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1. 发明授权

US4619959A Continuous production process of styrene-base resin 失效
标题翻译：苯乙烯基树脂的连续生产工艺
公开(公告)号：US4619959A
公开(公告)日：1986-10-28
申请号：US737531
申请日：1985-05-24
申请人： Tetsuyuki Matsubara , Norifumi Ito , Kazuo Sugazaki , Kouzo Ichikawa , Mune Iwamoto , Toshihiko Ando
发明人： Tetsuyuki Matsubara , Norifumi Ito , Kazuo Sugazaki , Kouzo Ichikawa , Mune Iwamoto , Toshihiko Ando
IPC分类号： C08F2/44 , C08F12/08 , C08F291/02 , C08K5/20
CPC分类号： C08F12/08
摘要： A process for producing a styrene-base resin having improved moldability and a good hue by continuously adding a specific higher fatty acid amide in a dissolved or molten state, and/or a mixture of a specific higher fatty acid amide and a specific metallic soap in a molten state, to a styrene-base resin in the course of its production by continuous bulk or solution polymerization. The above process is particularly effective for rubber-modified styrene-acrylonitrile resins.
摘要翻译：通过在溶解或熔融状态下连续加入特定的高级脂肪酸酰胺和/或特定的高级脂肪酸酰胺和特定的金属皂的混合物来制备具有改进的成型性和良好的色调的苯乙烯基树脂的方法熔融状态，通过连续的本体或溶液聚合在其生产过程中与苯乙烯基树脂接触。上述方法对于橡胶改性苯乙烯 - 丙烯腈树脂是特别有效的。

2. 发明授权

US5210132A Continuous process for preparing rubber modified high impact resin 失效
标题翻译：制备橡胶改性高冲击树脂的连续工艺
公开(公告)号：US5210132A
公开(公告)日：1993-05-11
申请号：US961026
申请日：1992-10-14
申请人： Tetsuyuki Matsubara , Norifumi Ito , Mune Iwamoto , Kazuo Sugazaki , Toshihiko Ando , Yasuo Furuta , Kouzo Ichikawa , Hitoshi Ozawa
发明人： Tetsuyuki Matsubara , Norifumi Ito , Mune Iwamoto , Kazuo Sugazaki , Toshihiko Ando , Yasuo Furuta , Kouzo Ichikawa , Hitoshi Ozawa
IPC分类号： C08F279/02 , C08F291/02
CPC分类号： C08F291/02 , C08F279/02
摘要： A process for preparing rubber modified high impact resins by dissolving a rubbery polymer in a monomer containing an aromatic vinyl monomer or a mixture of an aromatic vinyl monomer and a vinyl cyanide monomer followed by polymerizing the monomer, the two steps being carried out in at least two polymerization reactors with a particle disperser placed between the first and second reactors. High impact resins having excellent surface properties are obtained with a savings in a power consumption by controlling:(1) the relationship between the concentration of the polymerized monomer and the content of the rubbery polymer in the first reactor;(2) the relationship between the volume occupied by the polymerizing liquid in the first reactor and the inner volume of the particle disperser; and(3) the peripheral linear velocity of a shearing stirrer in the particle disperser.
摘要翻译：通过将橡胶状聚合物溶解在含有芳族乙烯基单体或芳香族乙烯基单体和乙烯基氰单体的混合物的单体中，然后使单体聚合，制备橡胶改性的高冲击性树脂的方法，这两个步骤至少进行两个具有放置在第一和第二反应器之间的分散器的聚合反应器。通过控制：（1）聚合单体的浓度与第一反应器中橡胶状聚合物的含量之间的关系，可以节省功耗，获得具有优异表面性能的高冲击性树脂; （2）第一反应器中的聚合液体占据的体积与粒子分散器的内体积之间的关系; 和（3）粒子分散器中的剪切搅拌器的外围线速度。

3. 发明授权

US5191023A Block-copolymerized-rubber-modified styrene copolymers 失效
标题翻译：嵌段共聚 - 橡胶改性苯乙烯共聚物
公开(公告)号：US5191023A
公开(公告)日：1993-03-02
申请号：US726951
申请日：1991-07-08
申请人： Mune Iwamoto , Norifumi Ito , Tetsuyuki Matsubara , Kazuo Sugazaki , Toshihiko Ando
发明人： Mune Iwamoto , Norifumi Ito , Tetsuyuki Matsubara , Kazuo Sugazaki , Toshihiko Ando
IPC分类号： C08F279/04 , C08F279/00 , C08F285/00 , C08F287/00
CPC分类号： C08F287/00
摘要： The present invention relates to rubber-modified styrene copolymer that exhibits excellent rigidity, impact strength, external appearance and fluidity, while retaining rigidity, impact properties and external appearance, and when prepared by copolymerizing a maleimide monomer, has high heat resistance and therefore is suitable for materials for components of electric equipments, electronic equipments, automobiles and business machines.

