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1. 发明授权

US5328616A Methods and apparatus for treating electroless plating baths 失效
标题翻译：化学镀浴的处理方法和设备
公开(公告)号：US5328616A
公开(公告)日：1994-07-12
申请号：US29942
申请日：1993-03-09
申请人： Nicholas M. Martyak , Bruce F. Monzyk , Henry H. Chien
发明人： Nicholas M. Martyak , Bruce F. Monzyk , Henry H. Chien
IPC分类号： B01D61/02 , B01D61/04 , B01J45/00 , C02F1/26 , C02F1/44 , C02F9/00 , C23C18/16 , B01D6/04
CPC分类号： B01D61/025 , B01D61/04 , B01J45/00 , C02F1/26 , C02F1/441 , C02F9/00 , C23C18/1617 , B01D2311/04 , C02F2101/20
摘要： Apparatus and methods for removing formate ions from electroless metal plating baths employing formaldehyde as a reducing agent and typically comprising polyvalent anions as metal chelant and/or counterion. The apparatus and methods employ anion filtration to separate polyvalent anions from monovalent formate ions and ion exchange units to remove metal and metal chelant species from formate-containing streams. Preferred aspects of this invention provide apparatus and methods for removing formate from electroless copper plating baths.
摘要翻译：从使用甲醛作为还原剂并通常包含多价阴离子作为金属螯合剂和/或抗衡离子的化学镀金属浴中除去甲酸根离子的装置和方法。该装置和方法采用阴离子过滤从单价甲酸根离子和离子交换单元中分离多价阴离子以从含甲酸的物流中除去金属和金属螯合物。本发明的优选方面提供了用于从无电镀铜浴中除去甲酸盐的设备和方法。

2. 发明授权

US5306336A Sulfate-free electroless copper plating baths 失效
标题翻译：无硫酸化无电镀铜浴
公开(公告)号：US5306336A
公开(公告)日：1994-04-26
申请号：US979097
申请日：1992-11-20
申请人： Nicholas M. Martyak , Bruce F. Monzyk , Henry H. Chien
发明人： Nicholas M. Martyak , Bruce F. Monzyk , Henry H. Chien
IPC分类号： C23C18/40 , C23C18/38
CPC分类号： C23C18/405
摘要： Sulfate-free electroless copper baths comprising cupric ions, formaldehyde, formate ions, hydroxyl ions, a copper counterion, e g. preferably a monovalent anion such as acetate, nitrate or formate, and copper chelant such as an alkali metal salt of aminotris(methylenephosphonic acid), biscarboxymethylaspartic acid, ethylenediaminetetra(methylenephosphonic acid), diethylenetriaminepenta(methylenephosphonic acid), gluconic acid, 1-hydroxyethylidene-1,1-diphosphonic acid, mucic acid, D-saccharac acid, tartaric acid and N,N,N',N'-tetrakis(2-hydroxypropyl)ethylenediamine are amenable to the recovery of copper, e.g. from purge streams, using the methods and apparatus including solvent extraction, e.g. employing hydroxamic acid extractants, anion filtration, ion-exchange and chelant precipitation.
摘要翻译：含有铜离子，甲醛，甲酸根离子，羟基离子，铜抗衡离子的无硫酸盐化学镀铜浴。优选一价阴离子如乙酸盐，硝酸盐或甲酸盐，以及铜螯合剂如氨基三（亚甲基膦酸）的碱金属盐，双羧甲基天冬氨酸，乙二胺四（亚甲基膦酸），二亚乙基三胺五（亚甲基膦酸），葡糖酸，1-羟基亚乙基 - 1,1-二膦酸，粘酸，D-糖酸，酒石酸和N，N，N'，N'-四（2-羟丙基）乙二胺可以回收铜，例如使用包括溶剂萃取的方法和设备，例如洗涤流。使用异羟肟酸萃取剂，阴离子过滤，离子交换和螯合沉淀。

