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1. 发明公开

EP0349307A2 Process for producing pitch-based carbon fibres superior in compressive physical properties 失效
标题翻译：一种用于碳质纤维的制造过程中具有改善的物理印刷性质。
公开(公告)号：EP0349307A2
公开(公告)日：1990-01-03
申请号：EP89306590.4
申请日：1989-06-29
申请人： NIPPON OIL COMPANY, LIMITED
发明人： Takashima, Hiroaki , Kato, Osamu , Azami, Kiyoshi , Nakajima, Hajime
IPC分类号： C10C3/00 , D01F9/12
CPC分类号： C10C3/00 , D01F9/145
摘要： A process for producing a pitch-based carbon fiber comprises hydrogenating a carbonaceous pitch in the presence of a hydrogenation catalyst to add to the pitch two moles or more hydrogen per pitch molecule; heat-treating the hydrogenated pitch at atmospheric pressure or under reduced pressure to obtain an optically anisotropic pitch; collecting from said optically anisotropic pitch a component which is insoluble in an organic solvent having a solubility parameter at 25°C of 7.4 to 9.0 and soluble in an organic solvent having a solubility parameter at 25°C of 9.2 to 11.0 to obtain a spinning pitch having an optically anisotropic phase content of 5% to 40% by volume; spinning said spinning pitch; and thereafter making the resulting pitch fiber infusible and then carbonizing the thus-infusiblized pitch fiber.
摘要翻译：一种用于生产沥青基碳纤维的方法包括加氢在加氢催化剂的存在下，碳质沥青添加到桨距两摩尔或每分子间距更氢; 热处理在大气压或在减压下，得到的光学各向异性沥青的氢化沥青; 从所述收集光学各向异性沥青的组分的所有这是在具有在25℃下的7.4的溶解度参数，以9.0不溶于有机溶剂和可溶于有机溶剂具有在25℃下的9.2的溶解度参数，以11.0得到的纺丝沥青具有5％至40％的光学各向异性相的含量以体积计; 所述纺纺丝沥青; 并且此后使所得到的沥青纤维不熔并进行碳化由此infusiblized沥青纤维。

2. 发明授权

EP0349307B1 Process for producing pitch-based carbon fibres superior in compressive physical properties 失效
标题翻译：一种用于碳质纤维的制造过程中具有改善的物理印刷性质。
公开(公告)号：EP0349307B1
公开(公告)日：1994-11-09
申请号：EP89306590.4
申请日：1989-06-29
申请人： NIPPON OIL COMPANY, LIMITED
发明人： Takashima, Hiroaki , Kato, Osamu , Azami, Kiyoshi , Nakajima, Hajime
IPC分类号： C10C3/00 , D01F9/12
CPC分类号： C10C3/00 , D01F9/145

3. 发明公开

EP0349307A3 Process for producing pitch-based carbon fibres superior in compressive physical properties 失效
标题翻译：基于沥青的碳纤维织物在压缩物理性能中的应用及其生产方法
公开(公告)号：EP0349307A3
公开(公告)日：1990-03-07
申请号：EP89306590.4
申请日：1989-06-29
申请人： NIPPON OIL COMPANY, LIMITED
发明人： Takashima, Hiroaki , Kato, Osamu , Azami, Kiyoshi , Nakajima, Hajime
IPC分类号： C10C3/00 , D01F9/12
CPC分类号： C10C3/00 , D01F9/145
摘要： A process for producing a pitch-based carbon fiber comprises hydrogenating a carbonaceous pitch in the presence of a hydrogenation catalyst to add to the pitch two moles or more hydrogen per pitch molecule; heat-treating the hydrogenated pitch at atmospheric pressure or under reduced pressure to obtain an optically anisotropic pitch; collecting from said optically anisotropic pitch a component which is insoluble in an organic solvent having a solubility parameter at 25°C of 7.4 to 9.0 and soluble in an organic solvent having a solubility parameter at 25°C of 9.2 to 11.0 to obtain a spinning pitch having an optically anisotropic phase content of 5% to 40% by volume; spinning said spinning pitch; and thereafter making the resulting pitch fiber infusible and then carbonizing the thus-infusiblized pitch fiber.

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