey Pfaendtner
IPC分类号： C21D7/06 , C23C4/18 , C23C8/02 , C23C26/00 , C23C28/00 , B05D3/12
CPC分类号： C23C28/321 , C21D7/06 , C23C4/18 , C23C8/02 , C23C26/00 , C23C28/345 , C23C28/3455 , Y10T428/12611 , Y10T428/12736 , Y10T428/12937 , Y10T428/12944
摘要： A beta-phase nickel aluminide (NiAl) overlay coating (24) and method for modifying the grain structure of the coating (24) to improve its oxidation resistance. The coating (24) is deposited by a method that produces a grain structure characterized by grain boundaries (44) exposed at the outer coating surface (36). The grain boundaries (44) may also contain precipitates (40) as a result of the alloyed chemistry of the coating (24). During or after deposition, the overlay coating (24) is caused to form new grain boundaries (34) that, though open to the outer surface (36) of the coating (24), are free of precipitates or contain fewer precipitates (40) than the as-deposited grain boundaries (44). New grain boundaries (34) are preferably produced by causing the overlay coating (24) to recrystallize during coating deposition or after deposition as a result of a surface treatment followed by heat treatment.
摘要翻译： β相镍铝化合物（NiAl）覆盖层（24）以及用于改变涂层（24）的晶粒结构以提高其抗氧化性的方法。通过产生以在外涂层表面（36）处暴露的晶界（44）为特征的晶粒结构的方法沉积涂层（24）。作为涂层（24）的合金化学的结果，晶界（44）也可以含有沉淀物（40）。在沉积期间或之后，使覆盖涂层（24）形成新的晶粒边界（34），其尽管向涂层（24）的外表面（36）开口，但没有沉淀物或含有较少的沉淀物（40）比沉积的晶界（44）。优选通过在涂布沉积期间或沉积后的覆盖涂层（24）进行再结晶，然后进行热处理后的表面处理，来制造新的晶界（34）。

4. 发明申请

US20060182892A9 BETA-PHASE NICKEL ALUMINIDE OVERLAY COATINGS AND PROCESS THEREFOR 有权
标题翻译： BETA相镍合金镀层及其工艺
公开(公告)号：US20060182892A9
公开(公告)日：2006-08-17
申请号：US10248056
申请日：2002-12-13
申请人： Irene Spitsberg , Joseph Rigney , Ramgopal Darolia , Elissa Lee , Jeffrey Pfaendtner
发明人： Irene Spitsberg , Joseph Rigney , Ramgopal Darolia , Elissa Lee , Jeffrey Pfaendtner
IPC分类号： B32B15/00 , B32B15/10 , B05D3/02 , B05D1/36
CPC分类号： C23C28/321 , C21D7/06 , C23C4/18 , C23C8/02 , C23C26/00 , C23C28/345 , C23C28/3455 , Y10T428/12611 , Y10T428/12736 , Y10T428/12937 , Y10T428/12944
摘要： A beta-phase nickel aluminide (NiAl) overlay coating (24) and method for modifying the grain structure of the coating (24) to improve its oxidation resistance. The coating (24) is deposited by a method that produces a grain structure characterized by grain boundaries (44) exposed at the outer coating surface (36). The grain boundaries (44) may also contain precipitates (40) as a result of the alloyed chemistry of the coating (24). During or after deposition, the overlay coating (24) is caused to form new grain boundaries (34) that, though open to the outer surface (36) of the coating (24), are free of precipitates or contain fewer precipitates (40) than the as-deposited grain boundaries (44). New grain boundaries (34) are preferably produced by causing the overlay coating (24) to recrystallize during coating deposition or after deposition as a result of a surface treatment followed by heat treatment.
摘要翻译： β相镍铝化合物（NiAl）覆盖层（24）以及用于改变涂层（24）的晶粒结构以提高其抗氧化性的方法。通过产生以在外涂层表面（36）处暴露的晶界（44）为特征的晶粒结构的方法沉积涂层（24）。由于涂层（24）的合金化学，晶界（44）也可含有沉淀物（40）。在沉积期间或之后，使覆盖涂层（24）形成新的晶粒边界（34），其尽管向涂层（24）的外表面（36）开口，但没有沉淀物或含有较少的沉淀物（40）比沉积的晶界（44）。优选通过在涂布沉积期间或沉积后的覆盖涂层（24）进行再结晶，然后进行热处理后的表面处理，来制造新的晶界（34）。

