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1. 发明申请

WO2005056177A1 WATER-ABSORBING AGENT, MANUFACTURE METHOD THEREOF, AND ABSORBENT AND ABSORBENT ARTICLE MADE THEREFROM 审中-公开
标题翻译：吸水剂，其制造方法以及其吸收和吸收制品
公开(公告)号：WO2005056177A1
公开(公告)日：2005-06-23
申请号：PCT/JP2004/018871
申请日：2004-12-10
申请人： NIPPON SHOKUBAI CO., LTD. , WADA, Katsuyuki , NAGASAWA, Makoto , ISHIZAKI, Kunihiko
发明人： WADA, Katsuyuki , NAGASAWA, Makoto , ISHIZAKI, Kunihiko
IPC分类号： B01J20/26
CPC分类号： A61L15/24 , A61F13/535 , A61F2013/15463 , A61F2013/530569 , A61F2013/530591 , A61F2013/530708 , A61F2013/530737 , A61F2013/530766 , A61L15/42 , A61L15/60
摘要： We have found that to improve the heat retention by diapers and other absorbents, a heat retention indicator 1 of a water-absorbing resin which is defined in the present invention needs be 3.0oC/min or less and also that particular requirements need be met to satisfy this condition. If the requirements are met, a water-absorbing resin, absorbent, and absorbent article can be provided which has a heat retention indicator 1 of 0 to 3.0oC/min or less and which exhibits excellent heat retention and absorption.
摘要翻译：我们已经发现，为了提高尿布和其它吸收剂的保温性能，本发明中限定的吸水树脂的保温指示剂1需要为3.0℃/分钟或更低，并且还需要满足特定要求满足这个条件。如果满足要求，则可以提供吸水性树脂，吸收性物品和吸收性物品，其具有0〜3.0℃/分钟以下的保温指示剂1，并且显示优异的保温性和吸收性。

2. 发明申请

WO2006109842A1 PRODUCTION PROCESS OF POLYACRYLIC ACID (SALT) WATER-ABSORBENT RESIN 审中-公开
标题翻译：聚丙烯酸（盐）吸水树脂的生产工艺
公开(公告)号：WO2006109842A1
公开(公告)日：2006-10-19
申请号：PCT/JP2006/307792
申请日：2006-04-06
申请人： NIPPON SHOKUBAI CO., LTD. , KAWANO, Takaaki , FUJIMARU, Hirotama , ISHIZAKI, Kunihiko , WADA, Katsuyuki
发明人： KAWANO, Takaaki , FUJIMARU, Hirotama , ISHIZAKI, Kunihiko , WADA, Katsuyuki
IPC分类号： C08F20/06 , C08F8/00
CPC分类号： C08F220/06 , A61L15/60 , C08F20/06 , C08F222/1006 , C08K5/01 , C08K5/04 , C08L33/02
摘要： The present invention allows for production, with a high productivity, of a water-absorbent resin having an improved relationship between absorption capacity and water-soluble polymer which are conflicting properties of the water-absorbent resin, being easily controlled for polymerization reaction, being of no odor, being less colored, and being of high absorption properties. In the present invention, acrylic acid composition is neutralized with a basic composition having an iron content of 0.2 to 5 ppm by weight (relative to a basic compound exclusive of a solvent); and then polymerizing a resultant neutralized product, the acrylic acid composition including: (i) a methoxyphenol content of 10 to 200 ppm by weight relative to the weight of acrylic acid; and (ii) at least one compound content of which is 0 to 10 ppm by weight relative to the weight of acrylic acid, the compound being selected from the group consisting of protoanemonin and furfural.
摘要翻译：本发明允许以高生产率生产具有吸收性能与吸水性树脂相互矛盾的水溶性聚合物之间的改善的吸水性树脂，容易控制聚合反应的吸水性树脂为没有气味，少着色，吸收性好。在本发明中，丙烯酸组合物用铁含量为0.2〜5重量ppm（相对于不含溶剂的碱性化合物）的碱性组合物中和; 然后使得到的中和产物聚合，所述丙烯酸组合物包括：（i）甲氧基苯酚的含量相对于丙烯酸的重量为10-200ppm; 和（ii）相对于丙烯酸的重量，至少一种化合物含量为0-10ppm（重量），该化合物选自原水鳖素和糠醛。

