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1. 发明授权

US08889009B2 Process for purifying low molecular weight hydridosilanes 有权
标题翻译：纯化低分子量硅藻土的方法
公开(公告)号：US08889009B2
公开(公告)日：2014-11-18
申请号：US13123827
申请日：2009-10-09
申请人： Nicole Brausch , Goetz Baumgarten , Guido Stochniol , Yuecel Oenal , Martin Trocha
发明人： Nicole Brausch , Goetz Baumgarten , Guido Stochniol , Yuecel Oenal , Martin Trocha
IPC分类号： C01B33/04 , C07F7/02 , B01D61/00
CPC分类号： C01B33/04 , B01D61/00 , C01B33/046 , Y02P20/582
摘要： The present invention relates to a process for purifying low molecular weight hydridosilane solutions, in which a solution to be purified comprising a) at least one low molecular weight hydridosilane, b) at least one solvent and c) at least one impurity selected from the group of the compounds having at least 20 silicon atoms and/or the group of the homogeneous catalyst systems is subjected to a crossflow membrane process with at least one membrane separation step using a permeation membrane.
摘要翻译：本发明涉及一种用于纯化低分子量氢硅烷溶液的方法，其中待纯化的溶液包含a）至少一种低分子量氢硅烷，b）至少一种溶剂和c）至少一种选自以下的杂质：的具有至少20个硅原子的化合物和/或该均相催化剂体系的组合，使用渗透膜进行至少一个膜分离步骤的横流膜方法。

2. 发明申请

US20110268642A1 PROCESS FOR PURIFYING LOW MOLECULAR WEIGHT HYDRIDOSILANES 有权
标题翻译：净化低分子量水合物的方法
公开(公告)号：US20110268642A1
公开(公告)日：2011-11-03
申请号：US13123827
申请日：2009-10-09
申请人： Nicole Brausch , Goetz Baumgarten , Guido Stochniol , Yuecel Oenal , Martin Trocha
发明人： Nicole Brausch , Goetz Baumgarten , Guido Stochniol , Yuecel Oenal , Martin Trocha
IPC分类号： C01B33/04
CPC分类号： C01B33/04 , B01D61/00 , C01B33/046 , Y02P20/582
摘要： The present invention relates to a process for purifying low molecular weight hydridosilane solutions, in which a solution to be purified comprising a) at least one low molecular weight hydridosilane, b) at least one solvent and c) at least one impurity selected from the group of the compounds having at least 20 silicon atoms and/or the group of the homogeneous catalyst systems is subjected to a crossflow membrane process with at least one membrane separation step using a permeation membrane.
摘要翻译：本发明涉及一种用于纯化低分子量氢硅烷溶液的方法，其中待纯化的溶液包含a）至少一种低分子量氢硅烷，b）至少一种溶剂和c）至少一种选自以下的杂质：的具有至少20个硅原子的化合物和/或该均相催化剂体系的组合，使用渗透膜进行至少一个膜分离步骤的横流膜方法。

3. 发明申请

US20110189072A1 PROCESS FOR PREPARING HIGHER HYDRIDOSILANES 失效
标题翻译：制备高水解硅藻土的方法
公开(公告)号：US20110189072A1
公开(公告)日：2011-08-04
申请号：US12999151
申请日：2009-05-25
申请人： Nicole Brausch , Andre Ebbers , Guido Stochniol , Martin Trocha , Yücel Önal , Jörg Sauer , Bernhard Stützel , Dorit Wolf , Harald Stüger
发明人： Nicole Brausch , Andre Ebbers , Guido Stochniol , Martin Trocha , Yücel Önal , Jörg Sauer , Bernhard Stützel , Dorit Wolf , Harald Stüger
IPC分类号： C01B33/021 , C01B33/04
CPC分类号： C01B33/04
摘要： Process for preparing higher hydridosilanes of the general formula H—(SiH2)n—H where n≧2, in which—one or more lower hydridosilanes—hydrogen, and—one or more transition metal compounds comprising elements of transition group VIII of the Periodic Table and the lanthanides are reacted at a pressure of more than 5 bar absolute, subsequently depressurized and the higher hydridosilanes are separated off from the reaction mixture obtained.
摘要翻译：制备通式为H（SiH 2）n -H的高级羟基硅烷的方法，其中n≥2，其中一个或多个低级羟基硅烷 - 氢，以及包含元素周期表第八族元素的一种或多种过渡金属化合物表和镧系元素在大于5巴绝对压力下反应，随后减压，并从所得反应混合物中分离出较高的氢硅烷。