3. 发明授权

US5277817A Apparatus and methods for treating electroless plating baths 失效
标题翻译：化学镀浴处理设备及方法
公开(公告)号：US5277817A
公开(公告)日：1994-01-11
申请号：US979514
申请日：1992-11-20
申请人： Nicholas M. Martyak , Bruce F. Monzyk , Henry H. Chien
发明人： Nicholas M. Martyak , Bruce F. Monzyk , Henry H. Chien
IPC分类号： B01D11/02 , B01D61/02 , C23C18/16 , B01D11/00 , B01D61/00
CPC分类号： B01D61/025 , B01D11/0288 , C23C18/1617 , Y10S210/912
摘要： Apparatus and methods for removing polyvalent by-product anions, e.g. borate and orthophosphate ions, from electroless metal plating baths employing borane or hypophosphite reducing agents and typically comprising monovalent anions or neutral zwitterions as metal chelant and/or counterion. The apparatus and methods of this invention employ (a) solvent extraction to remove metal species for recycle, (b) anion filtration to separate polyvalent anions from neutral zwitterions and monovalent anions and (c) ion exchange units to remove metal and metal chelant species from polyvalent anion-containing waste streams.
摘要翻译：用于除去多价副产物阴离子的装置和方法硼酸盐和正磷酸盐离子，使用硼烷或次亚磷酸盐还原剂，通常包含一价阴离子或中性两性离子作为金属螯合剂和/或抗衡离子。本发明的装置和方法使用（a）溶剂萃取以除去用于再循环的金属物质，（b）阴离子过滤以从中性两性离子和单价阴离子分离多价阴离子和（c）离子交换单元以从金属和金属螯合物物质中除去金属和金属螯合物含多价阴离子的废物流。

4. 发明授权

US5258061A Electroless nickel plating baths 失效
标题翻译：化学镀镍浴
公开(公告)号：US5258061A
公开(公告)日：1993-11-02
申请号：US979100
申请日：1992-11-20
申请人： Nicholas M. Martyak , Bruce F. Monzyk , Henry H. Chien
发明人： Nicholas M. Martyak , Bruce F. Monzyk , Henry H. Chien
IPC分类号： C23C18/34 , C23C18/36
CPC分类号： C23C18/34
摘要： Aqueous electroless nickel plating solutions comprising a water soluble nickel salt associated with a neutral zwitterion, e.g. alanine or glycine, and/or monovalent anion, e.g. lactate, nitrate, hypophosphite, acetate, sulfamate, hydrochloride, formate, propionate, trichloroacetate, trifluoroacetate, methanesulfonate, glycolate, aspartate or pyruvate, as counterion and chelant, a neutral, e.g. borate, or monovalent, e.g. hypophosphite, reducing agent, and a non-thiourea stabilizer, e.g. protonated dimethylamine or dimethylaminopropylamine or 2-hydroxyethanesulfonic acid. Valuable components of spent baths, e.g. nickel and neutral or monovalent anion species, can be advantageously recycled by employing solvent extraction and anion filtration operations.
摘要翻译：包含与中性两性离子相关的水溶性镍盐的水性无电镀镍溶液，例如丙氨酸或甘氨酸，和/或一价阴离子，例如乳酸盐，硝酸盐，次磷酸盐，乙酸盐，氨基磺酸盐，盐酸盐，甲酸盐，丙酸盐，三氯乙酸盐，三氟乙酸盐，甲磺酸盐，乙醇酸盐，天冬氨酸盐或丙酮酸盐，作为抗衡离子和螯合剂。硼酸盐，或单价的。次磷酸盐，还原剂和非硫脲稳定剂，例如，质子化二甲胺或二甲基氨基丙胺或2-羟基乙磺酸。废浴的有价值的成分，例如镍和中性或单价阴离子物质可以有利地通过使用溶剂萃取和阴离子过滤操作来回收。

5. 发明授权

US5306334A Electroless nickel plating solution 失效
标题翻译：化学镀镍溶液
公开(公告)号：US5306334A
公开(公告)日：1994-04-26
申请号：US916572
申请日：1992-07-20
申请人： Nicholas M. Martyak , Bruce F. Monzyk
发明人： Nicholas M. Martyak , Bruce F. Monzyk
IPC分类号： C23C18/36 , D06M11/83
CPC分类号： D06M11/83 , C23C18/36
摘要： Phosphorus-containing, crystalline, nickel-coated fabric, wherein said nickel contains 1 to 6 weight percent phosphorus, has crystallites greater than 3 nanometers and has a surface resistivity of less than 1 ohm/square is deposited onto a substrate a surface which is catalytic to electroless deposition of nickel by immersing the substrate into an electroless nickel plating solution consisting essentially of nickel salt, one or more organic acids, hypophosphite reducing agent, thiourea and ammonia and essentially no heavy metal, wherein the concentration of said thiourea is less than 1 ppm, maintained at a pH of 6.5 to 8.5 and a temperature less than 60.degree. C. Preferred plating solutions comprise essentially no lead or cadmium and have a molar ratio of nickel to hypophosphite in said solution is 0.4 to 0.55. Preferred organic acids are selected from the group consisting of lactic acid, acetic acid, propionic acid, pyruvic acid, aspartic acid and glycolic acid.
摘要翻译：含磷的结晶镍涂层织物，其中所述镍含有1至6重量百分比的磷，具有大于3纳米的微晶并且具有小于1欧姆/平方的表面电阻率沉积在基底上，所述表面是催化剂通过将基底浸入基本上由镍盐，一种或多种有机酸，次亚磷酸盐还原剂，硫脲和氨基本上不含重金属组成的化学镀镍溶液中来进行镍的无电沉积，其中所述硫脲的浓度小于1 ppm，维持在pH 6.5至8.5，温度低于60℃。优选的电镀溶液基本上不含铅或镉，并且所述溶液中镍与次磷酸盐的摩尔比为0.4至0.55。优选的有机酸选自乳酸，乙酸，丙酸，丙酮酸，天冬氨酸和乙醇酸。

