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1. 发明专利

JP2011157279A Rare earth complex, and fluorescent medium, light-emitting element, security medium and lighting device using the same 有权
标题翻译：稀土复合物，荧光介质，发光元件，安全中和使用其的照明装置
公开(公告)号：JP2011157279A
公开(公告)日：2011-08-18
申请号：JP2010017839
申请日：2010-01-29
申请人： Nitto Kasei Co Ltd , Toshiba Corp , 日東化成株式会社 , 株式会社東芝
发明人： IWANAGA HIRONORI , SATO TAKAHIRO , SASAOKA SHINICHI , ISHIDA TOSHIKAZU , WAZAKI TAKAHIRO
IPC分类号： C07F19/00 , C07C49/92 , C07F5/00 , C07F9/53 , C09K11/06 , H01L33/50 , H01L51/50
摘要： PROBLEM TO BE SOLVED: To provide a rare earth complex having high brightness and a long life, and to provide a fluorescent medium, a light-emitting medium, a security medium and a lighting device using the complex.
SOLUTION: The rare earth complex contains a plurality of rare earth ions, and a phosphine oxide ligand, and the phosphine oxide ligand has a molecular structure represented by formula (1) (wherein, m, n and o are each an integer of ≥1; R
1 to R
6 are the same or different and each saturated hydrocarbon which may be substituted, aryl which may be substituted, heteroaryl which may be substituted or aralkyl which may be substituted, and neighboring R
1 and R
2 , R
3 and R
4 or R
5 and R
6 on the same phosphorus atom may form a ring by bonding to each other).
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种具有高亮度和长寿命的稀土配合物，并提供荧光介质，发光介质，安全介质和使用该复合物的照明装置。解决方案：稀土配合物含有多个稀土离子和氧化膦配体，氧化膦配体具有由式（1）表示的分子结构（其中，m，n和o各自为整数 ≥1; R 1 至R 6相同或不同，可以被取代的每个饱和烃，可被取代的芳基，可被取代的杂芳基或芳烷基其可以被替代，并且相邻的R 1和R 2彼此之间是相互独立的，R 3 和R 4 或R

2. 发明专利

JP2007308411A Method for preparing bisphosphine oxide 有权
标题翻译：二氧化磷制备方法
公开(公告)号：JP2007308411A
公开(公告)日：2007-11-29
申请号：JP2006138329
申请日：2006-05-17
申请人： Nitto Kasei Co Ltd , 日東化成株式会社
发明人： ISHIDA TOSHIKAZU , SASAOKA SHINICHI
IPC分类号： C07F9/53 , C07B61/00
摘要： PROBLEM TO BE SOLVED: To provide a simple and high-yield method for preparing a bisphosphine oxide. SOLUTION: The method for preparing a bisphosphine oxide represented by formula (1) comprises steps of causing an organometallic reagent represented by a Grignard reagent to react with an diorganophosphite, causing the resulting reaction product to react with an intermediate halogenated compound to form a phosphine oxide represented by formula (5), and causing the resulting phosphine oxide represented by formula (5) to react with a phosphorous compound comprising a P-H bond capable of bonding to a double bond by an addition reaction in the presence of a catalyst. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：待解决的问题：提供制备双膦氧化物的简单且高产率的方法。解决方案：制备由式（1）表示的双膦氧化物的方法包括以下步骤：使由格氏试剂代表的有机金属试剂与二有机亚磷酸酯反应，使得到的反应产物与中间卤代化合物反应形成由式（5）表示的氧化膦和通过加成反应在催化剂存在下使得到的由式（5）表示的所得氧化膦与包含能够键合到双键的PH键的磷化合物反应。版权所有（C）2008，JPO＆INPIT