4. 发明授权

US08741253B2 Process for preparing higher hydridosilanes 失效
标题翻译：制备高级羟基硅烷的方法
公开(公告)号：US08741253B2
公开(公告)日：2014-06-03
申请号：US12999151
申请日：2009-05-25
申请人： Nicole Brausch , Andre Ebbers , Guido Stochniol , Martin Trocha , Yücel Önal , Jörg Sauer , Bernhard Stützel , Dorit Wolf , Harald Stüger
发明人： Nicole Brausch , Andre Ebbers , Guido Stochniol , Martin Trocha , Yücel Önal , Jörg Sauer , Bernhard Stützel , Dorit Wolf , Harald Stüger
IPC分类号： C01B33/04
CPC分类号： C01B33/04
摘要： Process for preparing higher hydridosilanes of the general formula H—(SiH2)n—H where n≧2, in which—one or more lower hydridosilanes—hydrogen, and—one or more transition metal compounds comprising elements of transition group VIII of the Periodic Table and the lanthanides are reacted at a pressure of more than 5 bar absolute, subsequently depressurized and the higher hydridosilanes are separated off from the reaction mixture obtained.
摘要翻译：制备通式为H（SiH 2）n -H的高级羟基硅烷的方法，其中n≥2，其中一个或多个低级羟基硅烷 - 氢，以及包含元素周期表第八族元素的一种或多种过渡金属化合物表和镧系元素在大于5巴绝对压力下反应，随后减压，并从所得反应混合物中分离出较高的氢硅烷。

5. 发明申请

US20050171389A1 Method for the hydroformylation of olefins 有权
标题翻译：烯烃加氢甲酰化的方法
公开(公告)号：US20050171389A1
公开(公告)日：2005-08-04
申请号：US10506603
申请日：2003-03-08
申请人： Walter Totsch , Detlef Arnoldi , Alfred Kaizik , Martin Trocha
发明人： Walter Totsch , Detlef Arnoldi , Alfred Kaizik , Martin Trocha
IPC分类号： C07B61/00 , C07C29/141 , C07C29/16 , C07C31/125 , C07C45/50 , C07C45/75 , C07C45/80 , C07C45/82 , C07C27/22 , C07C29/15
CPC分类号： C07C29/141 , C07C29/16 , C07C45/50 , C07C31/125 , C07C47/02
摘要： The invention relates to a process for preparing alcohols by hydroformylation of olefins or olefin mixtures, separation from the catalyst and subsequent hydrogenation, with an extraction being carried out after removal of the catalyst and before the hydrogenation of the aldehydes.
摘要翻译：本发明涉及通过烯烃或烯烃混合物的加氢甲酰化，从催化剂分离和随后的氢化制备醇的方法，在除去催化剂之后和醛的氢化之前进行萃取。

