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    • 2. 发明专利
    • Control method in plasma nitriding, and plasma nitriding system
    • 等离子体氮化物和等离子体氮化体系的控制方法
    • JP2008133518A
    • 2008-06-12
    • JP2006321560
    • 2006-11-29
    • Nissan Motor Co Ltd日産自動車株式会社
    • MATSUSHITA KAINCHIBA HIROTAKAUCHIYAMA NORIKOHONDA HIDEYUKI
    • C23C8/36H05H1/00
    • PROBLEM TO BE SOLVED: To provide a system which can precisely control the nitrogen energy during a plasma nitriding operation. SOLUTION: This control method in a plasma nitriding technique comprises the steps of: employing a signal which indicates an excited state of plasma during the plasma nitriding operation, as a measurement object; and controlling a plasma power source by feeding the measurement result back to the source. The control process includes: detecting a light from an aperture 5b of the side of a main body 5 of a furnace through a condensing lens system 3 during the plasma nitriding operation to determine the excited state of the plasma; guiding the detected light to an emission spectroscopy photometer 4 through an optical fiber 19; condensing the detected light with a condensing unit 19a; obtaining the spectrum of the light through a monochromator 17; detecting the spectrum with an ICCD detecting device 18 provided with a gate; and informing the intensity of the emission spectrum to a controller 20 through a signal line 21. The controller 20 has an interface 23 and a personal computer 22. The personal computer 22 calculates the intensity of the emission spectrum, compares the intensity with the preset intensity which has been set in an operating panel 25, and outputs the control signal corresponding to the difference between the intensities, to the plasma power source 8. COPYRIGHT: (C)2008,JPO&INPIT
    • 要解决的问题:提供一种能够在等离子体氮化操作期间精确控制氮能的系统。 解决方案:等离子体氮化技术中的这种控制方法包括以下步骤:在等离子体氮化操作期间采用表示等离子体的激发态的信号作为测量对象; 以及通过将测量结果馈送回源来控制等离子体电源。 控制过程包括:在等离子体氮化操作期间通过聚光透镜系统3从炉的主体5侧的孔5b检测光,以确定等离子体的激发状态; 将检测到的光通过光纤19引导到发射光谱光度计4; 用聚光单元19a冷凝检测到的光; 通过单色仪17获得光的光谱; 用设有门的ICCD检测装置18检测光谱; 并通过信号线21向控制器20通知发射光谱的强度。控制器20具有接口23和个人计算机22.个人计算机22计算发射光谱的强度,将强度与预设强度进行比较 其被设置在操作面板25中,并且将对应于强度差的控制信号输出到等离子体电源8.版权所有(C)2008,JPO&INPIT
    • 4. 发明专利
    • Metallic glass molded body and method for producing the same
    • 金属玻璃模制体及其制造方法
    • JP2011001588A
    • 2011-01-06
    • JP2009144655
    • 2009-06-17
    • Nissan Motor Co Ltd日産自動車株式会社
    • MATSUSHITA KAINYASUDA YOSHITERUKAWASHITA NOBUO
    • B22F3/00B22F1/02B22F3/14C22C45/02H01F1/153H01F1/24
    • PROBLEM TO BE SOLVED: To provide a method for producing a metallic glass molded body at low-cost, in which the degree of freedom in the shape of a part is high and cracking does not occur at processing of the part.SOLUTION: The method for producing the metallic glass molded body comprises: a first step of covering surfaces of base material particles essentially comprising a metallic glass with an insulating material containing an inorganic oxide so as to form insulating films and conducting press-molding of the base material particles so as to obtain a press-molded body in which pores are dispersed inside; and a second step of heating and further conducting press-molding of the press-molded body at a strain rate no larger than the plastic flow rate that occurs when the metallic glass component flows within the pores so as to obtain the metallic glass molded body.