6. 发明申请

US20140023555A1 FORMULATIONS AND METHODS TO REDUCE HEXAVALENT CHROME CONTAMINATION 有权
标题翻译：减少六价铬污染的制剂和方法
公开(公告)号：US20140023555A1
公开(公告)日：2014-01-23
申请号：US14008071
申请日：2012-03-30
申请人： Bruce F. Monzyk , Paul J. Usinowicz , Derik R. Heiss , Vinay V. Gadkari , John T. Stropki
发明人： Bruce F. Monzyk , Paul J. Usinowicz , Derik R. Heiss , Vinay V. Gadkari , John T. Stropki
IPC分类号： A62D3/37
CPC分类号： A62D3/37 , A62D2101/24 , A62D2101/43 , C23C22/83
摘要： The present invention includes formulations and methods to reduce Cr(VI) contamination, in which the formulation comprises (1) a reactive reducing agent comprising at least one reducing chemical capable of reducing Cr(VI) to Cr(III); and (b) one or more solvents. Moreover, the present invention includes formulations to reduce Cr(VI) within the coating, and Cr(VI) reducing kits with at least one color reference tool for evaluating the process and/or completion of the Cr(VI) reduction.
摘要翻译：本发明包括减少Cr（VI）污染的制剂和方法，其中制剂包含（1）包含至少一种能还原Cr（VI）至Cr（III）的还原性化合物的反应性还原剂; 和（b）一种或多种溶剂。此外，本发明包括用于减少涂层内的Cr（VI）的制剂和具有至少一种颜色参考工具的Cr（VI）还原试剂盒，用于评估Cr（VI）还原过程和/或完成。

7. 发明授权

US08034253B2 Decontaminant 失效
标题翻译：去污剂
公开(公告)号：US08034253B2
公开(公告)日：2011-10-11
申请号：US11718851
申请日：2005-11-14
申请人： Bruce F. Monzyk , Russell R. Greene , Chad M. Cucksey , John A. McArthur , F. Michael Von Fahnestock , Steven C. Lorence , Michael J. Murphy , Brian J. Blackstone , Thomas A. Malloy, IV
发明人： Bruce F. Monzyk , Russell R. Greene , Chad M. Cucksey , John A. McArthur , F. Michael Von Fahnestock , Steven C. Lorence , Michael J. Murphy , Brian J. Blackstone , Thomas A. Malloy, IV
IPC分类号： C09K3/00 , A62D3/00 , A62D9/00 , A62D3/30 , A62D3/38 , C01B7/00 , C01B11/00 , C01B13/00 , C01B15/00 , C11D3/39 , C02F1/00 , C01C1/00 , C01G49/00 , C01G49/02
CPC分类号： A62D3/38 , A62D2101/02 , A62D2101/04 , A62D2101/24 , A62D2101/26 , A62D2101/28 , A62D2101/43 , Y02W10/37
摘要： Method and composition for decomposing and detoxifying chemical warfare agents, organic toxic compounds (e.g., pesticides), and for removal of contaminants in materials including fuels. The method and composition are based on ferrate (VI). The ferrate is typically applied to a contaminated surface or volume with a phase transfer catalyst and/or with a carrier.
摘要翻译：用于分解和解毒化学战剂，有机有毒化合物（如农药）以及用于除去包括燃料在内的材料中的污染物的方法和组合物。该方法和组合物基于高铁酸盐（VI）。高铁酸盐通常用相转移催化剂和/或载体施加到污染的表面或体积上。

8. 发明授权

US07909788B2 Carbon dioxide removal from whole blood by photolytic activation 有权
标题翻译：通过光解活化从全血中去除二氧化碳
公开(公告)号：US07909788B2
公开(公告)日：2011-03-22
申请号：US12173044
申请日：2008-07-15
申请人： Bruce F. Monzyk , Eric C. Burckle
发明人： Bruce F. Monzyk , Eric C. Burckle
IPC分类号： A61M37/00
CPC分类号： A61M1/32 , A61M1/327 , A61M1/3681 , A61M1/3683
摘要： Apparatus and methods for removing carbon dioxide from whole blood. Hydrogen ions are generated from water in the blood, resulting in the formation and release of carbon dioxide from the blood.
摘要翻译：从全血中除去二氧化碳的装置和方法。从血液中的水产生氢离子，导致二氧化碳从血液中的形成和释放。