6. 发明授权

US09017630B2 Method for producing hydridosilanes 有权
标题翻译：生产氢硅烷的方法
公开(公告)号：US09017630B2
公开(公告)日：2015-04-28
申请号：US13504331
申请日：2010-11-08
申请人： Stephan Wieber , Matthias Patz , Martin Trocha , Hartwig Rauleder , Ekkehard Mueh , Harald Stueger , Christoph Walkner
发明人： Stephan Wieber , Matthias Patz , Martin Trocha , Hartwig Rauleder , Ekkehard Mueh , Harald Stueger , Christoph Walkner
IPC分类号： C01B33/04 , C01B33/107
CPC分类号： C01B33/04 , C01B33/043 , C01B33/10773 , Y10T428/31663
摘要： The invention relates to a method for producing hydridosilanes from halosilanes by a) reacting i) at least one halosilane of the generic formula SinX2n+2 (with n≧3 and X═F, Cl, Br and/or I) with ii) at least one catalyst of the generic formula NRR'aR″bYc with a=0 or 1, b=0 or 1, and c=0 or 1, and formula (I), wherein aa) R, R′ and/or R″ are —C1-C12 alkyl, —C1-C12 aryl, —C1-C12 aralkyl, —C1-C12 aminoalkyl, —C1-C12 aminoaryl, —C1-C12 aminoaralkyl, and/or two or three groups R, R′ and R″ (if c=0) together form a cyclic or bicyclic, heteroaliphatic or heteroaromatic system including N, with the proviso that at least one group R, R′ or R″ is unequal —CH3 and/or wherein bb) R and R′ and/or R″' (if c=1) are —C1-C12 alkylene, —C1-C12 arylene, —C1-C12 aralkylene, —C1-C12 heteroalkylene, —C1-C12 heteroarylene, —C1-C12 heteroaralkylene and/or —N═, or cc) (if a=b=c=0) R═≡C-R′″ (with R′″═—C1-C10 alkyl, —C1-C10 aryl and/or —C1-C10 aralkyl), while forming a mixture comprising at least one halosilane of the generic formula SimX2m+2 (with m>n and X═F, Cl, Br and/or I) and SiX4 (with X═F, Cl, Br and/or I), and b) hydrogenating the at least one halosilane of the generic formula SimH2m+2 while forming a hydridosilane of the generic formula SimH2m+2. The invention also relates to the hydridosilanes producible according to said method and to their use.
摘要翻译：本发明涉及一种由卤代硅烷生产氢硅烷的方法，其通过以下步骤：a）使i）至少一种通式为SinX2n + 2（n≥3，X = F，Cl，Br和/或I）的卤代硅烷与ii） a = 0或1，b = 0或1，c = 0或1和式（I）的通式NRR'aR“bYc的至少一种催化剂，其中aa）R，R'和/或R” 是-C 1 -C 12烷基，-C 1 -C 12芳基，-C 1 -C 12芳烷基，-C 1 -C 12氨基烷基，-C 1 -C 12氨基芳基，-C 1 -C 12氨基烷基和/或两个或三个基团R，R'和R “（如果c = 0）一起形成包括N的环状或双环，杂脂族或杂芳族体系，条件是至少一个基团R，R'或R”不等于-CH 3和/或其中bb）R和R' 和/或R“'（如果c = 1）是-C 1 -C 12亚烷基，-C 1 -C 12亚芳基，-C 1 -C 12亚芳基，-C 1 -C 12杂亚烷基，-C 1 -C 12亚杂芳基，-C 1 -C 12杂亚烷基和/ 或-N =或cc）（如果a = b = c = 0）R≡≡CR'“（其中R'”= C 1 -C 10烷基，-C 1 -C 10芳基和/或-C 1 -C 10芳烷基），同时形成包含通式SimX2m + 2（具有m> n和X = F，Cl，Br和/或I）的至少一种卤代硅烷和SiX 4（具有X = F，Cl，Br和 /或I），和b）在形成通式SimH 2 m + 2的氢硅烷的同时使通式SimH 2 m + 2的至少一种卤代硅烷氢化。本发明还涉及根据所述方法可生产的氢硅石及其用途。