3. 发明专利

JP2010095514A Linear tetraphosphine tetraoxide, rare-earth metal complex comprising the linear tetraphosphine tetraoxide as ligand and use of the complex 审中-公开
标题翻译：线性四噻吩四氢呋喃，包含线性四噻吩四氢呋喃作为配体的稀土金属络合物和复合物的使用
公开(公告)号：JP2010095514A
公开(公告)日：2010-04-30
申请号：JP2009205616
申请日：2009-09-07
申请人： Nitto Kasei Co Ltd , 日東化成株式会社
发明人： ISHIDA TOSHIKAZU , WAZAKI TAKAHIRO , SASAOKA SHINICHI
IPC分类号： C07F9/53 , C07C49/92 , C07F5/00 , C09D11/00 , C09K11/06 , H01L51/50
CPC分类号： Y02B20/181
摘要： PROBLEM TO BE SOLVED: To provide a ligand for achieving a rare-earth metal complex stably exerting high emission intensity and exhibiting high solubility to organic media. SOLUTION: A linear tetraphosphine tetraoxide represented by general formula (1) [wherein, R 1 , R 2 , R 3 , R 4 , R 5 and R 6 represent the same or different (substituted) saturated hydrocarbon, (substituted) aryl, (substituted) heteroaryl or (substituted) aralkyl, or R 1 and R 2 , and R 5 and R 6 on the same phosphorus atom may be bonded to form a ring; and l, m and n each represents the same or different ≥2 integer] is provided. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供一种用于实现稳定地发挥高发光强度并且表现出对有机介质的高溶解度的稀土金属络合物的配体。解决方案：由通式（1）表示的线性四氧化膦四氧化物[其中，R 1，R 2，R 3，R 3，R 3，（取代的）芳基，（取代的）杂芳基或（取代的）杂芳基或（取代的）饱和烃，（取代的）取代的）芳烷基，或者在相同的磷原子上的R 1 SP 1和/或SP 2和/或SP 6 可以键合形成环; 并且l，m和n各自表示相同或不同的≥2整数]。版权所有（C）2010，JPO＆INPIT

4. 发明专利

JP2009107943A Method for producing bisphosphine oxide 审中-公开
标题翻译：生产二氧化磷氧化物的方法
公开(公告)号：JP2009107943A
公开(公告)日：2009-05-21
申请号：JP2007279425
申请日：2007-10-26
申请人： Nitto Kasei Co Ltd , 日東化成株式会社
发明人： WAZAKI TAKAHIRO , SASAOKA SHINICHI , ISHIDA TOSHIKAZU
IPC分类号： C07F9/53 , C07F9/54 , C07F9/6553
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a bisphosphine oxide, which allows the easy production of the compound in a high yield, while enabling the free molecular designing of the bisphosphine oxide. SOLUTION: This method for producing the bisphosphine oxide (1) comprises (I) a process of reacting a phosphonium salt (2) with a phosphorus compound (3) or a phosphorus compound (4) in the presence of a catalyst to obtain a phosphorus compound (5), and (II) a process of alkali-hydrolyzing the phosphorus compound (5) to produce the bisphosphine oxide (1). Another method for producing the bisphosphine oxide (1) comprises (I) a process of alkali-hydrolyzing the phosphonium salt (2) to produce a phosphine oxide (8), and (II) a process of reacting the phosphine oxide (8) with the phosphorus compound (3) or the phosphorus compound (4) in the presence of a catalyst to obtain the bisphosphine oxide (1). COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：待解决的问题：提供一种双膦氧化物的制备方法，其能够以高产率容易地生产化合物，同时能够进行双氧化膦的自由分子设计。解决方案：该制备双氧化膦（1）的方法包括（I）在催化剂存在下使鏻盐（2）与磷化合物（3）或磷化合物（4）反应的方法，得到磷化合物（5），（II）将磷化合物（5）碱解水解，生成双氧化膦（1）的方法。制备双氧化膦（1）的另一种方法包括（I）将鏻盐（2）碱解水解以生产氧化膦（8）的方法，和（II）使氧化膦（8）与磷化合物（3）或磷化合物（4）在催化剂存在下反应，得到双氧化膦（1）。版权所有（C）2009，JPO＆INPIT

