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1. 发明授权

US4199434A Feedstock treatment 失效
标题翻译：原料处理
公开(公告)号：US4199434A
公开(公告)日：1980-04-22
申请号：US876882
申请日：1978-02-13
申请人： Morgan C. Sze , Thomas M. Bennett , Harold Unger
发明人： Morgan C. Sze , Thomas M. Bennett , Harold Unger
IPC分类号： C09C1/48 , C10B55/00
CPC分类号： C09C1/48 , C10B55/00 , B01J19/00
摘要： A pyrolysis fuel oil is treated by soaking in the presence of sulfur for a period of time sufficient to react the highly unsaturated compounds present in the oil, followed by heating the soaked fuel oil at a temperature of from 850.degree. F. to 1100.degree. F. and an outlet pressure of from 300 to 600 psig to provide a treated feed having an API gravity of -3.degree. or less. The feed may be employed for the production of needle coke and/or carbon black and/or electrode binder pitch.
摘要翻译：通过在硫存在下浸泡处理热解燃料油足以使存在于油中的高度不饱和化合物反应足够的时间，然后在850°F至1100°F的温度下加热浸渍的燃料油并且出口压力为300至600psig，以提供API比重为-3度或更小的经处理的进料。饲料可用于生产针状焦炭和/或炭黑和/或电极粘合剂沥青。

2. 发明授权

US4547284A Coke production 失效
标题翻译：可口可乐生产
公开(公告)号：US4547284A
公开(公告)日：1985-10-15
申请号：US640228
申请日：1984-08-13
申请人： Morgan C. Sze , Thomas M. Bennett , Andre A. Simone , Dennis F. Ogren , Mikio Nakaniwa , Kenji Furukawa
发明人： Morgan C. Sze , Thomas M. Bennett , Andre A. Simone , Dennis F. Ogren , Mikio Nakaniwa , Kenji Furukawa
IPC分类号： C10B55/00 , C10G9/14
CPC分类号： C10B55/00
摘要： In the delayed coking of a coking feedstock wherein the feedstock is continuously heated in a coking heater and introduced into a coke drum, the heater is operated to provide a coke drum temperature of from 415.degree. to 455.degree. C., and, after filling of the drum to the desired level, feedstock introduction is discontinued and the coke drum contents are heated at a temperature of 450.degree. C. to 500.degree. C., and which heating temperature is at least 10.degree. C. greater than the coking temperature, by passing a non-coking vapor through the contents of the drum to reduce the volatile combustible matter content to a value of 4% to 10% by weight and thereby reduce the CTE of the formed coke. The process is applicable to the production of needle coke from various kinds of feedstocks, in particular from a petroleum feedstock wherein the feedstock is initially treated by thermal soaking in the presence of sulfur, followed by thermal cracking to increase the aromaticity. Noncrystalline substances may be removed prior to coking to further improve the process.
摘要翻译：在焦化原料的延迟焦化中，其中原料在焦化加热器中连续加热并引入焦炭鼓中，操作加热器以提供415℃至455℃的焦炭鼓温度，并且在填充将鼓转到所需水平，原料引入停止，并将焦碳鼓内容物在450℃至500℃的温度下加热，并且该加热温度比焦化温度高至少10℃，由使非焦化蒸气通过鼓的内容物，以将易挥发的可燃物含量减少到4重量％至10重量％，从而降低形成的焦炭的CTE。该方法适用于从各种原料，特别是石油原料生产针状焦，其中原料最初通过在硫的存在下进行热浸，然后进行热裂解以增加芳香性。在结焦之前可以除去非结晶物质以进一步改善该方法。

3. 发明授权

US4108798A Process for the production of petroleum coke 失效
标题翻译：石油焦生产工艺
公开(公告)号：US4108798A
公开(公告)日：1978-08-22
申请号：US702647
申请日：1976-07-06
申请人： Morgan C. Sze , Thomas M. Bennett , Andre A. Simone , Kiyoshige Hayashi , Mikio Nakaniwa , Nobuyuki Kobayashi , Yoshihiko Hase
发明人： Morgan C. Sze , Thomas M. Bennett , Andre A. Simone , Kiyoshige Hayashi , Mikio Nakaniwa , Nobuyuki Kobayashi , Yoshihiko Hase
IPC分类号： C10B57/04 , C01B31/04 , C10B55/00 , C10G9/00 , C10G51/02 , C10G9/14 , C10G37/02
CPC分类号： C10B55/00 , C10G51/023
摘要： A high crystalline coke can be prepared by heat-soaking a petroleum feedstock in the presence of added dissolved sulfur, heating to effect controlled thermal cracking thereof, separating non-crystalline substances as pitch, recovering a heavy cokable residue from the pitch free feed, and subjecting the residue to delayed coking.
摘要翻译：可以通过在加入的溶解硫的存在下加热石油原料，加热以实现其受控制的热裂解，将非结晶物质分离为沥青，从无沥青游离进料中回收重的可还原残余物，并制备高结晶焦炭，以及使残留物延迟焦化。

