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1. 发明专利

JP2013006786A Method for producing fluorinated alkane 审中-公开
标题翻译：生产氟化碱的方法
公开(公告)号：JP2013006786A
公开(公告)日：2013-01-10
申请号：JP2011139071
申请日：2011-06-23
申请人： Nippon Zeon Co Ltd , 日本ゼオン株式会社
发明人： SUGIMOTO TATSUYA
IPC分类号： C07C17/093 , C07C19/08
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a fluorinated alkane in a good yield, in fluorinating an alkyl sulfonate by an interchange reaction with an alkali metal fluoride.SOLUTION: This method can produce the target fluorinated alkane in a good yield by virtue of using a reactor equipped with a screw type agitation blades or a rotary kiln type reactor in an interchange reaction with an alkali metal fluoride, even in a reaction pattern yielding a massive amount of solid contents.
摘要翻译：待解决的问题：为了提供以高产率生产氟化烷烃的方法，通过与碱金属氟化物的交换反应氟化烷基磺酸盐。解决方案：该方法可以通过使用装有螺旋式搅拌叶片的反应器或与碱金属氟化物进行交换反应的回转窑式反应器，即使在反应中也能以良好的产率生产目标氟化烷烃形成大量固体含量。版权所有（C）2013，JPO＆INPIT

2. 发明专利

JP2012188359A Processes for producing halogenofluorinated cycloalkane and hydrofluorinated cycloalkane 有权
标题翻译：产生卤代环丙烷和氢化环己酮的方法
公开(公告)号：JP2012188359A
公开(公告)日：2012-10-04
申请号：JP2011051035
申请日：2011-03-09
申请人： Nippon Zeon Co Ltd , 日本ゼオン株式会社
发明人： SUGIMOTO TATSUYA
IPC分类号： C07C17/04 , C07C17/354 , C07C23/06 , C07C23/08
摘要： PROBLEM TO BE SOLVED: To provide processes for producing a halogenofluorinated cycloalkane and a hydrofluorinated cycloalkane.SOLUTION: A treatment of a fluorinated cycloalkene with a halogenating agent having n-Y bonds (Y is a chlorine atom or a bromine atom) in the presence of an alkaline metal fluoride can convert the fluorinated cycloalkene to a gem-halogenofluorinated cycloalkane. Hydrogenation of the gem-halogenofluorinated cycloalkane can produce a 1H,1H-fluorinated cycloalkane.
摘要翻译：待解决的问题：提供制备卤代氟化环烷烃和氢氟化环烷烃的方法。解决方案：在碱金属氟化物的存在下，用具有n-Y键（Y为氯原子或溴原子）的卤化剂处理氟化环烯烃可将氟化环烯烃转化为偕 - 卤代氟化环烷烃。偕 - 卤代氟化环烷烃的氢化可以产生1H，1H-氟化的环烷烃。版权所有（C）2013，JPO＆INPIT

3. 发明专利

JP2012171884A Method of producing hydrogen-containing fluorodiene compound 审中-公开
标题翻译：生产含氢氟烷化合物的方法
公开(公告)号：JP2012171884A
公开(公告)日：2012-09-10
申请号：JP2011033361
申请日：2011-02-18
申请人： Nippon Zeon Co Ltd , 日本ゼオン株式会社
发明人： SUGIMOTO TATSUYA
IPC分类号： C07C17/23 , C07B61/00 , C07C21/18
摘要： PROBLEM TO BE SOLVED: To provide a method of industrially producing a hydrogen-containing fluorodiene compound.SOLUTION: The method of producing a hydrogen-containing fluorodiene compound includes (1) treating a compound represented by formula: ClCH-CHCl-CClX-CHClY (X and Y are each different and represent a chlorine atom or a hydrogen atom) with a fluorine gas to produce a compound represented by formula: ClCF-CFCl-CClZ-CFClW (Z and W are each different and represent a fluorine atom or a chlorine atom), (2) then hydrogenating the resulting compound to produce a compound represented by formula: ClCF-CFCl-CClT-CFClU (T and U are each different and represent a hydrogen atom or a fluorine atom), and (3) then dechlorinating the resulting compound to produce a hydrogen-containing fluorodiene represented by formula: CF=CFCT=CFU (T and U are each different and represent a hydrogen atom or a fluorine atom).
摘要翻译：待解决的问题：提供工业生产含氢氟二烯化合物的方法。解决方案：含氢氟二烯化合物的制造方法包括：（1）处理由下式表示的化合物：ClCH - > Cl - CClX-CHClY（X和Y 各自不同，表示氯原子或氢原子）与氟气反应以制备由下式表示的化合物：C CFCl-CClZ-CFClW（Z和W分别为各自不同，表示氟原子或氯原子），（2）然后氢化所得化合物以制备由下式表示的化合物：ClCF -CFCl-CClT-CFClU（ T和U各自不同，表示氢原子或氟原子），（3）然后使所得化合物脱氯以制备由下式表示的含氢氟二烯：CF 2