9. 发明授权

US07883610B2 Photolytic oxygenator with carbon dioxide and/or hydrogen separation and fixation 有权
标题翻译：光解氧合器与二氧化碳和/或氢气分离固定
公开(公告)号：US07883610B2
公开(公告)日：2011-02-08
申请号：US10525689
申请日：2003-08-21
申请人： Bruce F. Monzyk , Eric C. Burckle
发明人： Bruce F. Monzyk , Eric C. Burckle
IPC分类号： B01J19/08 , B01J19/12 , C25B1/04
CPC分类号： C25B9/00 , B01D53/62 , B01D53/965 , C01B3/042 , C01B13/0207 , C01B15/01 , C25B1/003 , Y02C10/04 , Y02E60/364 , Y02E60/368 , Y02P20/152
摘要： Apparatus for oxygenating an enclosed space as well as removing carbon dioxide from the enclosed space. The apparatus comprises a photolytic cell (16) having an anode compartment with a photo-active surface having the ability to convert water to oxygen; a cathode compartment having the ability to convert carbon dioxide and hydrogen to a solid or liquid medium; and a light source (20) for providing light photons (21) to said photolytic cell and activating the photo-reactive surface.
摘要翻译：用于对封闭空间进行氧化以及从封闭空间除去二氧化碳的装置。该装置包括具有阳离子室的光解室（16），所述阳极室具有能够将水转化为氧的光活性表面; 具有将二氧化碳和氢气转化成固体或液体介质的能力的阴极室; 以及用于向所述光解细胞提供光子（21）并激活光反应表面的光源（20）。

10. 发明授权

US06838069B2 Apparatus and method for ammonia removal from waste streams 失效
标题翻译：从废物流中去除氨的装置和方法
公开(公告)号：US06838069B2
公开(公告)日：2005-01-04
申请号：US10346896
申请日：2003-01-17
申请人： Scott J. Blonigen , Alex G. Fassbender , Robert D. Litt , Bruce F. Monzyk , Richelle Neff
发明人： Scott J. Blonigen , Alex G. Fassbender , Robert D. Litt , Bruce F. Monzyk , Richelle Neff
IPC分类号： B01D53/58 , B01D53/04 , B01J20/34 , B01J45/00 , B01J49/00 , C02F1/28 , C02F1/42
CPC分类号： B01D53/0423 , B01D53/04 , B01D53/10 , B01D2253/10 , B01D2253/104 , B01D2253/1085 , B01D2253/202 , B01D2253/206 , B01D2257/406 , B01D2259/40088 , B01D2259/40092 , B01J20/06 , B01J20/3433 , B01J20/3475 , B01J45/00 , B01J49/53 , Y10S210/903
摘要： Apparatus, materials, and methods for removing ammonia from fluid using metal hydroxides (e.g. zinc hydroxide) and metal cation loaded media (e.g. zinc loaded ion exchange resins); the metal hydroxides and metal cation loaded media may be regenerated with a weak acid (pKa between 3 and 7). Alternatively, ammonia is removed from fluids by using H2SO4 and ZnSO4 and metal cation loaded media; the metal cation loaded media may be regenerated with H2SO4 and ZnSO4; the ammonia containing H2SO4 and H2SO4 may be concentrated as necessary to form (NH4)2SO4.ZnSO4.6H2O (ammonium zinc sulfate hexahydrate) crystals. These crystals are removed from the mother liquor and heated to temperatures exceeding 200° C. releasing NH3 and H2O vapor upon the decomposition of the crystals.
摘要翻译：使用金属氢氧化物（例如氢氧化锌）和金属负载介质（例如负载锌的离子交换树脂）从流体中除去氨的设备，材料和方法; 金属氢氧化物和金属负载介质可以用弱酸（pKa在3和7之间）再生。或者，通过使用H 2 SO 4和ZnSO 4和金属负载介质从流体中除去氨; 金属负载介质可以用H 2 SO 4和ZnSO 4再生; 可以根据需要浓缩含有H 2 SO 4和ZnSO 4的氨以形成（NH 4）2 SO 4·ZnSO 4·6H 2 O（六水合硫酸锌）晶体。将这些晶体从母液中除去并加热到超过200℃的温度，在晶体分解时释放出NH 3和H 2 O的蒸气。

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