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1. 发明授权

US07094811B2 Energy absorbing flexible foams produced in part with a double metal cyanide catalyzed polyol 有权
标题翻译：能量吸收的柔性泡沫部分由双金属氰化物催化的多元醇制成
公开(公告)号：US07094811B2
公开(公告)日：2006-08-22
申请号：US10263536
申请日：2002-10-03
申请人： Neil H. Nodelman , David A. Radovich , Albert Magnotta , Carl E. Holsinger
发明人： Neil H. Nodelman , David A. Radovich , Albert Magnotta , Carl E. Holsinger
IPC分类号： C09J9/00 , C08G18/28
CPC分类号： C08G18/4866 , C08G18/6685 , C08G65/2663 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08G2350/00
摘要： Energy absorbing flexible foams can be produced by reacting an isocyanate with a first polyol, prepared at least in part by an active double metal cyanide catalyst and a second polyether polyol is prepared at least in part by a basic or acidic catalyst.
摘要翻译：吸收能量的柔性泡沫可以通过使异氰酸酯与至少部分由活性双金属氰化物催化剂制备的第一多元醇反应制备，第二聚醚多元醇至少部分由碱性或酸性催化剂制备。

2. 发明申请

US20080125508A1 Reduction of MDI emissions in cavity filling NVH polyurethane foams 有权
标题翻译：减少腔体填充NVH聚氨酯泡沫中的MDI排放
公开(公告)号：US20080125508A1
公开(公告)日：2008-05-29
申请号：US11604953
申请日：2006-11-28
申请人： Jack W. Jenny , David A. Radovich
发明人： Jack W. Jenny , David A. Radovich
IPC分类号： C08G18/02
CPC分类号： C08G18/632 , C08G18/4072 , C08G18/5024 , C08G18/7664 , C08G2101/005 , C08G2101/0083 , C08G2350/00
摘要： This invention relates to reactive systems for the production of cavity filling polyurethane foams for NVH (noise vibration and harshness) application areas in which the system exhibits reduced isocyanate emissions. These foams comprises a polyisocyanate comprising a polymethylene poly(phenylisocyanate).
摘要翻译：本发明涉及用于生产用于NVH（噪声振动和粗糙度）应用领域的空腔填充聚氨酯泡沫的反应系统，其中系统显示减少的异氰酸酯排放。这些泡沫包括多异氰酸酯，其包含聚亚甲基聚（异氰酸苯酯）。

3. 发明授权

US4128512A Post treatment of flexible polyurethane foam with organic siloxanes for increasing the water absorbency and penetration 失效
标题翻译：用有机硅氧烷处理柔性聚氨酯泡沫，以提高吸水性和渗透性
公开(公告)号：US4128512A
公开(公告)日：1978-12-05
申请号：US845690
申请日：1977-10-26
申请人： Keith G. Spitler , David A. Radovich
发明人： Keith G. Spitler , David A. Radovich
IPC分类号： C08J9/42 , C08J9/00 , C08G18/44
CPC分类号： C08J9/42 , C08J2375/04 , C08J2483/00 , Y10S521/905
摘要： The instant invention is directed to the post treatment of flexible polyurethane foams. It has been found that the water absorbency and penetration of flexible polyurethane foams can be enhanced by washing and/or impregnating the foam with an aqueous solution of specified organic siloxane surfactants and allowing the treated foam to dry.
摘要翻译：本发明涉及柔性聚氨酯泡沫的后处理。已经发现，通过用指定的有机硅氧烷表面活性剂的水溶液洗涤和/或浸渍泡沫体并且使经处理的泡沫体干燥，可以提高柔性聚氨酯泡沫的吸水性和渗透性。