3. 发明申请

WO2006088115A1 WATER ABSORBING AGENT, WATER ABSORBING ARTICLE AND METHOD FOR PRODUCTION OF WATER ABSORBING AGENT 审中-公开
标题翻译：吸水剂，吸水剂及其吸水剂的生产方法
公开(公告)号：WO2006088115A1
公开(公告)日：2006-08-24
申请号：PCT/JP2006/302782
申请日：2006-02-10
申请人： NIPPON SHOKUBAI CO., LTD. , KIMURA, Kazuki , FUJINO, Shin-ichi , WADA, Katsuyuki , ISHIZAKI, Kunihiko
发明人： KIMURA, Kazuki , FUJINO, Shin-ichi , WADA, Katsuyuki , ISHIZAKI, Kunihiko
IPC分类号： C08J3/12
CPC分类号： A61L15/60 , B01J20/26 , B01J20/264 , B01J20/267 , B01J20/28004 , B01J20/2803 , B01J20/28047 , B01J20/30 , B01J20/3028 , B01J2220/68 , C08J3/245 , C08J2300/14 , Y10T428/2982 , Y10T428/2991 , Y10T428/2998
摘要： An object of the present invention is to provide a water absorbing agent having a low amount of residual monomer, small variance of the amount of residual monomer among ranges of particle size distribution and favorable absorption properties, and being sanitary; an absorbing article; and a method for the production of a water absorbing agent. The water absorbing agent of the present invention has the amount of residual monomer of not higher than 500 ppm, and a residual monomer index of not greater than 0.30.The method for the production includes a first step of obtaining a hydrogel polymer by polymerizing an aqueous solution of a monomer including an unsaturated carboxylic acid and/or a salt thereof in the presence of a crosslinking agent;a second step of obtaining a water absorbent resin precursor which is in powder form and includes particles having a particle size of 300 to 850 µm and particles having a particle size of smaller than 300 µm as main components by drying said hydrogel polymer followed by pulverization and classification to adjust the particle size distribution,a third step of obtaining a water absorbent resin by heating a mixture of said water absorbent resin precursor and a surface crosslinking agent, which can form an ester bond around the surface of said water absorbent resin precursor,a fourth step of adding by spraying an aqueous solution that includes a sulfur-containing reducing agent to said water absorbent resin, and a fifth step of subjecting the mixture of the water absorbent resin and said aqueous solution to a heat treatment under an airflow of not lower than 40°C but not higher than 120°C.
摘要翻译：本发明的目的是提供一种具有少量残留单体的吸水剂，在粒度分布范围和吸收性能良好之间的残留单体量的变化小，并且是卫生的; 吸收物品和吸水剂的制造方法。本发明的吸水剂的残留单体的量不高于500ppm，残留单体指数不大于0.30。制备方法包括通过聚合水性聚合物获得水凝胶聚合物的第一步骤包含不饱和羧酸和/或其盐的单体在交联剂存在下的溶液;第二步，获得粉末形式的吸水性树脂前体，并且包括粒度为300至850μm的颗粒粒径小于300μm的颗粒作为主要组分，通过干燥所述水凝胶聚合物，然后粉碎和分级以调节粒度分布;第三步骤，通过加热所述吸水性树脂前体的混合物获得吸水性树脂以及可在所述吸水性树脂前体的表面周围形成酯键的表面交联剂，第四步骤通过将包含含硫还原剂的水溶液喷雾到所述吸水性树脂中而添加，第五步是在吸水性树脂和所述水溶液的混合物在不低于40°的气流下进行热处理但不高于120℃。