5. 发明申请

US20050136283A1 NI-BASE SUPERALLOY HAVING A THERMAL BARRIER COATING SYSTEM 失效
标题翻译：具有热障涂层系统的NI-BASE SUPERALLOY合金
公开(公告)号：US20050136283A1
公开(公告)日：2005-06-23
申请号：US10707543
申请日：2003-12-19
申请人： Jeffrey Pfaendtner , Deborah Schorr , Ramgopal Darolia , Joseph Rigney , Irene Spitsberg , William Walston
发明人： Jeffrey Pfaendtner , Deborah Schorr , Ramgopal Darolia , Joseph Rigney , Irene Spitsberg , William Walston
IPC分类号： C22C19/03 , C23C4/00 , C23C28/00 , C23C30/00 , F01D5/00 , F01D5/28 , B32B15/01
CPC分类号： C23C28/321 , C23C28/3215 , C23C28/325 , C23C28/345 , C23C28/3455 , F01D5/288 , F05D2220/3212 , F05D2300/13 , Y10T428/12611 , Y10T428/12736 , Y10T428/1275 , Y10T428/12875 , Y10T428/12944 , Y10T428/12986
摘要： An article and TBC coating system thereon that in combination exhibit significantly improved spallation resistance. The article comprises a substrate formed of a metal alloy containing ruthenium and one or more refractory elements (e.g., tantalum, tungsten, molybdenum, rhenium, hafnium, etc.). The substrate is protected by a coating system comprising an aluminum-containing bond coat on the surface of the substrate and a ceramic coating bonded to the substrate by the bond coat. The bond coat, preferably an aluminide, is deposited so as to be substantially free of ruthenium, though ruthenium is present in the bond coat as a result of diffusion from the substrate into the bond coat.
摘要翻译：其上的一种制品和TBC涂层体系组合显示出显着改善的防剥落性。该制品包括由含有钌和一种或多种难熔元素（例如钽，钨，钼，铼，铪等）的金属合金形成的基材。基材由包括基材表面的含铝粘合涂层的涂层体系和通过粘合涂层粘合到基材上的陶瓷涂层保护。沉积粘合涂层，优选铝化物，以便基本上不含钌，尽管由于从基材扩散到粘合涂层中，钌存在于粘合涂层中。

6. 发明申请

US20060093801A1 COATING SYSTEMS CONTAINING BETA PHASE AND GAMMA-PRIME PHASE NICKEL ALUMINIDE 有权
标题翻译：包含BET相和GMAMA-PRIME相镍铬酸盐的涂料体系
公开(公告)号：US20060093801A1
公开(公告)日：2006-05-04
申请号：US10904844
申请日：2004-12-01
申请人： Ramgopal Darolia , Joseph Rigney , Gillion Marijnissen , Eric Vergeldt , Annejan Kloosterman
发明人： Ramgopal Darolia , Joseph Rigney , Gillion Marijnissen , Eric Vergeldt , Annejan Kloosterman
IPC分类号： B32B15/01 , B63H1/26 , B32B15/00
CPC分类号： F01D5/288 , C23C4/18 , C23C10/02 , C23C10/48 , C23C10/50 , C23C10/52 , C23C28/021 , C23C28/321 , C23C28/3455 , C23C30/00 , F05D2230/90 , F05D2300/611 , Y10T428/12611 , Y10T428/12618 , Y10T428/12736 , Y10T428/12937 , Y10T428/12944 , Y10T428/12951 , Y10T428/24967 , Y10T428/264 , Y10T428/265 , Y10T428/31678
摘要： A coating and process for depositing the coating on a substrate. The coating is a nickel aluminide overlay coating of predominantly the beta (NiAl) and gamma-prime (Ni3Al) intermetallic phases, and is suitable for use as an environmental coating and as a bond coat for a thermal barrier coating (TBC). The coating can be formed by depositing nickel and aluminum in appropriate amounts to yield the desired beta+gamma prime phase content. Alternatively, nickel and aluminum can be deposited so that the aluminum content of the coating exceeds the appropriate amount to yield the desired beta+gamma prime phase content, after which the coating is heat treated to diffuse the excess aluminum from the coating into the substrate to yield the desired beta+gamma prime phase content.
摘要翻译：用于将涂层沉积在基材上的涂层和方法。涂层是主要是β（NiAl）和γ-prime（Ni 3 Al 3 Al）金属间相的镍铝化物覆盖涂层，并且适合用作环境涂层和作为粘合涂层隔热涂层（TBC）。可以通过以适当的量沉积镍和铝来形成所述涂层，以产生所需的β+γ初相相含量。或者，可以沉积镍和铝，使得涂层的铝含量超过适当的量以产生所需的β+γ初相相含量，之后热处理涂层以将过量的铝从涂层扩散到基底中产生期望的β+γ'相相含量。