4. 发明授权

US07223890B2 Isocyanate reactive mixture and process for preparing same 有权
标题翻译：异氰酸酯反应混合物及其制备方法
公开(公告)号：US07223890B2
公开(公告)日：2007-05-29
申请号：US10683241
申请日：2003-10-10
申请人： David A. Radovich , Richard G. Skorpenske , Gary W. Munko
发明人： David A. Radovich , Richard G. Skorpenske , Gary W. Munko
IPC分类号： C00C43/00
CPC分类号： C08G18/4009 , C08G18/283 , C08G18/2865 , C08G18/4866 , C08G18/61
摘要： The present invention relates to an improved isocyanate reactive mixture containing at least one DMC-catalyzed polyol and about 0.25 to about 15 wt. %, based on the total weight of the isocyanate-reactive mixture, of at least one ethylene oxide (EO) containing water compatibilizer. The isocyanate reactive mixtures of the present invention may find use in the preparation of polyurethane foams, coatings, elastomers, sealants, adhesives and the like.
摘要翻译：本发明涉及含有至少一种DMC催化的多元醇和约0.25至约15wt。％的改进的异氰酸酯反应混合物。基于异氰酸酯反应性混合物的总重量，含有至少一种含有水相增容剂的环氧乙烷（EO）。本发明的异氰酸酯反应性混合物可用于制备聚氨酯泡沫，涂料，弹性体，密封剂，粘合剂等。

5. 发明授权

US5801210A Method and apparatus for the production of essentially void free foams 失效
公开(公告)号：US5801210A
公开(公告)日：1998-09-01
申请号：US960493
申请日：1997-10-29
申请人： David A. Radovich , David D. Steppan , Keith G. Spitler , James D. Shoup
发明人： David A. Radovich , David D. Steppan , Keith G. Spitler , James D. Shoup
IPC分类号： B29C44/34 , C08G18/08 , C08J9/12 , C08J9/00 , C08J9/14 , C08G18/14
CPC分类号： C08J9/122 , B29C44/3446 , B29C44/348 , C08G18/0895 , C08G2101/0008 , C08G2101/005 , C08J2375/04
摘要： A process for the manufacture of polyurethane foam comprising the steps of (i) mixing at a reaction index of 40 to 400: (a) a polyisocyanate blend comprising at least one polyisocyanate and optionally, additives and fillers; (b) a polyol blend comprising isocyanate reactive components and optionally, water, additional blowing agents, catalysts, surfactants, fillers and other additives; wherein either or both said polyisocyanate blend or said polyol blend contain between 0.3 to about 20 wt. % CO.sub.2 based on the total weight of said polyisocyanate blend and said polyol blend; (ii) introducing and uniformly mixing in liquid form of CO.sub.2 as a blowing agent into either or both said polyisocyanate blend or said polyol blend and maintaining said CO.sub.2 in said liquid form. The present invention also relates to an apparatus, which performs the above-mentioned process.

6. 发明授权

US4452924A Flexible polyurethane foams having improved load bearing characteristics 失效
标题翻译：柔性聚氨酯泡沫具有改善的承载特性
公开(公告)号：US4452924A
公开(公告)日：1984-06-05
申请号：US491681
申请日：1983-05-05
申请人： David A. Radovich
发明人： David A. Radovich
IPC分类号： C08G18/10 , C08G18/50 , C08G18/14 , C08G18/32
CPC分类号： C08G18/5045 , C08G18/10 , C08G2101/0008 , C08G2101/005
摘要： The present invention is directed to the discovery that the substitution of isocyanate coupled polyols for polyols conventionally used in the art leads to flexible polyurethane foams having significantly enhanced load bearing properties. More particularly, the present invention is directed to a process for the production of a flexible polyurethane foam having improved load bearing characteristics and to the foams so produced. The present process broadly comprises reacting an organic polyisocyanate with a coupled polyol in the presence of a blowing agent, a catalyst and a foam stabilizer. The coupled polyol consists essentially of the reaction product of an organic polyisocyanate and an organic compound having a hydroxy functionality ("functionality" as used herein is intended to mean the average number of reaction groups per molecule) of greater than 2, wherein the ratio of hydroxyl groups to isocyanate groups is greater than 1.0.
摘要翻译：本发明涉及这样的发现，即本领域常规使用的多元醇的异氰酸酯偶联多元醇的取代导致具有显着增强的承载性质的柔性聚氨酯泡沫。更具体地说，本发明涉及生产具有改进的承载特性的柔性聚氨酯泡沫塑料的方法和如此生产的泡沫体的方法。本发明方法广泛地包括在发泡剂，催化剂和泡沫稳定剂的存在下使有机多异氰酸酯与偶联的多元醇反应。偶联多元醇基本上由有机多异氰酸酯和具有羟基官能团的有机化合物的反应产物组成（“本文所用的官能度”意指每个分子的平均反应基团数）大于2，其中，羟基与异氰酸酯基的比例大于1.0。

