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1. 发明授权

US4205046A Reactor for phosphoric acid production 失效
标题翻译：磷酸生产反应器
公开(公告)号：US4205046A
公开(公告)日：1980-05-27
申请号：US940147
申请日：1978-09-06
申请人： Neculai Popovici
发明人： Neculai Popovici
IPC分类号： B01J16/00 , B01J19/18 , C01B25/22 , F01C1/08 , F01C1/00
CPC分类号： B01J16/00 , B01J19/1862 , C01B25/2204 , B01J2219/00114 , B01J2219/00121
摘要： There is disclosed a reactor designed to produce phosphoric acid by wet process. The reaction vessel proper is a cylindrical body divided into two compartments by a sinusoidal wall. The first space formed inside by the cylindrical wall of the vessel and the sinusoidal one and by one curved segment joining them is semi-circular and serves as pre-mixer provided with a stirring device and a pocket to allow the fluid flowing down through the bottom to reach the reaction space overhead. The reaction vat has two compartments and provided with a series of stirring devices so located as to permit an efficient, intimate mixture of the reaction medium. The vat is integrally roofed by a tight cover with many orifices left in it fitted for connection sleeves, such as: supply, gas venting, sight holes, and manholes, etc. The reactor incorporates as an integral unit a space devoted to the pre-mixing of reactants and means to guide the reaction medium through the reaction vessel; in this way the retention time required for the reaction process and calcium sulphate crystallization is decreased.
摘要翻译：公开了一种设计用于通过湿法生产磷酸的反应器。反应容器本体是通过正弦壁分成两个隔室的圆柱体。由容器的圆柱形壁形成的第一空间和连接它们的正弦曲线和一个弯曲段形成的第一空间是半圆形的，并且用作预混合器，其设置有搅拌装置和袋，以使流体向下流过底部达到反应空间的开销。反应槽具有两个隔室并且设置有一系列搅拌装置，以便允许反应介质的有效且紧密的混合。大桶通过紧密的盖子整齐地顶盖，许多孔留在其中，用于连接套管，例如：供气，排气，观察孔和检修孔等。反应器作为一个整体单元组合，混合反应物和引导反应介质通过反应容器的装置; 以这种方式，反应过程和硫酸钙结晶所需的保留时间降低。

2. 发明授权

US4242308A Controllable reaction medium single reactor for phosphoric acid production 失效
标题翻译：磷酸生产的可控反应介质单反应器
公开(公告)号：US4242308A
公开(公告)日：1980-12-30
申请号：US957949
申请日：1978-11-06
申请人： Neculai Popovici , Mihail Dochia , Mihai Dumitrescu , Iosif Spirea , Iacob Samoil
发明人： Neculai Popovici , Mihail Dochia , Mihai Dumitrescu , Iosif Spirea , Iacob Samoil
IPC分类号： B01J16/00 , B01J19/18 , C01B25/22 , B01F7/16 , B01J1/20 , B01J8/10
CPC分类号： C01B25/2204 , B01J16/00 , B01J19/1862 , B01J2219/00114 , B01J2219/00153
摘要： Apparatus for the continuous production of phosphoric acid from phosphate-containing rock and sulfuric acid, consisting of a reaction tank with a cylindrical side wall and a planar horizontal bottom and cover, wherein the improvement comprises a rigid vertical internal S-shaped baffle with one end smoothly merging into the said cylindrical side wall of the reaction tank and the other end freely projecting into the tank so as to permit of free circulation and flow of the reaction mixture from one side of the baffle to the other but dividing the reaction tank into two distinct zones.
摘要翻译：用于从含磷酸盐岩和硫酸连续生产磷酸的装置，其由具有圆柱形侧壁和平面水平底部和盖子的反应罐组成，其中改进包括具有一端的刚性垂直内部S形挡板平稳地融入反应罐的所述圆柱形侧壁，另一端自由地突出到罐中，以允许反应混合物从挡板的一侧自由循环和流动到另一侧，但将反应罐分成两部分不同的区域。

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