4. 发明授权

US4808661A Rubber dispersed copolymer resin 失效
标题翻译：橡胶分散共聚树脂
公开(公告)号：US4808661A
公开(公告)日：1989-02-28
申请号：US899867
申请日：1986-08-25
申请人： Mune Iwamoto , Norifumi Ito , Kazuo Sugazaki , Tetsuyuki Matsubara , Toshihiko Ando
发明人： Mune Iwamoto , Norifumi Ito , Kazuo Sugazaki , Tetsuyuki Matsubara , Toshihiko Ando
IPC分类号： C08L23/06 , C08F279/02 , C08L23/10 , C08L25/00 , C08L25/12 , C08L35/06 , C08L51/04 , C08L55/02 , C08L55/04
CPC分类号： C08L35/06 , C08F279/02 , C08L25/12 , C08L51/04 , C08L55/02
摘要： The invention provides a rubber dispersed copolymer resin having excellent heat resistance, impact strength and moldability and composed of (1) a dispersed phase formed of a rubbery polymer and copolymerized styrene-type, acrylonitrile-type and maleimide-type monomers, said rubbery polymer specifically controlled occluding the copolymer of monomers, being grafted with the copolymer and/or forming a multicomponent gel together with copolymers, and (2) a continuous phase formed at least of a specifically controlled copolymer of the styrenetype, acrylonitrile-type and maleimide-type monomers. The resin is useful as a molding material for electric appliances, electronic equipment and cars.
摘要翻译：本发明提供了具有优异的耐热性，冲击强度和成型性的橡胶分散共聚物树脂，它由（1）由橡胶状聚合物和共聚苯乙烯型丙烯腈 - 型马来酰亚胺型单体形成的分散相组成，所述橡胶状聚合物特别控制阻塞共聚物与共聚物接枝和/或与共聚物一起形成多组分凝胶，和（2）至少形成苯乙烯类，丙烯腈型和马来酰亚胺型单体的特异性控制共聚物的连续相。该树脂可用作电器，电子设备和汽车的成型材料。

5. 发明授权

US4972024A Anionically-polymerized-rubber-modified styrene copolymers 失效
标题翻译：阴离子聚合橡胶改性苯乙烯共聚物
公开(公告)号：US4972024A
公开(公告)日：1990-11-20
申请号：US224329
申请日：1988-07-26
申请人： Mune Iwamoto , Norifumi Ito , Kazuo Sugazaki , Tetsuyuki Matsubara , Toshihiko Ando , Yasuo Furuta
发明人： Mune Iwamoto , Norifumi Ito , Kazuo Sugazaki , Tetsuyuki Matsubara , Toshihiko Ando , Yasuo Furuta
IPC分类号： C08F279/04 , C08F287/00 , C08F297/04
CPC分类号： C08F287/00 , C08F279/04 , C08F297/04
摘要： Disclosed herein is a rubber-modified styrene copolymer which contains as an impact strength modifier a rubbery polymer having a viscosity of 2-250 centipoises as measured at 25.degree. C. as a 5 wt. % styrene solution and a styrene insoluble content lower than 0.1 wt. %, produced by anionic polymerization and dispersed in a continuous phase of a styrene-acrylonitrile copolymer. The rubbery polymer contains small particles of the same styrene-acrylonitrile copolymer occluded in the form of cells. The areas of particles in each of which the maximum cell diameter is smaller than 0.1 .mu.m are at least 40% of the area of all the particles of the rubbery polymer and the volume average particle size of these particles is 0.1-0.4 .mu.m. The weight ratio of the monomers in the styrene-acrylonitrile copolymer is 90/10.gtoreq.styrene/acrylonitrile.gtoreq.55/45. Per 100 parts by weight of the copolymer, the proportions of polymers having a molecular weight greater than 1,000,000 is smaller than 0.5 part by weight while the proportion of polymers having a molecular weight greater than 1,200,000 is smaller than 0.01 part by weight.
摘要翻译：本文公开了一种橡胶改性苯乙烯共聚物，其包含作为冲击强度改性剂的橡胶状聚合物，其粘度为2550厘泊，在25℃下测量为5重量％％苯乙烯溶液和低于0.1重量％的苯乙烯不溶物含量。％，通过阴离子聚合制备并分散在苯乙烯 - 丙烯腈共聚物的连续相中。橡胶状聚合物含有以细胞形式封闭的相同苯乙烯 - 丙烯腈共聚物的小颗粒。最大电池直径小于0.1μm的颗粒面积至少为橡胶状聚合物颗粒面积的40％，这些颗粒的体积平均粒径为0.1-0.4μm。苯乙烯 - 丙烯腈共聚物中单体的重量比为90/10> / =苯乙烯/丙烯腈> / = 55/45。每100重量份共聚物，分子量大于1,000,000的聚合物的比例小于0.5重量份，而分子量大于1,200,000的聚合物的比例小于0.01重量份。