4. 发明专利

JP2009269892A New halogen-containing compound and method for producing the same 有权
标题翻译：新的含氢化合物及其生产方法
公开(公告)号：JP2009269892A
公开(公告)日：2009-11-19
申请号：JP2008124376
申请日：2008-05-12
申请人： Nippon Zeon Co Ltd , 日本ゼオン株式会社
发明人： NAKASUGI SHIGEMASA , ISHIMURA TAKAYUKI , SUGIMOTO TATSUYA
IPC分类号： C07C49/16 , C07C17/18 , C07C17/25 , C07C19/10 , C07C21/18 , C07C45/63
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a new halogen-containing ketone compound, a halogen-containing alkene compound and a halogen-containing alkane compound which are precursors of a perfluoroalkyne compound used as a production raw material of a fluorine-containing polymer, a medicine or an agrochemical, and as a gas for a plasma reaction used in a semiconductor production process, in high yields and high selectivity. SOLUTION: This new halogen-containing ketone compound is obtained by reacting chlorine, bromine or iodine with a ketone compound as a starting material, and then by performing a reaction with phosphorus pentachloride, the new halogen-containing alkene compound and new halogen-containing alkane compound are obtained. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：提供一种制备新的含卤素酮化合物，含卤素的烯烃化合物和含卤素的烷烃化合物的方法，它们是用作生产原料的全氟炔化合物的前体含氟聚合物，药物或农用化学品，以及用于半导体生产过程中用于等离子体反应的气体，以高产率和高选择性。解决方案：这种新的含卤素酮化合物是通过使氯，溴或碘与酮化合物作为原料反应，然后通过与五氯化磷反应，新的含卤素的烯烃化合物和新的卤素的烷烃化合物。版权所有（C）2010，JPO＆INPIT

5. 发明专利

JP2009149701A Azeotropic mixture composition, azeotropic mixture-like composition, cleaning solvent and coating solvent 审中-公开
标题翻译： AZEOTROPIC MIXTURE组合物，AZEOTROPIC混合物组合物，清洁溶剂和涂料溶剂
公开(公告)号：JP2009149701A
公开(公告)日：2009-07-09
申请号：JP2007326166
申请日：2007-12-18
申请人： Nippon Zeon Co Ltd , 日本ゼオン株式会社
发明人： KIYAMA HARUYUKI , SUGIMOTO TATSUYA
IPC分类号： C11D7/50 , B08B3/08 , C09D7/12 , C09D201/00 , C11D3/44
摘要： PROBLEM TO BE SOLVED: To provide an azeotropic mixture composition, an azeotropic mixture-like composition, a cleaning solvent and a coating solvent using the composition, the composition which is stable causing no depletion of an ozone layer, has excellent material applicability, excellent dissolving performance, cleaning performance and cleaning finishing property, and hardly ignites.
SOLUTION: The azeotropic mixture composition or the azeotropic mixture-like composition, contains 85 to 95 wt.% of 1,1,2,2,3,3,4-heptafluorocyclopentane and 5 to 15 wt.% of 1,1,1,2,2,3,4,5,5,5-decafluoro-3-methoxy-4-(trifluoromethyl)-pentane. The cleaning solvent and the coating solvent comprise the above composition.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：为了使用该组合物提供共沸混合物组合物，共沸混合物组合物，清洗溶剂和涂布溶剂，稳定而不会耗尽臭氧层的组合物具有优异的材料适用性优异的溶解性能，清洁性能和清洁整理性能，几乎不点燃。解决方案：共沸混合物组合物或共沸混合物组合物含有85至95重量％的1,1,2,2,3,3,4-七氟环戊烷和5至15重量％的1， 1,1,2,2,3,4,5,5,5-十氟-3-甲氧基-4-（三氟甲基） - 戊烷。清洗溶剂和涂料溶剂包括上述组合物。版权所有（C）2009，JPO＆INPIT