    • 要解决的问题:提供一种低成本地制造金属玻璃成型体的方法,其中部件形状的自由度高,并且在加工部件时不会发生开裂。解决方案:该方法 用于制造金属玻璃成型体的步骤包括:第一步骤,用基本上包含金属玻璃的基材颗粒的表面覆盖含有无机氧化物的绝缘材料,以形成绝缘膜,并对基材颗粒进行加压成型,以便 得到孔分散在其内的压制体; 以及第二步骤,以不大于当金属玻璃组分在孔内流动而发生的塑性流动速率的应变速率加热和进一步进行加压成型体的压制成型,从而获得金属玻璃成型体。
    • 5. 发明专利
    • Sintered soft magnetic material, and its manufacturing method
    • 烧结软磁材料及其制造方法
    • JP2009135413A
    • 2009-06-18
    • JP2008186182
    • 2008-07-17
    • Nissan Motor Co Ltd日産自動車株式会社
    • MATSUSHITA KAINOWADA MASARUOTANI KEIZOYASUDA YOSHITERUYAMAGUCHI TAKUO
    • H01F1/24B22F1/02H02K1/02
    • PROBLEM TO BE SOLVED: To provide a sintered soft magnetic material capable of enduring use in a high-revolution compact motor.
      SOLUTION: This sintered soft magnetic material comprises; base material particles containing iron being a ferromagnetic material as a main constituent; an intermediate layer covering the base material particles and formed of a metal; an insulating coating covering the intermediate layer and formed of an inorganic oxide; a mutual diffusion layer present on an interface between the base material particles and the intermediate layer; a nonstoichiometric oxide layer present on an interface between the intermediate layer and the insulating coating. In the sintered soft magnetic material, the oxide of the metal has standard free energy of formation larger than that of the inorganic oxide, and the nonstoichiometric oxide layer contains a reactant between the metal and/or the inorganic oxide and oxygen.
      COPYRIGHT: (C)2009,JPO&INPIT
    • 要解决的问题:提供一种耐久性高的小型电动机中使用的烧结软磁性材料。 该解决方案:该烧结软磁材料包括: 以铁磁材料为主要成分的含铁的基材粒子; 覆盖基材颗粒并由金属形成的中间层; 覆盖中间层并由无机氧化物形成的绝缘涂层; 存在于基材颗粒与中间层之间的界面上的相互扩散层; 存在于中间层和绝缘涂层之间的界面上的非化学计量氧化层。 在烧结软磁材料中,金属的氧化物具有大于无机氧化物的标准形成自由能,非化学计量氧化物层在金属和/或无机氧化物与氧之间含有反应物。 版权所有(C)2009,JPO&INPIT
    • 6. 发明专利
    • Metallic glass compact and method for manufacturing the same
    • 金属玻璃紧固件及其制造方法
    • JP2010138439A
    • 2010-06-24
    • JP2008314969
    • 2008-12-10
    • Nissan Motor Co Ltd日産自動車株式会社
    • MATSUSHITA KAINYASUDA YOSHITERUYAMAGUCHI TAKUO
    • C22C33/02B22F1/02B22F3/00C22C45/02H01F1/153H01F1/24H01F41/02H02K1/02H02K15/12
    • PROBLEM TO BE SOLVED: To provide a method for manufacturing a metallic glass compact which constitutes a powder magnetic core and can enhance the strength. SOLUTION: The method for manufacturing the metallic glass compact includes the steps of: heating the substrate particles each containing metallic glass as a main constituent while pressurizing them, and sintering a particulates body of the substrate particles. The sintering step can be divided into two stages. The first stage includes pressurizing the substrate particles so that the density of the particulates body becomes less than 90% of true density while reducing a ratio of voids among the substrate particles which constitute the particulates body, when heating the substrate particles to a temperature lower than the glass transition temperature of the metallic glass. Thereby, the density of the particulates body is enhanced. The subsequent second stage includes pressurizing the substrate particles under the condition that a distortion-varying rate (%/°C) of the particulates body with respect to the unit temperature is larger than that in the first stage, while further heating the particulates body in a range of the Tg or higher but lower than the Tx of the metallic glass. COPYRIGHT: (C)2010,JPO&INPIT
    • 要解决的问题:提供一种制造构成粉末磁芯并可提高强度的金属玻璃压块的方法。 解决方案:用于制造金属玻璃压块的方法包括以下步骤:加热每个包含金属玻璃作为主要成分的基底颗粒,同时对其加压,并烧结基底颗粒的微粒体。 烧结步骤可分为两个阶段。 第一阶段包括对基材颗粒进行加压,使得当将基体颗粒加热至低于(或)的温度时,颗粒体的密度变得小于真密度的90%,同时减小构成颗粒体的基材颗粒之间的空隙比) 金属玻璃的玻璃化转变温度。 由此,能够提高微粒体的密度。 随后的第二阶段包括在微粒体相对于单元温度的变形变化率(%/℃)大于第一阶段的变形率(%/℃)的情况下,同时将微粒体进一步加热的条件下对基材颗粒进行加压 Tg或更高但低于金属玻璃的Tx的范围。 版权所有(C)2010,JPO&INPIT
    • 7. 发明专利
    • Molded product of metal glass, and method of producing the same
    • 金属玻璃的模制产品及其生产方法
    • JP2010138438A
    • 2010-06-24
    • JP2008314967
    • 2008-12-10
    • Nissan Motor Co Ltd日産自動車株式会社
    • MATSUSHITA KAINYASUDA YOSHITERUYAMAGUCHI TAKUO
    • B22F3/00B22F1/02B22F3/10H01F1/24H02K1/02H02K15/02
    • PROBLEM TO BE SOLVED: To provide a method of producing a metal glass formed body which composes a powder magnetic core, and whose strength can be improved.