4. 发明申请

WO2006033477A1 PARTICULATE WATER-ABSORBING AGENT CONTAINING WATER-ABSORBENT RESIN AS A MAIN COMPONENT 审中-公开
标题翻译：含有吸水树脂的颗粒吸水剂作为主要成分
公开(公告)号：WO2006033477A1
公开(公告)日：2006-03-30
申请号：PCT/JP2005/018073
申请日：2005-09-22
申请人： NIPPON SHOKUBAI Co., Ltd. , WADA, Katsuyuki , UEDA, Hiroko , KIMURA, Kazuki , ISHIZAKI, Kunihiko
发明人： WADA, Katsuyuki , UEDA, Hiroko , KIMURA, Kazuki , ISHIZAKI, Kunihiko
IPC分类号： C08J3/24 , A61L15/60 , C08L101/14
CPC分类号： C08J3/24 , A61L15/46 , A61L15/60 , A61L2300/30 , A61L2300/404 , A61L2300/802 , C08J2300/14 , Y10T428/24893 , Y10T428/24942 , Y10T428/2982 , Y10T442/653
摘要： A problem to be solved of the present invention is to provide a particulate water-absorbing agent which not only ensures the many conventional physical properties (absorption rate, centrifuge retention capacity, absorbency against pressure, particle size distribution etc.) but also prevents odor which is generated after the resin is swollen by absorption. The water absorbent agent of the present invention therefore does not cause odor in actual use. As a result of intensive study of the foregoing problem, the present invention offers a way of controlling a specific odor component, which is generated from impurities and/or by-product derived from the raw material, after the high temperature process. In this way, the present invention successfully provides a water absorbent agent not causing odor after the resin is swollen by absorption.
摘要翻译：本发明要解决的问题是提供一种颗粒状吸水剂，其不仅确保了许多常规物理性质（吸收速率，离心保留能力，耐压吸收性，粒度分布等），而且还防止了气味在树脂通过吸收溶胀后产生。因此，本发明的吸水剂在实际使用中不会产生气味。通过深入研究上述问题，本发明提供一种在高温处理之后控制由原料衍生的杂质和/或副产物产生的特定气味成分的方法。以这种方式，本发明成功地提供了在树脂通过吸收溶胀而不产生气味的吸水剂。

5. 发明申请

WO2006014031A1 PARTICULATE WATER-ABSORBING AGENT WITH WATER-ABSORBING RESIN AS MAIN COMPONENT, METHOD FOR PRODUCTION OF THE SAME, AND ABSORBING ARTICLE 审中-公开
标题翻译：具有吸水树脂的颗粒吸水剂作为主要组分，其制备方法和吸收性物品
公开(公告)号：WO2006014031A1
公开(公告)日：2006-02-09
申请号：PCT/JP2005/014809
申请日：2005-08-05
申请人： NIPPON SHOKUBAI CO., LTD. , WADA, Katsuyuki , UEDA, Hiroko , KANTO, Teruyuki , ISHIZAKI, Kunihiko , IMURA, Motohiro
发明人： WADA, Katsuyuki , UEDA, Hiroko , KANTO, Teruyuki , ISHIZAKI, Kunihiko , IMURA, Motohiro
IPC分类号： B01J20/26 , B01J20/30 , A61F13/15 , A61F13/53
CPC分类号： B01J20/261 , A61F13/531 , A61F2013/530569 , A61F2013/5307 , A61F2013/530751 , A61L15/60 , B01J20/26 , B01J20/2803 , B01J2220/68 , C08F6/18 , C08F220/06
摘要： A particulate water-absorbing agent including a water-absorbing resin having superior property, and being suited for practical applications at high concentrations in absorbing cores such as diapers and the like without generation of any odor of the organic solvent can be obtained because no organic solvent is included.
摘要翻译：可以获得包含具有优异性能的吸水性树脂的颗粒状吸水剂，因为不产生有机溶剂的气味，因此可以获得高吸收性物质如尿布等的实际应用，因为没有有机溶剂已经包括了。