5. 发明专利

JP2008091215A Tin oxide film former, tin oxide film formation method using it, and tin oxide film formed by it 审中-公开
标题翻译：氧化锌薄膜，氧化锌薄膜形成方法及其使用的氧化锌薄膜
公开(公告)号：JP2008091215A
公开(公告)日：2008-04-17
申请号：JP2006270898
申请日：2006-10-02
申请人： Nitto Kasei Co Ltd , 日東化成株式会社
发明人： OKADA TAKAYUKI , SASAOKA SHINICHI
IPC分类号： H01B13/00 , C01G19/02 , H01B5/14
摘要： PROBLEM TO BE SOLVED: To provide a tin oxide film former capable of forming a tin oxide film at low temperatures. SOLUTION: This tin oxide film former contains at least one kind out of organic tin compounds comprising: (1) a compound formed of one tin atom bonded to (p) organic groups each having a double bond at the β-position (when p is 2-4, the organic groups are identical or different from one another), any one kind within (m) halogen atoms, hydroxyl groups, alkoxy groups and acyloxy groups, and any one kind within (n) halogen atoms, hydroxyl groups, alkoxy groups and acyloxy groups (p is an integer of 1-4, m and n are each an integer of 0-3, and p+m+n=4); (2) a compound formed of one tin atom bonded to two organic groups each having a double bond at the β-position, and an oxygen atom bonded by one double bond; and (3) a compound formed of one tin atom bonded to one organic group having a double bond at the β-position, an oxygen atom bonded by one double bond, and one hydroxyl group; wherein the organic groups in (1), (2) and (3) are identical or different from one another. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种能够在低温下形成氧化锡膜的氧化锡成膜剂。该氧化锡成膜剂含有至少一种有机锡化合物，该有机锡化合物包括：（1）由一个锡原子键合到（p）有机基团的化合物，所述化合物在β-位上具有双键当p为2-4时，有机基团相同或不同），（m）卤素原子，羟基，烷氧基和酰氧基中的任何一种，（n）个卤素原子内的任何一种，羟基基团，烷氧基和酰氧基（p为1-4的整数，m和n各自为0-3的整数，p + m + n = 4）; （2）由在一个双键上具有双键的两个有机基团连接的一个锡原子和一个双键键合的氧原子形成的化合物; 和（3）由一个与β位上具有双键的有机基团结合的一个锡原子，一个双键键合的氧原子和一个羟基形成的化合物; 其中（1），（2）和（3）中的有机基团彼此相同或不同。版权所有（C）2008，JPO＆INPIT

6. 发明专利

JP2006316197A Process for producing polysilanes 审中-公开
标题翻译：生产多晶硅的工艺
公开(公告)号：JP2006316197A
公开(公告)日：2006-11-24
申请号：JP2005141566
申请日：2005-05-13
申请人： Nitto Kasei Co Ltd , 日東化成株式会社
发明人： KITAMURA HITOSHI , SASAOKA SHINICHI , IWAMOTO TAKESHI
IPC分类号： C08G77/60
摘要： PROBLEM TO BE SOLVED: To provide a process for producing a polysilane that requires no complicated operations, is excellent in safety and can be used for producing a desired polysilane at a low cost. SOLUTION: The process for producing a polysilane comprises allowing magnesium to act upon one or more kinds selected from the group consisting of a dihalosilane compound represented by formula (1): (R 1 ) 2 Si(X 1 ) 2 , a trihalosilane compound represented by formula (2): R 2 Si(X 2 ) 3 and a tetrahalosilane compound represented by formula (3): Si(X 3 ) 4 in a solvent in the presence of an alkali metal salt and a metal complex represented by formula (4). COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：为了提供不需要复杂操作的聚硅烷的制造方法，安全性优异，可以以低成本制造所需的聚硅烷。解决方案：聚硅烷的制造方法包括使镁作用于选自由式（1）表示的二卤代硅烷化合物中的一种或多种：（R 1 SP＆lt; SP＆gt;）SB 由式（2）表示的三卤代硅烷化合物：R（SP）2 Si（X 1 ）< （3）表示的四卤代硅烷化合物：在溶剂中的Si（X 3 ） 3 在由式（4）表示的碱金属盐和金属配合物的存在下进行。版权所有（C）2007，JPO＆INPIT

7. 发明专利

JP2011012020A Tetraphosphine tetraoxide, method for producing the same and use thereof 有权
标题翻译：四噻吩四氢呋喃，其生产方法及其用途
公开(公告)号：JP2011012020A
公开(公告)日：2011-01-20
申请号：JP2009157572
申请日：2009-07-02
申请人： Nitto Kasei Co Ltd , 日東化成株式会社
发明人： SASAOKA SHINICHI , WAZAKI TAKAHIRO , ISHIDA TOSHIKAZU
IPC分类号： C07F9/53 , C07B61/00 , C07F5/00
摘要： PROBLEM TO BE SOLVED: To provide a new phosphine oxide, a method for producing the compound and a method for extracting rare earth metals by using the compound.SOLUTION: Tetraphosphine tetraoxide is expressed by formula (1) (wherein Rand Rare each aryl or the like; and n is an integer of ≥2). A rare earth metal complex coordinated with the tetraphosphine tetraoxide is obtained by contacting the compound with a rear earth metal salt in a solvent. The compound is produced by reacting a compound (4) with diphenylphosphine oxide, or the like.
摘要翻译：要解决的问题：提供新的氧化膦，该化合物的制造方法和使用该化合物的稀土金属的提取方法。溶液：四氧化四铁由式（1）表示（其中，兰德稀有各芳基或 like; n为≥2的整数）。通过使化合物与溶剂中的后土金属盐接触，获得与四氧化四铁配位的稀土金属络合物。该化合物通过使化合物（4）与二苯基氧化膦等反应制备。