6. 发明授权

US4758644A Bromostyrene composition 失效
标题翻译：溴苯乙烯组成
公开(公告)号：US4758644A
公开(公告)日：1988-07-19
申请号：US943892
申请日：1986-12-18
申请人： Mune Iwamoto , Norifumi Ito , Kazuo Sugazaki , Tetsuyuki Matsubara , Toshihiko Ando
发明人： Mune Iwamoto , Norifumi Ito , Kazuo Sugazaki , Tetsuyuki Matsubara , Toshihiko Ando
IPC分类号： C07C15/42 , C07C17/00 , C07C17/42 , C07C25/28 , C07C67/00 , C08K5/13 , C08F12/16
CPC分类号： C07C17/42
摘要： A bromostyrene composition having overcome the unstability of bromostyrenes and being stable at the time of its storage and transportation is provided, which composition comprises 100 parts by weight of a styrene substituted with one, two or three bromine atoms on the benzene nucleus thereof or a mixture of the foregoing, 20 to 3,000 parts by weight of an aromatic vinyl compound such as styrene and 0.001 to 0.05 part by weight of a polymerization inhibitor.
摘要翻译：提供了克服溴苯乙烯不稳定性并在其储存和运输时稳定的溴苯乙烯组合物，该组合物包含100重量份在苯核上被一个，两个或三个溴原子取代的苯乙烯或混合物的20〜3,000重量份的苯乙烯等芳香族乙烯基化合物和阻聚剂0.001〜0.05重量份。

7. 发明授权

US5480947A Diguanamines and preparation process, derivatives and use thereof 失效
公开(公告)号：US5480947A
公开(公告)日：1996-01-02
申请号：US414007
申请日：1995-03-30
申请人： Tetsuya Oishi , Hiroshi Ozawa , Minato Karasawa , Masamitsu Inomata , Izumi Mega , Atsuyoshi Yamauchi , Kazunori Kamada , Shigeru Nakahata , Katsumi Sakamoto , Tatsunobu Nakashima , Akito Watanabe , Jin Suzuki , Kouhei Ohkawa , Satoshi Furusawa , Hiroshi Ono , Kazuo Sugazaki
发明人： Tetsuya Oishi , Hiroshi Ozawa , Minato Karasawa , Masamitsu Inomata , Izumi Mega , Atsuyoshi Yamauchi , Kazunori Kamada , Shigeru Nakahata , Katsumi Sakamoto , Tatsunobu Nakashima , Akito Watanabe , Jin Suzuki , Kouhei Ohkawa , Satoshi Furusawa , Hiroshi Ono , Kazuo Sugazaki
IPC分类号： B32B5/16 , C07D251/18 , C08F283/00 , C08G12/30 , C08G18/38 , C08G59/00 , C08G59/50 , C08G73/06 , C08J9/00 , C08J9/14 , C08L61/26 , C08G8/36
CPC分类号： C08J9/14 , C07D251/18 , C08G12/30 , C08G18/3851 , C08G59/5086 , C08L61/26 , C08G2101/00 , C08J2361/26
摘要： Provided by the present invention are novel diguanamine derivatives, led by 2,5/2,6-bis(4,6-diamino-1,3,5-triazin-2-yl)-bicyclo[2.2.1]heptanes and 1,3/1,4-bis(4,6-diamino-1,3,5-triazin-2-yl)-cyclohexanes, and derivatives thereof, applications of these compounds in fields such as adhesives and paints, utilization of these compounds in flame-retarding, thermal stabilization and compatibilization methods of resins, thermosetting molding compositions and thermosetting expansion-molding compositions making use of these compounds, as well as polymeric microspheres also using these compounds. These compounds are expected to find wide spread industrial utility as various excellent properties can be obtained by using them.