6. 发明申请

WO2005092955A1 PARTICULATE WATER ABSORBING AGENT WITH IRREGULARLY PULVERIZED SHAPE 审中-公开
标题翻译：颗粒状吸水剂与非正式粉碎形状
公开(公告)号：WO2005092955A1
公开(公告)日：2005-10-06
申请号：PCT/JP2005/006551
申请日：2005-03-29
申请人： NIPPON SHOKUBAI CO., LTD. , ISHIZAKI, Kunihiko , KITANO, Takahiro , ADACHI, Yoshifumi , UEDA, Hiroko , WADA, Katsuyuki
发明人： ISHIZAKI, Kunihiko , KITANO, Takahiro , ADACHI, Yoshifumi , UEDA, Hiroko , WADA, Katsuyuki
IPC分类号： C08J3/12
CPC分类号： C08J3/12 , C08J3/245 , C08J2300/14 , Y10T428/249924 , Y10T428/254 , Y10T428/2982 , Y10T428/2991 , Y10T428/2998 , Y10T442/2344
摘要： The present invention provides a particulate water absorbing agent for a thin type absorbing substrate suitable for actual use. A particulate water absorbing agent having irregularly pulverized shape, characterized by comprising, a surface crosslinked water-absorbing resin obtained by crosslinking polymerization of an unsaturated monomer with an acid group and/or salts thereof, which absorbing agent contains agglomerated particles therein and further satisfies (i) centrifuge retention capacity (CRC) in a physiological saline solution of not lower than 32 g/g, (ii) mass median particle size (D50) of 200 to 400 µm, and (iii) particles smaller than 600 µm and not smaller than 150 µm of 95 to 100% by weight. By using the particulate water absorbing agent, such absorbing articles can be obtained as have few rugged surface after water absorption, excellent liquid permeation property.
摘要翻译：本发明提供一种适用于实际使用的薄型吸收性基材用颗粒状吸水剂。具有不规则粉碎形状的颗粒状吸水剂，其特征在于，包含通过使不饱和单体与酸基和/或其盐交联聚合得到的表面交联吸水性树脂，所述吸收剂含有附聚颗粒，并进一步满足（ i）在不低于32g / g的生理盐水溶液中离心保留容量（CRC），（ii）质量中值粒径（D50）为200-400μm，（iii）小于600μm并且不小于 95〜100重量％的150μm以上。通过使用颗粒状吸水剂，可以获得这样的吸收制品，其吸水后的表面几乎不渗透，液体渗透性优异。