6. 发明专利

JP2004292329A Method for producing perfluoroalkyne compound 有权
公开(公告)号：JP2004292329A
公开(公告)日：2004-10-21
申请号：JP2003084471
申请日：2003-03-26
申请人： Nippon Zeon Co Ltd , 日本ゼオン株式会社
发明人： SUGIMOTO TATSUYA , SUZUKI TAKEFUMI , YAMADA TOSHIRO
IPC分类号： C07C17/25 , C07B61/00 , C07C21/22
摘要： PROBLEM TO BE SOLVED: To provide a method for efficiently, industrially and advantageously producing a perfluoroalkyne compound useful as a gas for a plasma reaction, a raw material for producing fluorine-containing polymers, medicines or agrochemicals, an etching agent, or the like, used in a semiconductor production process.
SOLUTION: This method for producing the perfluoroalkyne compound is carried out as follows. A dihydrohalogenoalkane compound (formula 1) and/or a monohydrohalogenoalkene compound (formula 2) represented by the following formulae (formula 1) R
1 -CHA-CHB-R
2 (wherein, R
1 and R
2 are each mutually same or different and are each a 1-6C perfluoroalkyl group; and A and B are each independently a halogen atom selected from F, Cl, Br and I) and (formula 2) R
1 -CX=CY-R
2 (wherein, either one of X and Y is hydrogen and the other is a halogen atom selected from F, Cl, Br and I) are reacted in the presence of a basic compound or zeolite.
COPYRIGHT: (C)2005,JPO&NCIPI

7. 发明专利

JP2013095669A Method for producing fluorine-containing alkane 审中-公开
标题翻译：生产含氟烷烃的方法
公开(公告)号：JP2013095669A
公开(公告)日：2013-05-20
申请号：JP2011236720
申请日：2011-10-28
申请人： Nippon Zeon Co Ltd , 日本ゼオン株式会社
发明人： SUGIMOTO TATSUYA
IPC分类号： C07C17/16 , C07C19/08
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a fluorinated alkane by which damage due to hydrogen fluoride can be reduced and the yield of the fluorinated alkane can be increased in the method for producing fluorinated alkanes using a fluorine-containing ylide as a fluorinating agent.SOLUTION: Hydrogen fluoride is added to olefins and the amount of free hydrogen fluoride is reduced by adding olefins when fluorinated alkanes are produced from alcohols using the fluorine-containing ylide as the fluorinating agent.
摘要翻译：待解决的问题：提供一种氟化烷烃的制备方法，其中使用氟含量的氟化烷烃的制造方法可以降低由于氟化氢引起的损伤并且可以提高氟化烷烃的收率作为氟化剂。解决方案：当使用含氟叶立德作为氟化剂由醇制备氟化烷烃时，通过加入烯烃，将氟化氢加入到烯烃中，游离氟化氢的量减少。版权所有（C）2013，JPO＆INPIT

8. 发明专利

JP2011144148A Hydrogen-containing halogenated cyclopentane, and method for producing heptafluorocyclopentene 审中-公开
标题翻译：含氢化的环戊烷酮，以及生产氢溴酸环戊酯的方法
公开(公告)号：JP2011144148A
公开(公告)日：2011-07-28
申请号：JP2010007758
申请日：2010-01-18
申请人： Nippon Zeon Co Ltd , 日本ゼオン株式会社
发明人： SUGIMOTO TATSUYA
IPC分类号： C07C17/10 , C07B61/00 , C07C17/25 , C07C23/08
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a monohalogenoheptafluorocyclopentane and 1H-heptafluorocyclopentene from 1H, 1H, 2H-heptafluorocyclopentane by-produced when producing the 1H-heptafluorocyclopentene by vapor-phase hydrogenation reaction or the like of chloroheptafluorocyclopentene on a noble metal catalyst.
SOLUTION: The halogenoheptafluorocyclopentane is produced by bringing 1H, 1H, 2H-heptafluorocyclopentane into contact with a halogenation agent in the presence of a radical source. The halogenoheptafluorocyclopentane is brought into contact with an alkaline material to cause dehydrohalogenation reaction to provide the 1H-heptafluorocyclopentene.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供一种在通过气相氢化反应等制备1H-七氟环戊烯时在1H，1H，2H-七氟环戊烷上生成单卤代四氟环戊烷和1H-七氟环戊烯的方法，贵金属催化剂。解决方案：在自由基源存在下使1H，1H，2H-七氟环戊烷与卤化剂接触来制备卤代五氟环戊烷。使卤代五氟环戊烷与碱性物质接触以引起脱卤化氢反应以提供1H-七氟环戊烯。版权所有（C）2011，JPO＆INPIT