7. 发明申请

US20050266266A1 Nickel aluminide coating with improved oxide stability 失效
标题翻译：镍铝镀层具有改善的氧化物稳定性
公开(公告)号：US20050266266A1
公开(公告)日：2005-12-01
申请号：US10855687
申请日：2004-05-27
申请人： Joseph Rigney , David Clarke , Ramgopal Darolia
发明人： Joseph Rigney , David Clarke , Ramgopal Darolia
IPC分类号： F01D5/28 , C04B35/486 , C22C19/03 , C23C4/04 , C23C4/08 , C23C4/18 , C23C8/02 , C23C28/00 , F02C7/00 , B32B15/04
CPC分类号： C04B35/486 , C04B2235/3206 , C04B2235/3208 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3229 , C04B2235/3232 , C23C4/18 , C23C8/02 , C23C28/321 , C23C28/345 , C23C28/3455 , Y10T428/12493 , Y10T428/12535 , Y10T428/12618 , Y10T428/12736 , Y10T428/12944
摘要： In one embodiment of the invention, a NiAl overlay bond coating composition comprises a NiAl alloy. The alloy comprises Zr and at least one modifying element in an amount effective to form a stabilized oxide structure comprising stabilized zirconia including a substantially tetragonal structure upon oxidation of the alloy. The tetragonal structure is stabilized such that it does not change phases and revert to a monoclinic or monoclinic and tetragonal structure, which is not substantially tetragonal, upon thermal cycling.
摘要翻译：在本发明的一个实施方案中，NiAl覆盖层涂层组合物包含NiAl合金。合金包含Zr和至少一种修饰元素，其量有效地形成稳定的氧化物结构，其包含在合金氧化时包括基本上四方晶结构的稳定的氧化锆。四方结构被稳定，使得其在热循环时不改变相并恢复为单斜晶体或单斜晶体和四方晶体结构，其基本上不是四边形。

8. 发明申请

US20070292710A1 Method for repairing components using environmental bond coatings and resultant repaired components 审中-公开
标题翻译：使用环境粘合剂涂层修补部件的方法以及由此修复的部件
公开(公告)号：US20070292710A1
公开(公告)日：2007-12-20
申请号：US11605082
申请日：2006-11-28
申请人： Joseph Rigney , Ramgopal Darolia
发明人： Joseph Rigney , Ramgopal Darolia
IPC分类号： C25D11/02 , B32B15/00
CPC分类号： C23C10/02 , C23C18/54 , C23C28/321 , C23C28/3215 , C23C28/325 , C23C28/345 , C23C28/3455 , C25D7/04 , Y10T428/1259 , Y10T428/12736 , Y10T428/12771 , Y10T428/12937 , Y10T428/12944 , Y10T428/265
摘要： According to an embodiment of the invention, a repaired component is disclosed. The repaired component comprises an engine run component having a base metal substrate, a portion of the base metal substrate between about 1-3 mils in thickness and an overlying bond coat having been removed to create a remaining base metal substrate of reduced thickness. The repaired component further comprises a lower growth environmental bond coating comprising an alloy having an aluminum content of about 10-60 atomic percent applied to the remaining base metal substrate so that upon subsequent repair of the component, less than about 1-3 mils in thickness of the remaining base metal substrate is removed because of less environmental coating growth into the substrate than the prior bond coat. Advantageously, the repaired component has extended component life and increased repairability.
摘要翻译：根据本发明的实施例，公开了修理的部件。被修复的部件包括具有贱金属基底的发动机运行部件，贱金属基底的厚度在约1-3密耳之间的部分和已经去除的上覆接合涂层，以产生厚度减小的剩余基底金属基底。修复的部件还包括较低生长环境粘合涂层，其包含施加到剩余的贱金属基底上的约10-60原子百分比的铝含量的合金，使得在随后修复部件时，厚度小于约1-3密耳剩余的贱金属基底被去除，因为比现有的粘合涂层更少的环境涂层生长到基底中。有利地，修复的部件具有延长的部件寿命和增加的可修复性。