7. 发明申请

US20120214005A1 METHOD FOR PRODUCING HYDRIDOSILANES 有权
标题翻译：生产水合物的方法
公开(公告)号：US20120214005A1
公开(公告)日：2012-08-23
申请号：US13504331
申请日：2010-11-08
申请人： Stephan Wieber , Matthias Patz , Martin Trocha , Hartwig Rauleder , Ekkehard Mueh , Harald Stueger , Christoph Walkner
发明人： Stephan Wieber , Matthias Patz , Martin Trocha , Hartwig Rauleder , Ekkehard Mueh , Harald Stueger , Christoph Walkner
IPC分类号： B32B9/04 , C01B33/04
CPC分类号： C01B33/04 , C01B33/043 , C01B33/10773 , Y10T428/31663
摘要： The invention relates to a method for producing hydridosilanes from halosilanes by a) reacting i) at least one halosilane of the generic formula SinX2n+2 (with n≧3 and X═F, Cl, Br and/or I) with ii) at least one catalyst of the generic formula NRR'aR″bYc with a=0 or 1, b=0 or 1, and c=0 or 1, and formula (I), wherein aa) R, R′ and/or R″ are —C1-C12 alkyl, —C1-C12 aryl, —C1-C12 aralkyl, —C1-C12 aminoalkyl, —C1-C12 aminoaryl, —C1-C12 aminoaralkyl, and/or two or three groups R, R′ and R″ (if c=0) together form a cyclic or bicyclic, heteroaliphatic or heteroaromatic system including N, with the proviso that at least one group R, R′ or R″ is unequal —CH3 and/or wherein bb) R and R′ and/or R″' (if c=1) are —C1-C12 alkylene, —C1-C12 arylene, —C1-C12 aralkylene, —C1-C12 heteroalkylene, —C1-C12 heteroarylene, —C1-C12 heteroaralkylene and/or —N═, or cc) (if a=b=c=0) R═≡C-R′″ (with R′″═—C1-C10 alkyl, —C1-C10 aryl and/or —C1-C10 aralkyl), while forming a mixture comprising at least one halosilane of the generic formula SimX2m+2 (with m>n and X═F, Cl, Br and/or I) and SiX4 (with X═F, Cl, Br and/or I), and b) hydrogenating the at least one halosilane of the generic formula SimH2m+2 while forming a hydridosilane of the generic formula SimH2m+2. The invention also relates to the hydridosilanes producible according to said method and to their use
摘要翻译：本发明涉及一种由卤代硅烷生产氢硅烷的方法，其通过以下步骤：a）使i）至少一种通式为SinX2n + 2（n≥3，X = F，Cl，Br和/或I）的卤代硅烷与ii） a = 0或1，b = 0或1，c = 0或1和式（I）的通式NRR'aR“bYc的至少一种催化剂，其中aa）R，R'和/或R” 是-C 1 -C 12烷基，-C 1 -C 12芳基，-C 1 -C 12芳烷基，-C 1 -C 12氨基烷基，-C 1 -C 12氨基芳基，-C 1 -C 12氨基烷基和/或两个或三个基团R，R'和R “（如果c = 0）一起形成包括N的环状或双环，杂脂族或杂芳族体系，条件是至少一个基团R，R'或R”不等于-CH 3和/或其中bb）R和R' 和/或R“'（如果c = 1）是-C 1 -C 12亚烷基，-C 1 -C 12亚芳基，-C 1 -C 12亚芳基，-C 1 -C 12杂亚烷基，-C 1 -C 12亚杂芳基，-C 1 -C 12杂亚烷基和/ 或-N =或cc）（如果a = b = c = 0）R≡≡CR'“（其中R'”= C 1 -C 10烷基，-C 1 -C 10芳基和/或-C 1 -C 10芳烷基），同时形成包含通式SimX2m + 2（具有m> n和X = F，Cl，Br和/或I）的至少一种卤代硅烷和SiX 4（具有X = F，Cl，Br和 /或I），和b）在形成通式SimH 2 m + 2的氢硅烷的同时使通式SimH 2 m + 2的至少一种卤代硅烷氢化。本发明还涉及根据所述方法可生产的氢硅石及其用途

8. 发明授权

US06960699B2 Method for the hydroformylation of olefins 有权
公开(公告)号：US06960699B2
公开(公告)日：2005-11-01
申请号：US10506603
申请日：2003-03-08
申请人： Walter Tötsch , Detlef Arnoldi , Alfred Kaizik , Martin Trocha
发明人： Walter Tötsch , Detlef Arnoldi , Alfred Kaizik , Martin Trocha
IPC分类号： C07B61/00 , C07C29/141 , C07C29/16 , C07C31/125 , C07C45/50 , C07C45/75 , C07C45/80 , C07C45/82 , C07C29/14
CPC分类号： C07C29/141 , C07C29/16 , C07C45/50 , C07C31/125 , C07C47/02
摘要： The invention relates to a process for preparing alcohols by hydroformylation of olefins or olefin mixtures, separation from the catalyst and subsequent hydrogenation, with an extraction being carried out after removal of the catalyst and before the hydrogenation of the aldehydes.