4. 再颁专利

USRE32265E Hydrogenation of high boiling hydrocarbons 失效
标题翻译：高沸点烃的氢化
公开(公告)号：USRE32265E
公开(公告)日：1986-10-14
申请号：US735101
申请日：1985-05-17
申请人： Harold Unger , Morgan C. Sze , Roger P. Van Dreisen
发明人： Harold Unger , Morgan C. Sze , Roger P. Van Dreisen
IPC分类号： C10G67/02 , C10G67/06 , F02B3/06
CPC分类号： C10G67/06 , C10G67/02 , F02B3/06
摘要： .[.In a hydrogenation operation employing an ebullated catalytic bed, recycle is recovered from the hydrogenated product with at least 25%, by volume, of the recycle boiling above 950.degree. F. The recycle is cooled to a temperature of from 350.degree. to 600.degree. F. to separate coke precursors, prior to recycle to the hydrogenation. Higher conversion levels can be achieved by effecting recycle in such manner..]..Iadd.Disclosed is a hydrogenation process using at least one fluidized catalytic stage and a recycle material of heavy hydrogenated effluent. The heavy effluent material is cooled to a temperature within 350.degree.-600.degree. F. to separate toluene and heptane insoluble coke precursors prior to recycle. This separation may be enhanced by the use of centrifugation, filtration or a bed of particulate material (e.g. calcined coke). .Iaddend.

5. 发明授权

US4411768A Hydrogenation of high boiling hydrocarbons 失效
标题翻译：高沸点烃的氢化
公开(公告)号：US4411768A
公开(公告)日：1983-10-25
申请号：US370416
申请日：1982-04-21
申请人： Harold Unger , Morgan C. Sze , Roger P. Van Driesen
发明人： Harold Unger , Morgan C. Sze , Roger P. Van Driesen
IPC分类号： C10G67/06 , F02B3/06 , C10G47/26 , C10G47/36
CPC分类号： C10G67/06 , F02B3/06
摘要： In a hydrogenation operation employing an ebullated catalytic bed, recycle is recovered from the hydrogenated product with at least 25%, by volume, of the recycle boiling above 950.degree. F. The recycle is cooled to a temperature of from 350.degree. to 600.degree. F. to separate coke precursors, prior to recycle to the hydrogenation. Higher conversion levels can be achieved by effecting recycle in such manner.
摘要翻译：在使用沸腾催化床的氢化操作中，从氢化产物回收至少25体积％的循环沸点高于950°F的循环。再循环冷却至350至600°F 在再循环到氢化之前分离焦炭前体。通过以这种方式进行回收可以实现更高的转化水平。

6. 发明授权

US3965194A Production of formaldehyde in carbon steel reactors 失效
标题翻译：在碳钢反应堆中生产甲醛
公开(公告)号：US3965194A
公开(公告)日：1976-06-22
申请号：US408106
申请日：1973-10-19
申请人： Morgan C. Sze , Harold Unger
发明人： Morgan C. Sze , Harold Unger
IPC分类号： C07C47/052 , B01J19/00 , B01J19/02 , C07C45/00 , C07C45/38 , C07C67/00 , C07C45/16
CPC分类号： B01J19/02 , B01J19/002 , C07C45/38 , B01J2219/0286
摘要： A carbon steel reactor can be used for producing formaldehyde from methanol by passivating the reactor with respect to formic acid production by treatment with either hydrogen sulfide in the absence of oxygen or a mixture of sulfur dioxide and oxygen.
摘要翻译：碳钢反应器可用于通过在不存在氧气或二氧化硫和氧气的混合物的情况下通过硫化氢处理而使甲酸生成相对于反应器而生成甲醛来生产甲醛。

7. 发明授权

US4208191A Production of pipeline gas from coal 失效
标题翻译：从煤炭生产管道煤气
公开(公告)号：US4208191A
公开(公告)日：1980-06-17
申请号：US910823
申请日：1978-05-30
申请人： Morgan C. Sze
发明人： Morgan C. Sze
IPC分类号： C10J3/00 , C10L3/08
CPC分类号： C10J3/00 , C10L3/08 , C10J2300/093 , C10J2300/1662
摘要： Acid gases are removed from a coal gasification gas, followed by contacting the gas with a reduced iron catalyst at conditions selected to primarily produce methane, and some olefins together with carbon dioxide as byproduct. After separation of carbon dioxide byproduct, the gas is contacted with a nickel catalyst under methanation conditions to produce additional methane and convert olefins to alkanes to thereby produce a pipeline gas having an increased heating value.
摘要翻译：从煤气化气体中除去酸性气体，然后在选择主要产生甲烷的条件下将气体与还原铁催化剂接触，一些烯烃和二氧化碳作为副产物。在分离二氧化碳副产物之后，气体在甲烷化条件下与镍催化剂接触以产生额外的甲烷并将烯烃转化为烷烃，从而产生具有增加的热值的管线气体。