9. 发明专利

JP2011105625A Method of isomerizing heptafluorocyclopentene, and use thereof 审中-公开
标题翻译：异丙基环戊烯的异构化方法及其用途
公开(公告)号：JP2011105625A
公开(公告)日：2011-06-02
申请号：JP2009260942
申请日：2009-11-16
申请人： Nippon Zeon Co Ltd , 日本ゼオン株式会社
发明人： SUGIMOTO TATSUYA
IPC分类号： C07C5/25 , B01J27/12 , B01J31/02 , C07B61/00 , C07C23/08
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method of isomerizing 3H-heptafluorocyclopentene and 4H-heptafluorocyclopentene. SOLUTION: The 3H-heptafluorocyclopentene and/or the 4H-heptafluorocyclopentene can be isomerized into 1H-heptafluorocyclopentene by causing the same to contact a metal fluoride. By using the process, 1H-heptafluorocyclopentene of higher purity can be obtained. Specifically, the method of producing 1H-heptafluorocyclopentene includes: dehydrofluorinating 1H, 2H-octafluorocyclopentane to produce 1H-heptafluorocyclopentene comprising 3H-heptafluorocyclopentene and/or 4H-heptafluorocyclopentene; isomerizing the resulting 3H-heptafluorocyclopentene and/or 4H-heptafluorocyclopentene present in the 1H-heptafluorocyclopentene; and subsequently distilling the reaction product to obtain highly pure 1H-heptafluorocyclopentene. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供3H-七氟环戊烯和4H-七氟环戊烯异构化的方法。解决方案：3H-七氟环戊烯和/或4H-七氟环戊烯可以通过使其与金属氟化物接触而异构化成1H-七氟环戊烯。通过使用该方法，可以获得更高纯度的1H-七氟环戊烯。具体地说，制备1H-七氟环戊烯的方法包括：将1H，2H-八氟环戊烷脱氟化氢，得到包含3H-七氟环戊烯和/或4H-七氟环戊烯的1H-七氟环戊烯; 异构化存在于1H-七氟环戊烯中的所得3H-七氟环戊烯和/或4H-七氟环戊烯; 随后蒸馏反应产物得到高纯度的1H-七氟环戊烯。版权所有（C）2011，JPO＆INPIT

10. 发明专利

JP2010229116A Method for producing 2-halogeno-3-hydroperfluoroalkene compound 审中-公开
标题翻译： 2-卤代-3-羟基喹啉酮化合物的制备方法
公开(公告)号：JP2010229116A
公开(公告)日：2010-10-14
申请号：JP2009081286
申请日：2009-03-30
申请人： Nippon Zeon Co Ltd , 日本ゼオン株式会社
发明人： NAKASUGI SHIGEMASA , ISHIMURA TAKAYUKI , SUGIMOTO TATSUYA , TSUTSUMI TAKASHI
IPC分类号： C07C17/20 , C07C21/18
摘要： PROBLEM TO BE SOLVED: To provide a method for industrially advantageously synthesizing a 2-halogeno-3-hydroperfluoroalkene compound.
SOLUTION: A 3-hydroperfluoroalkene compound represented by formula A: CF
3 CF=CH(CF
2 )
n CF
3 (wherein n is an integer of 1-5) and a 2-hydroperfluoroalkene compound represented by formula B: CF
3 CH=CF(CF
2 )
n CF
3 (wherein n is an integer of 1-5) are halogenated with a halogenating agent in the presence of a catalyst to produce the 2-halogeno-3-hydroperfluoroalkene compound represented by formula C: CF
3 CX=CH(CF
2 )CF
3 (wherein X is chlorine, bromine or iodine and n is an integer of 1-5).
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供工业上有利地合成2-卤代-3-氢氟烯基化合物的方法。解决方案：由式A表示的3-氢氟烯基化合物：CF 3 SB = CF（CF 2 SBB）CF 3 SBB 3 （其中n为1-5的整数）和由式B表示的2-氢全氟烯烃化合物：CF 3 SB = CF（CF 2 ）在催化剂存在下，用卤化剂卤化CF 3 SB（其中n为1-5的整数），生成2-卤代-3-氢氟烯烃由式C表示的化合物：CF 3 SB = CH（CF 2 SBR）CF 3 SB（其中X是氯，溴或碘，n是 1-5的整数）。版权所有（C）2011，JPO＆INPIT

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