9. 发明授权

US06492564B1 Process for the catalytically carrying out multiphase reactions, in particular hydroformylations 有权
标题翻译：催化进行多相反应的方法，特别是加氢甲酰化反应
公开(公告)号：US06492564B1
公开(公告)日：2002-12-10
申请号：US09585425
申请日：2000-06-02
申请人： Klaus-Diether Wiese , Guido Protzmann , Juergen Koch , Dirk Roettger , Martin Trocha
发明人： Klaus-Diether Wiese , Guido Protzmann , Juergen Koch , Dirk Roettger , Martin Trocha
IPC分类号： C07C4500
CPC分类号： C07C45/50 , B01J8/06 , B01J19/2415 , B01J19/2435 , B01J19/26 , B01J2208/00274 , B01J2208/00283 , B01J2219/00033 , B01J2219/00103 , B01J2219/0011 , B01J2219/185 , C07C47/02
摘要： The invention relates to a catalytic process for carrying out multiphase reactions in a tubular reactor, with the catalyst being present in the continuous phase and at least one starting material in a disperse phase and the loading factor B of the tubular reactor being equal to or greater than 0.8. The process is especially suitable in particular for the hydroformylation of olefins. The aldehydes thus prepared can ideally be used for the preparation of alcohols, carboxylic acids or in aldol condensations.
摘要翻译：本发明涉及用于在管式反应器中进行多相反应的催化方法，其中催化剂存在于连续相中，并且至少一种起始原料在分散相中，并且管式反应器的负载因子B等于或大于大于0.8。该方法特别适用于烯烃的加氢甲酰化。如此制备的醛可以理想地用于制备醇，羧酸或醛醇缩合物。

10. 发明授权

US09561965B2 Method for hydrogenating higher halogen-containing silane compounds 有权
标题翻译：氢化较高含卤素硅烷化合物的方法
公开(公告)号：US09561965B2
公开(公告)日：2017-02-07
申请号：US14649092
申请日：2013-11-27
申请人： Min-Zae Oh , Jens Haubrock , Thorsten Schwaertzke , Imad Moussallem , Martin Trocha
发明人： Min-Zae Oh , Jens Haubrock , Thorsten Schwaertzke , Imad Moussallem , Martin Trocha
IPC分类号： B01J29/90 , C01B33/04 , C01B3/00 , C01B33/107
CPC分类号： C01B33/04 , C01B3/0015 , C01B6/006 , C01B33/107 , Y02E60/328
摘要： The present invention relates to a continuous process for hydrogenating halogen-containing silane compounds having at least three silicon atoms, in which at least one halogen-containing silane compound having at least three silicon atoms and at least one hydrogenating agent are converted continuously to form at least one hydridosilane compound having at least 3 silicon atoms and oxidized hydrogenating agent, and wherein oxidized hydrogenating agent is withdrawn and reduced, and the reaction product of this reduction reaction is sent back to the hydrogenation, to the hydridosilane compounds obtainable by this process and to the use thereof.
摘要翻译：本发明涉及一种用于氢化含有至少三个硅原子的含卤素的硅烷化合物的连续方法，其中至少一种具有至少三个硅原子的含卤素的硅烷化合物和至少一种氢化剂被连续地转化成至少一个具有至少3个硅原子的氢硅烷化合物和氧化的氢化剂，并且其中将氧化的氢化剂排出并还原，并将该还原反应的反应产物送回氢化，得到可通过该方法获得的氢硅烷化合物，其使用。

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