8. 发明授权

US5936048A Method for preparing modified resins and their applications 失效
标题翻译：改性树脂的制备方法及应用
公开(公告)号：US5936048A
公开(公告)日：1999-08-10
申请号：US102876
申请日：1998-06-24
申请人： Tetsuya Oishi , Kazuo Sugazaki , Jin Suzuki
发明人： Tetsuya Oishi , Kazuo Sugazaki , Jin Suzuki
IPC分类号： C08F8/00 , C08F8/08 , C08F8/28 , C08F8/30 , C08G12/00 , C08G59/06 , C08G61/00 , C08G63/91 , C08G65/48 , C08G69/48 , C08K5/00 , C08L23/26 , C08L63/00 , C08L67/02 , C08L71/12 , H05K3/34 , C08G59/14 , C08K3/32 , C08K5/49
CPC分类号： C08L71/126 , C08F8/00 , C08F8/08 , C08F8/28 , C08F8/30 , C08F8/40 , C08G12/00 , C08G59/063 , C08G61/00 , C08G63/914 , C08G65/485 , C08G69/48 , C08K5/0066 , C08L23/26 , C08L63/00 , C08L67/02 , B23K2201/42 , H05K2201/10734 , H05K2203/081 , H05K2203/087 , H05K2203/1105 , H05K2203/176 , H05K3/3436 , H05K3/3494
摘要： There are herein disclosed a method for preparing a modified resin which comprises thermal/reaction by the use of a norbornenyl group-containing compound typified by norbornenecarboguanamine or its derivative, a method for preparing an epoxy-modified resin which comprises the step of reacting the above-mentioned modified resin and an epoxide, a flame-retarding method, a thermal stabilization method, a compatibilizing method and a surface modification method which comprise utilizing the modified resin, as well as a coating resin composition and an adhesive resin composition containing the modified resin.According to the preparation methods of the present invention, the deterioration of a material scarcely occurs, and a functional group which is excellent in flame retardancy, thermal stability, compatibility and the like can be introduced to the resins. By the utilization of these techniques, there can be obtained a flame-retardant material having a good char formability, a thermally stable material whose molded articles can inhibit heat deterioration, a material excellent in miscibility between different kinds of resins, a surface-modified material which is excellent in adhesion and coating properties and the like.
摘要翻译：本文公开了一种制备改性树脂的方法，该改性树脂包括通过使用以降冰片烯基组合物为代表的降冰片烯基组合物或其衍生物的热/反应，一种环氧改性树脂的制备方法，该方法包括使上述所述改性树脂和环氧化物，阻燃方法，热稳定化方法，相容化方法和表面改性方法，包括使用改性树脂，以及涂料树脂组合物和含有改性树脂的粘合剂树脂组合物。根据本发明的制备方法，几乎不发生材料的劣化，并且可以将具有优异的阻燃性，热稳定性，相容性等的官能团引入到树脂中。通过利用这些技术，可以获得具有良好的成型性的阻燃材料，其成型制品可以抑制热劣化的热稳定材料，不同种类的树脂之间的混溶性优异的材料，表面改性材料其粘合性和涂布性等优异。