7. 发明申请

WO2002100451A2 WATER-ABSORBING AGENT AND PRODUCTION PROCESS THEREFOR, AND SANITARY MATERIAL 审中-公开
标题翻译：吸水剂及其生产工艺及卫生材料
公开(公告)号：WO2002100451A2
公开(公告)日：2002-12-19
申请号：PCT/JP2002/005642
申请日：2002-06-07
申请人： NIPPON SHOKUBAI CO., LTD. , NAKASHIMA, Yasuhisa , IKEUCHI, Hiroyuki , FUJITA, Yasuhiro , NAGASAWA, Makoto , SAKAMOTO, Shigeru , DAIROKU, Yorimichi , WADA, Katsuyuki , FUJINO, Shinichi , KITAYAMA, Toshimasa , HITOMI, Kazuhisa
发明人： NAKASHIMA, Yasuhisa , IKEUCHI, Hiroyuki , FUJITA, Yasuhiro , NAGASAWA, Makoto , SAKAMOTO, Shigeru , DAIROKU, Yorimichi , WADA, Katsuyuki , FUJINO, Shinichi , KITAYAMA, Toshimasa , HITOMI, Kazuhisa
IPC分类号： A61L15/60
CPC分类号： A61L15/60
摘要： There is provided: a production process for a water-absorbing agent having stable properties in a short time; and a water-absorbing agent. The production process comprises the step of blending an acid-group-containing water-absorbent resin powder with a noncrosslinkable water-soluble inorganic base and/or an irreducible alkaline-metal-salt pH buffer and further with a dehydratable crosslinking agent reactable with the acid group, thereby subjecting the resin powder to crosslinking treatment, or comprises the step of blending an acid-group-containing water-absorbent resin powder with the above base and/or pH buffer and further with a crosslinking agent reactable with the acid group, thereby subjecting the resin powder to crosslinking treatment, wherein the resin powder has a weight-average particle diameter of 300 to 600 µm wherein the ratio of fine powders having particle diameters of not larger than 150 µm in the resin is not more than 10 weight %.
摘要翻译：提供了一种在短时间内具有稳定性能的吸水剂的生产方法; 和吸水剂。生产方法包括将含酸基的吸水性树脂粉末与不可交联的水溶性无机碱和/或不可还原的碱金属盐pH缓冲剂以及可与酸反应的可脱水交联剂从而使树脂粉末进行交联处理，或者包括将含酸基的吸水性树脂粉末与上述碱和/或pH缓冲剂以及与酸基反应的交联剂混合的步骤，由此使树脂粉末进行交联处理，其中树脂粉末的重均粒径为300〜600μm，其中树脂中粒径不大于150μm的细粉末的比例不大于10重量％。

8. 发明申请

WO2006101271A1 METHOD OF MANUFACTURING WATER-ABSORBENT RESIN AGGLOMERATES, AND WATER-ABSORBENT RESIN AGGLOMERATES 审中-公开
标题翻译：制造吸水树脂粘合剂的方法和吸水树脂粘合剂
公开(公告)号：WO2006101271A1
公开(公告)日：2006-09-28
申请号：PCT/JP2006/306774
申请日：2006-03-24
申请人： NIPPON SHOKUBAI Co., Ltd. , NAGASHIMA, Teruhisa , NAGASAWA, Makoto , WADA, Katsuyuki
发明人： NAGASHIMA, Teruhisa , NAGASAWA, Makoto , WADA, Katsuyuki
IPC分类号： C08J3/12
CPC分类号： C08J3/12 , C08J2300/14 , C08J2333/08
摘要： The subject invention provides water-absorbent resin agglomerates having high strength and superior absorbency, and a method of producing water-absorbent resin agglomerates which can prevent agglomeration of hydrated water-absorbent resin, allowing the resin agglomerates to be efficiently dried and cured. A method of producing water-absorbent resin agglomerates according to the present invention comprises the steps of: (a) mixing first water-absorbent resin particles and an aqueous solution so as to produce a hydrated water-absorbent resin; and (b) mixing the hydrated water-absorbent resin with second water-absorbent resin particles or fine particles.
摘要翻译：本发明提供了具有高强度和优异吸收性的吸水性树脂凝聚体，以及可以防止水合吸水性树脂附聚的吸水性树脂凝聚体的制造方法，能够有效地干燥和固化树脂附聚物。根据本发明的吸水性树脂凝聚体的制造方法包括以下步骤：（a）将第一吸水性树脂颗粒和水溶液混合以制备水合吸水性树脂; 和（b）将水合吸水性树脂与第二吸水性树脂颗粒或细颗粒混合。