7. 发明授权

US07678840B2 Reduction of MDI emissions in cavity filling NVH polyurethane foams 有权
标题翻译：减少腔体填充NVH聚氨酯泡沫中的MDI排放
公开(公告)号：US07678840B2
公开(公告)日：2010-03-16
申请号：US11604953
申请日：2006-11-28
申请人： Jack W. Jenny , David A. Radovich
发明人： Jack W. Jenny , David A. Radovich
IPC分类号： C08G18/06
CPC分类号： C08G18/632 , C08G18/4072 , C08G18/5024 , C08G18/7664 , C08G2101/005 , C08G2101/0083 , C08G2350/00
摘要： This invention relates to reactive systems for the production of cavity filling polyurethane foams for NVH (noise vibration and harshness) application areas in which the system exhibits reduced isocyanate emissions. These foams comprises a polyisocyanate comprising a polymethylene poly(phenylisocyanate).
摘要翻译：本发明涉及用于生产用于NVH（噪声振动和粗糙度）应用领域的空腔填充聚氨酯泡沫的反应系统，其中系统显示减少的异氰酸酯排放。这些泡沫包括多异氰酸酯，其包含聚亚甲基聚（异氰酸苯酯）。

8. 发明授权

US4569952A Flexible polyurethane foams having improved load bearing characteristics and mixtures useful therein 失效
标题翻译：具有改进的承载特性的柔性聚氨酯泡沫和其中有用的混合物
公开(公告)号：US4569952A
公开(公告)日：1986-02-11
申请号：US696942
申请日：1985-01-31
申请人： David A. Radovich , Alicia H. Keddie
发明人： David A. Radovich , Alicia H. Keddie
IPC分类号： C08G18/50 , C08G18/65 , C08G65/26 , C08G18/14 , C08G18/32
CPC分类号： C08G18/6535 , C08G18/5033 , C08G65/2627 , C08G2101/0008 , C08G2101/0058 , C08G2101/0083
摘要： The present invention is directed to a process for the production of a flexible polyurethane foam comprising reacting an organic polyisocyanate and a polyol, in the presence of a blowing agent, a catalyst, and a foam stabilizer, the improvement wherein a foam of increased load bearing is obtained by including in the reaction mixture from about 8 to about 25 parts by weight per 100 parts by weight of said polyol of a mixture comprising(a) from 30 to 100 percent by weight of an addition product of an alkylene oxide and an aromatic diamine, said addition product having an average hydroxyl functionality of at least 2.5 and as high as 6, and having an hydroxyl number of from about 150 to about 810 and containing no free amine hydrogen, and(b) from 0 to 70 percent by weight of an alkanolamine having at least one hydroxyl group and having at least two active hydrogens, wherein the hydroxyl number of the combination of the polyol, the mixture, and any other isocyanate-reactive components, excluding water, is from 25 to 300, said process further being characterized as being conducted in the absence of a tin catalyst.
摘要翻译：本发明涉及一种生产柔性聚氨酯泡沫的方法，包括在发泡剂，催化剂和泡沫稳定剂的存在下使有机多异氰酸酯和多元醇反应，改进之处在于增加负载承载力的泡沫通过在反应混合物中包含约8至约25重量份的每100重量份所述多元醇的混合物，所述混合物包含（a）30至100重量％的环氧烷和芳族化合物的加成产物二胺，所述加成产物的平均羟基官能度至少为2.5，高达6，羟值为约150至约810，不含游离胺氢，和（b）0至70重量％的具有至少一个羟基并具有至少两个活性氢的链烷醇胺，其中多元醇，混合物和任何其它异氰酸酯反应性组分的组合的羟值为包括水，为25至300，所述方法进一步表征为在不存在锡催化剂的情况下进行。