9. 发明申请

US20070160775A1 PHYSICAL VAPOR DEPOSITION PROCESS AND APPARATUS THEREFOR 审中-公开
标题翻译：物理蒸气沉积工艺及其设备
公开(公告)号：US20070160775A1
公开(公告)日：2007-07-12
申请号：US11306740
申请日：2006-01-10
申请人： Gillion Marijnissen , Eric Vergeldt , Joseph Rigney , Annejan Kloosterman , Ramgopal Darolia
发明人： Gillion Marijnissen , Eric Vergeldt , Joseph Rigney , Annejan Kloosterman , Ramgopal Darolia
IPC分类号： C23C8/00 , C23C16/00
CPC分类号： C23C14/30 , C23C14/16 , C23C14/243 , C23C14/246
摘要： A PVD process and apparatus for depositing a coating from multiple sources of materials with different vapor pressures. The process entails forming molten pools of different first and second materials in a coating chamber of the apparatus, supporting an article within the chamber, and evaporating the molten pools with an energy beam to deposit a coating on the article with a controlled composition that contains at least a first metal and a relatively lesser amount of at least one reactive metal having a lower vapor pressure than the first metal. The first material contains at least the first metal, and the second material contains the reactive metal and at least a second metal. The second and reactive metals are combined to cause the second material to have a lower melting temperature and wider melting range than the reactive metal.
摘要翻译：用于从具有不同蒸汽压力的多种材料源沉积涂层的PVD工艺和设备。该方法需要在装置的涂覆室中形成不同的第一和第二材料的熔池，在室内支撑物品，并用能量束蒸发熔池，以将涂层沉积在具有受控组成的包含在至少一种第一金属和相对较少量的至少一种具有比第一金属更低的蒸气压的活性金属。第一材料至少包含第一金属，第二材料包含反应性金属和至少第二金属。将第二和反应性金属组合以使第二材料具有比反应性金属更低的熔融温度和更宽的熔化范围。

10. 发明申请

US20060093850A1 COATING SYSTEMS CONTAINING GAMMA-PRIME NICKEL ALUMINIDE COATING 有权
标题翻译：包含GAMMA-PRIME镍铬铝涂料的涂料体系
公开(公告)号：US20060093850A1
公开(公告)日：2006-05-04
申请号：US10904220
申请日：2004-10-29
申请人： Ramgopal Darolia , Joseph Rigney , William Walston
发明人： Ramgopal Darolia , Joseph Rigney , William Walston
IPC分类号： B32B15/01 , B32B15/04
CPC分类号： F01D5/288 , F05C2201/0466 , F05D2230/90 , F05D2300/611 , Y10T428/12611 , Y10T428/12618 , Y10T428/12875 , Y10T428/12931 , Y10T428/12937 , Y10T428/12944
摘要： An overlay coating for articles used in hostile thermal environments. The coating has a predominantly gamma prime-phase nickel aluminide (Ni3Al) composition suitable for use as an environmental coating and as a bond coat for a thermal barrier coating. The coating has a composition of, by weight, at least 6% to about 15% aluminum, about 2% to about 5% chromium, optionally one or more reactive elements in individual or combined amounts of up to 4%, optionally up to 2% silicon, optionally up to 60% of at least one platinum group metal, and the balance essentially nickel. A thermal-insulating ceramic layer may be deposited on the coating.
摘要翻译：用于敌对热环境中的物品的覆盖涂层。该涂层主要具有适合用作环境涂层和用作热障涂层的粘合涂层的γ初始相铝酸镍（Ni 3 Al 3 Al）组合物。该涂层具有按重量计至少6％至约15％的铝，约2％至约5％的铬，任选的一种或多种反应性元素的组合物，其个体或组合量可达4％，任选至多2 ％硅，任选至多60％的至少一种铂族金属，余量基本上为镍。绝热陶瓷层可以沉积在涂层上。

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