8. 发明授权

US4092271A Supported vanadia catalyst for nitrile production and process for preparing the catalyst 失效
标题翻译：用于腈生产的支持的钒氧化物催化剂和用于制备催化剂的方法
公开(公告)号：US4092271A
公开(公告)日：1978-05-30
申请号：US819771
申请日：1977-07-28
申请人： Morgan C. Sze
发明人： Morgan C. Sze
IPC分类号： B01J23/22 , C07D213/84 , B01J21/04 , B01J21/08 , B01J23/04
CPC分类号： C07D213/84 , B01J23/22 , C07C253/28
摘要： Vanadia supported on a silica-alumina or gamma-alumina support in an amount to provide a vanadia to support weight ratio ranging from about 0.3:1 to about 3:1 substantially entirely within the pores of the support, the vanadia having been placed in molten form substantially within the pores of a support having a surface area greater than about 50m.sup.2 gram, a porosity greater than about 0.4 cc/gram which further includes an alkali metal, with the vanadium metal to alkali metal mole ratio being from 2:1 to 30:1. At least a portion of the alkali metal is preferably in the form of alkali metal vanadate. The catalyst is used for the production of nitriles from a compound containing at least one alkyl group.
摘要翻译： Vanadia负载在二氧化硅 - 氧化铝或γ-氧化铝载体上，其用量基本上完全在载体的孔内提供氧化钒至约0.3:1至约3:1的载体重量比，将氧化钒置于熔融基本上在表面积大于约50m 2克，孔隙率大于约0.4cc /克的支撑体的孔内形成，其还包含碱金属，其中钒金属与碱金属的摩尔比为2:1至30 ：1。至少一部分碱金属优选为碱金属钒酸盐的形式。催化剂用于从含有至少一个烷基的化合物制备腈。

9. 发明授权

US3949010A Production of chlorinated hydrocarbons 失效
标题翻译：生产氯化碳氢化合物
公开(公告)号：US3949010A
公开(公告)日：1976-04-06
申请号：US458654
申请日：1974-04-08
申请人： Morgan C. Sze
发明人： Morgan C. Sze
IPC分类号： C07C19/045 , B01J10/00 , C07C17/00 , C07C17/15 , C07C17/154 , C07C17/156 , C07C17/158 , C07C17/25 , C07C19/01 , C07C21/06 , C07C67/00 , C07C21/00
CPC分类号： B01J10/005 , C07C17/15
摘要： Oxidized molten chloride salts are employed for chlorinating and/or oxychlorinating a feed in a first reactor and then passed by gravity to a second reactor situated below the first reactor and operated at a pressure higher than the first reactor wherein the molten salt is oxidized. The oxidized salt is returned to the first reactor. Vinyl chloride or chloromethanes can be produced by the process.
摘要翻译：氧化的氯化氯盐用于在第一反应器中对进料进行氯化和/或氧氯化，然后通过重力通过位于第一反应器下方的第二反应器，并在高于熔融盐被氧化的第一反应器的压力下操作。将氧化的盐返回到第一反应器。可以通过该过程生产氯乙烯或氯甲烷。

10. 发明授权

US4342642A Steam pyrolysis of hydrocarbons 失效
标题翻译：烃的蒸汽热解
公开(公告)号：US4342642A
公开(公告)日：1982-08-03
申请号：US185153
申请日：1980-09-08
申请人： William V. Bauer , Morgan C. Sze
发明人： William V. Bauer , Morgan C. Sze
IPC分类号： C10G9/20 , F28F1/40 , F28F13/06 , C10G9/14 , B01J19/24 , C10G9/36
CPC分类号： F28F1/40 , F28F13/06 , C10G2400/20
摘要： A portion of a steam pyrolysis tubular coil, preferably the outlet portion, is provided with an insert to provide a radiation absorption surface within the tube. The insert is dimensioned to increase heat flux without adversely increasing pressure drop. A preferred insert has a central body and outwardly extending vanes in contact with the interior of the coil.
摘要翻译：蒸汽热解管状线圈的一部分，优选地为出口部分，设置有插入件以在管内提供辐射吸收表面。插入件的尺寸被设计成增加热通量而不会不利地增加压降。优选的插入件具有与线圈内部接触的中心体和向外延伸的叶片。

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