9. 发明授权

US4546122A Flexible polyurethane foams 失效
标题翻译：柔性聚氨酯泡沫
公开(公告)号：US4546122A
公开(公告)日：1985-10-08
申请号：US638325
申请日：1984-08-06
申请人： David A. Radovich , Michael K. Lowery
发明人： David A. Radovich , Michael K. Lowery
IPC分类号： C08G18/10 , C08G18/50 , C08G18/14 , C08G18/32 , C08G18/64
CPC分类号： C08G18/5045 , C08G18/10 , C08G2101/0008 , C08G2101/005 , Y10S521/904
摘要： The present invention is directed to a process for the production of a flexible polyurethane foam comprising reacting(a) an organic polyisocyanate, and(b) a coupled polyol which consists essentially of the reaction product of an organic polyisocyanate and an organic compound having a hydroxy functionality of at least 2 and a primary hydroxy group content of at least 30%, the ratio of hydroxyl groups in said organic compound to isocyanate groups being greater than 1,(c) in the presence of(i) a blowing agent,(ii) a catalyst, and(iii) a foam stabilizer, said foam stabilizer being capable of producing a flexible polyurethane foam meeting the standard specifications for high resilience polyurethane foam as set forth in ASTM D-3770-79, when used in a foam formulation based on toluene diisocyanate and either (A) a polymer polyol prepared by polymerizing one or more ethylenically unsaturated monomers in a polyether polyol, or (B) a dispersion of polyurea and/or polyhydrazodicarbonamide in a hydroxyl group containing material.
摘要翻译：本发明涉及一种生产柔性聚氨酯泡沫的方法，包括使（a）有机多异氰酸酯和（b）偶联多元醇反应，所述偶联多元醇基本上由有机多异氰酸酯和具有羟基的有机化合物的反应产物组成至少2的官能团和至少30％的伯羟基含量，所述有机化合物中的羟基与异氰酸酯基团的比例大于1，（c）在（i）发泡剂存在下，（ii ）催化剂，和（iii）泡沫稳定剂，所述泡沫稳定剂能够生产符合ASTM D-3770-79中所述的高回弹性聚氨酯泡沫塑料的标准规格的柔性聚氨酯泡沫，当用于基于泡沫配方的和（A）通过聚醚多元醇中聚合一种或多种烯键式不饱和单体制备的聚合物多元醇，或（B）聚脲和/或聚二酰氨基脲I的分散体 n是含羟基的材料。

10. 发明申请

US20080125507A1 Reduction of VOC emissions from low density cavity filling NVH polyurethane foams 审中-公开
标题翻译：从低密度空腔填充NVH聚氨酯泡沫中减少VOC排放
公开(公告)号：US20080125507A1
公开(公告)日：2008-05-29
申请号：US11604952
申请日：2006-11-28
申请人： Jack W. Jenny , David A. Radovich , Kenneth H. Sumner
发明人： Jack W. Jenny , David A. Radovich , Kenneth H. Sumner
IPC分类号： C08L75/04 , C08J9/00
CPC分类号： C08G18/5024 , C08G18/4072 , C08G18/632 , C08G2101/005 , C08G2101/0083 , C08G2290/00 , C08G2350/00
摘要： This invention relates to reactive systems for the production of low density, cavity filling polyurethane foams for NVH (noise vibration and harshness) application areas in which the system exhibits reduced VOC emissions. These foams comprises an isocyanate-reactive component having a viscosity of at least about 3,000 mPa·s, at 23° C., and comprises at least one amine-initiated compound which contains isocyanate-reactive groups.
摘要翻译：本发明涉及用于生产用于NVH（噪声振动和粗糙度）应用领域的低密度空腔填充聚氨酯泡沫的反应系统，其中系统显示减少的VOC排放。这些泡沫包括在23℃下具有至少约3,000mPa.s的粘度的异氰酸酯反应性组分，并且包含至少一种含有异氰酸酯反应性基团的胺引发化合物。

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