9. 发明授权

US5674947A Method for preparing modified resins and their applications 失效
标题翻译：改性树脂的制备方法及应用
公开(公告)号：US5674947A
公开(公告)日：1997-10-07
申请号：US514730
申请日：1995-08-14
申请人： Tetsuya Oishi , Kazuo Sugazaki , Jin Suzuki
发明人： Tetsuya Oishi , Kazuo Sugazaki , Jin Suzuki
IPC分类号： C08F8/00 , C08F8/08 , C08F8/28 , C08F8/30 , C08G12/00 , C08G59/06 , C08G61/00 , C08G63/91 , C08G65/48 , C08G69/48 , C08K5/00 , C08L23/26 , C08L63/00 , C08L67/02 , C08L71/12 , H05K3/34 , C08F277/00 , C08F271/02 , C08F283/08 , C08F283/02
CPC分类号： C08L71/126 , C08F8/00 , C08F8/08 , C08F8/28 , C08F8/30 , C08F8/40 , C08G12/00 , C08G59/063 , C08G61/00 , C08G63/914 , C08G65/485 , C08G69/48 , C08K5/0066 , C08L23/26 , C08L63/00 , C08L67/02 , B23K2201/42 , H05K2201/10734 , H05K2203/081 , H05K2203/087 , H05K2203/1105 , H05K2203/176 , H05K3/3436 , H05K3/3494
摘要： There are herein disclosed a method for preparing a modified resin which comprises thermal/reaction by the use of a norbornenyl group-containing compound typified by norbornenecarboguanamine or its derivative, a method for preparing an epoxy-modified resin which comprises the step of reacting the above-mentioned modified resin and an epoxide, a flame-retarding method, a thermal stabilization method, a compatibilizing method and a surface modification method which comprise utilizing the modified resin, as well as a coating resin composition and an adhesive resin composition containing the modified resin. According to the, preparation methods of the present invention, the deterioration of a material scarcely occurs, and a functional group which is excellent in flame retardancy, thermal stability, compatibility and the like can be introduced to the resins. By the utilization of these techniques, there can be obtained a flame-retardant material having a good char formability, a thermally stable material whose molded articles can inhibit heat deterioration, a material excellent in miscibility between different kinds of resins, a surface-modified material which is excellent in adhesion and coating properties and the like.
摘要翻译：本文公开了一种制备改性树脂的方法，该改性树脂包括通过使用以降冰片烯基组合物为代表的降冰片烯基组合物或其衍生物的热/反应，一种环氧改性树脂的制备方法，该方法包括使上述所述改性树脂和环氧化物，阻燃方法，热稳定化方法，相容化方法和表面改性方法，包括使用改性树脂，以及涂料树脂组合物和含有改性树脂的粘合剂树脂组合物。根据本发明的制备方法，几乎不发生材料的劣化，并且可以向树脂中引入阻燃性，热稳定性，相容性等优异的官能团。通过利用这些技术，可以获得具有良好的成型性的阻燃材料，其成型制品可以抑制热劣化的热稳定材料，不同种类的树脂之间的混溶性优异的材料，表面改性材料其粘合性和涂布性等优异。

10. 发明授权

US5545702A Diguanamines and preparation process, derivatives and use thereof 失效
标题翻译：二uan胺及其制备方法，衍生物及其应用
公开(公告)号：US5545702A
公开(公告)日：1996-08-13
申请号：US538600
申请日：1995-10-03
申请人： Tetsuya Oishi , Hiroshi Ozawa , Minato Karasawa , Masamitsu Inomata , Izumi Mega , Atsuyoshi Yamauchi , Kazunori Kamada , Shigeru Nakahata , Katsumi Sakamoto , Tatsunobu Nakashima , Akito Watanabe , Jin Suzuki , Kouhei Ohkawa , Satoshi Furusawa , Hiroshi Ono , Kazuo Sugazaki
发明人： Tetsuya Oishi , Hiroshi Ozawa , Minato Karasawa , Masamitsu Inomata , Izumi Mega , Atsuyoshi Yamauchi , Kazunori Kamada , Shigeru Nakahata , Katsumi Sakamoto , Tatsunobu Nakashima , Akito Watanabe , Jin Suzuki , Kouhei Ohkawa , Satoshi Furusawa , Hiroshi Ono , Kazuo Sugazaki
IPC分类号： B32B5/16 , C07D251/18 , C08F283/00 , C08G12/30 , C08G18/38 , C08G59/00 , C08G59/50 , C08G73/06 , C08J9/00 , C08J9/14 , C08L61/26 , C08L61/34
CPC分类号： C08J9/14 , C07D251/18 , C08G12/30 , C08G18/3851 , C08G59/5086 , C08L61/26 , C08G2101/00 , C08J2361/26
摘要： Provided by the present invention are novel diguanamine derivatives, led by 2,5/2,6-bis(4,6-diamino-1,3,5-triazin-2-yl)-bicyclo[2.2.1]heptanes and 1,3/1,4-bis(4,6-diamino-1,3,5-triazin-2-yl)-cyclohexanes, and derivatives thereof, applications of these compounds in fields such as adhesives and paints, utilization of these compounds in flame-retarding, thermal stabilization and compatibilization methods of resins, thermosetting molding compositions and thermosetting expansion-molding compositions making use of these compounds, as well as polymeric microspheres also using these compounds. These compounds are expected to find wide spread industrial utility as various excellent properties can be obtained by using them.
摘要翻译：本发明提供的是由2,5 / 2,6-双（4,6-二氨基-1,3,5-三嗪-2-基） - 双环[2.2.1]庚烷和1 ，3 / 1,4-双（4,6-二氨基-1,3,5-三嗪-2-基） - 环己烷及其衍生物，这些化合物在粘合剂和油漆等领域的应用，这些化合物的利用使用这些化合物的树脂的阻燃，热稳定化和增容方法，热固性模塑组合物和使用这些化合物的热固性膨胀成型组合物，以及也使用这些化合物的聚合物微球。预期这些化合物可以获得广泛的工业实用性，因为通过使用它们可以获得各种优异的性能。

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