8. 发明专利

JP2009051787A Macrocyclic tetraphosphonium salt and method for producing the same, and method for producing macrocyclic phosphine tetraoxide 审中-公开
标题翻译：大分子四面体盐及其生产方法，以及生产大环磷酰四氢呋喃的方法
公开(公告)号：JP2009051787A
公开(公告)日：2009-03-12
申请号：JP2007221611
申请日：2007-08-28
申请人： Nitto Kasei Co Ltd , 日東化成株式会社
发明人： SASAOKA SHINICHI , ISHIDA TOSHIKAZU , WAZAKI TAKAHIRO
IPC分类号： C07F9/6568
摘要： PROBLEM TO BE SOLVED: To provide methods for easily producing a cyclic phosphine oxide and a cyclic phosphonium salt as its intermediate in high yield, respectively. SOLUTION: The method for producing a cyclic phosphonium salt of general formula (4) comprises the step (I) of conducting a reaction between a bisphosphinoalkane and an α, ω-dihalogenoalkane. The other method for producing a cyclic phosphine oxide comprises the step (II) of subjecting the cyclic phosphonium salt obtained by the step (I) to alkali hydrolysis. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：待解决的问题：提供分别容易地以高产率制备环氧化膦和环状鏻盐作为其中间体的方法。解决方案：制备通式（4）的环状鏻盐的方法包括在双膦酰基烷烃和α，ω-二卤代烷烃之间进行反应的步骤（I）。制备环氧化膦的另一种方法包括使由步骤（I）获得的环状鏻盐进行碱水解的步骤（II）。版权所有（C）2009，JPO＆INPIT

9. 发明专利

JP2007308412A Method for preparing bisphosphine oxide 有权
标题翻译：二氧化磷制备方法
公开(公告)号：JP2007308412A
公开(公告)日：2007-11-29
申请号：JP2006138330
申请日：2006-05-17
申请人： Nitto Kasei Co Ltd , 日東化成株式会社
发明人： ISHIDA TOSHIKAZU , SASAOKA SHINICHI
IPC分类号： C07F9/53 , C07F7/18 , C07F9/6553
摘要： PROBLEM TO BE SOLVED: To provide a simple and high-yield method for preparing a bisphosphine oxide. SOLUTION: The method for preparing a bisphosphine oxide represented by general formula (1) comprises steps of causing an organometallic reagent prepared from a halogenated compound represented by general formula (2) to react with a phosphorous compound represented by general formula (3) to form a phosphine oxide represented by general formula (4), and causing the phosphine oxide represented by general formula (4) to react with a phosphorous compound represented by general formula (5) or a phosphorous compound represented by general formula (6) in the presence of a catalyst. COPYRIGHT: (C)2008,JPO&INPIT

10. 发明专利

IN7743DEN2014A ELECTRODEPOSITION COATING COMPOSITION AND CATALYST FOR ELECTRODEPOSITION COATING COMPOSITION 未知
公开(公告)号：IN7743DEN2014A
公开(公告)日：2015-05-15
申请号：IN7743DEN2014
申请日：2014-09-17
申请人： NITTO KASEI CO LTD
发明人： SASAOKA SHINICHI , HANEDA HIDEO , ISHIDA TOSHIKAZU
IPC分类号： C09D201/00 , C09D5/44 , C09D7/12
摘要： The purpose of the present invention is to provide an organic tin free cationic electrodeposition coating composition which does not contain any organic tin compound and can ensure good coating film curability under baking conditions that are equivalent to those employed in the conventional techniques. The present invention provides an electrodeposition coating composition comprising a titanium compound (A) and a base resin (B) wherein the titanium compound (A) is a titanium compound having a specific structure.

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