      SOLUTION: The method is used for producing the metal glass formed body composed of: a metal glass; an insulation film composed of an inorganic oxide covering the metal glass; and a mutual diffusion layer present on the grain boundary between the metal glass and the insulation film. The production method includes: a stage where sintering is performed at the glass transition temperature of the metal glass or above and less than the crystallization starting temperature; and a cooling stage where, subsequently to the sintering stage, after cooling is started, during the cooling while lowering temperature, the temperature is held at a constant temperature.
      COPYRIGHT: (C)2010,JPO&INPIT
    • 解决的问题:提供一种制造构成粉末磁芯的金属玻璃成形体的方法,其强度可以得到改善。 解决方案:该方法用于制造金属玻璃成形体,其由金属玻璃构成; 由覆盖金属玻璃的无机氧化物构成的绝缘膜; 以及存在于金属玻璃和绝缘膜之间的晶界上的相互扩散层。 制造方法包括:在金属玻璃的玻璃化转变温度以上且小于结晶起始温度进行烧结的阶段; 以及冷却阶段,在冷却开始之后,在烧结阶段之后,在降温的同时,将温度保持在恒定温度。 版权所有(C)2010,JPO&INPIT
    • 8. 发明专利
    • Method of manufacturing transition metal nitride
    • 制造金属过渡金属的方法
    • JP2008138265A
    • 2008-06-19
    • JP2006326961
    • 2006-12-04
    • Nissan Motor Co Ltd日産自動車株式会社
    • MATSUSHITA KAINUCHIYAMA NORIKOCHIBA HIROTAKAHONDA HIDEYUKI
    • C23C8/80C23C8/26C23G1/08H01M8/02H01M8/10
    • Y02P70/56
    • PROBLEM TO BE SOLVED: To provide a transition metal nitride containing a low oxygen content and a high nitrogen content. SOLUTION: A base material comprising a stainless steel is subjected to gas nitriding to form a transition metal nitride on a surface layer part of the base material. A transition metal nitride layer containing the high oxygen content formed by the gas nitriding is removed by applying surface treatment to the surface part of the surface layer using a phosphoric acid-based solution or a solution containing a phosphoric acid and a fluoride-based solution. Thus, the transition metal nitride layer containing the low oxygen content and high nitrogen content is left behind on the surface of the base material. Since the transition metal nitride contains the low oxygen content and high nitrogen content, it has excellent conductivity. COPYRIGHT: (C)2008,JPO&INPIT
    • 待解决的问题:提供含有低氧含量和高氮含量的过渡金属氮化物。 解决方案:将包含不锈钢的基材进行气体氮化,以在基材的表面层部分上形成过渡金属氮化物。 通过使用磷酸类溶液或含有磷酸和氟化物类溶液的溶液对表层的表面部进行表面处理,除去含有由气体氮化形成的高氧含量的过渡金属氮化物层。 因此,含有低氧含量和高氮含量的过渡金属氮化物层留在基材的表面上。 由于过渡金属氮化物含有低氧含量和高氮含量,因此具有优异的导电性。 版权所有(C)2008,JPO&INPIT