9. 发明申请

WO2008026783A1 WATER ABSORBING AGENT AND PRODUCTION METHOD THEREOF 审中-公开
标题翻译：吸水剂及其生产方法
公开(公告)号：WO2008026783A1
公开(公告)日：2008-03-06
申请号：PCT/JP2007/067455
申请日：2007-08-31
申请人： NIPPON SHOKUBAI Co., Ltd. , IKEUCHI, Hiroyuki , SAKAMOTO, Shigeru , MACHIDA, Sayaka , WADA, Katsuyuki
发明人： IKEUCHI, Hiroyuki , SAKAMOTO, Shigeru , MACHIDA, Sayaka , WADA, Katsuyuki
IPC分类号： C08L33/02 , B01J20/26
CPC分类号： C08F220/00 , A61L15/60 , B01J20/267 , C08F2/14
摘要： A water absorbing agent includes water absorbent resin particles which are obtained by polymerizing a water-soluble ethylenic unsaturated monomer and which internally include a cross-linked structure, wherein a pressurized void average radius index is 140 or more. As a result, it is possible to provide a water absorbing agent which essentially includes water absorbent resin particles and is suitable for use in a sanitary material. Specifically, it is possible to improve not only a performance for absorbing and retaining aqueous liquid without pressure or under pressure but also (i) a performance for quickly absorbing aqueous liquid with a great help of a performance of a fibrous material, (ii) a performance for dispersing the aqueous liquid after absorbing the aqueous liquid, and (iii) a performance for retaining the aqueous liquid after absorbing the aqueous liquid.
摘要翻译：吸水剂包括通过聚合水溶性烯属不饱和单体并且内部包含交联结构而获得的吸水性树脂颗粒，其中加压孔隙平均半径指数为140以上。结果，可以提供基本上包含吸水性树脂颗粒并适用于卫生材料的吸水剂。具体而言，不仅可以提高在没有压力或压力的情况下吸收和保持水性液体的性能，还可以（i）在纤维材料的性能的帮助下快速吸收水性液体的性能，（ii）在吸收水性液体之后分散水性液体的性能，和（iii）在吸收水性液体之后保持水性液体的性能。

10. 发明申请

WO2004113452A1 WATER ABSORBENT RESIN COMPOSTION AND PRODUCTION METHOD THEREOF 审中-公开
标题翻译：吸水树脂组合物及其制备方法
公开(公告)号：WO2004113452A1
公开(公告)日：2004-12-29
申请号：PCT/JP2004/009242
申请日：2004-06-23
申请人： NIPPON SHOKUBAI Co.,Ltd. , ADACHI, Yoshifumi , KITANO, Takahiro , FUJINO, Shinichi , WADA, Katsuyuki , TORII, Kazushi , IWAMURA, Taku , MACHIDA, Sayaka
发明人： ADACHI, Yoshifumi , KITANO, Takahiro , FUJINO, Shinichi , WADA, Katsuyuki , TORII, Kazushi , IWAMURA, Taku , MACHIDA, Sayaka
IPC分类号： C08L101/14
CPC分类号： A61L15/60 , A61F2013/530686 , A61F2013/530744
摘要： The production method of a water absorbent resin composition including a particulate water absorbent resin, wherein: 95 wt % or more of particles whose particle diameter is less than 850 µm and not less, than 106 µm are contained, and a weight average particle diameter of the particles is less than 500 µm and not less than 300 µ m and a logarith mic standard deviation (σξ) of a particle size distribution is 0.45 or less, and a water-soluble component of the water absorbent composition is 35 wt % or less, and a multivalent metal component is contained, and an extraction rate of the multivalent metal component is 5.0 wt % or more and less than 100 wt %, thereby providing the water absorbent resin composition, free from any coagulation of particles in high humidity, which has superiror absorbent property in terms of an absorbency and a diffusing absorbency under pressure.
摘要翻译：包含颗粒状吸水性树脂的吸水性树脂组合物的制造方法，其中，含有95重量％以上的粒径小于850μm且不小于106μm的颗粒，重均粒径为颗粒小于500μm且不小于300μm，并且粒度分布的对数麦克风标准偏差（sigmaxi）为0.45以下，吸水性组合物的水溶性成分为35重量％以下，并且含有多价金属成分，多价金属成分的提取率为5.0重量％以上且小于100重量％，从而提供在高湿度下不会发生任何凝结的吸水性树脂组合物，其中，在吸收性和压力下的扩散吸收性方面具有超吸收性。

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