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    • 3. 发明申请
    • Method For Producing Ultra-High Purity, Optical Quality, Glass Articles
    • 生产超高纯度,光学质量,玻璃制品的方法
    • US20080203625A1
    • 2008-08-28
    • US11817230
    • 2006-02-15
    • Monika OswaldJurgen MeyerKlaus Deller
    • Monika OswaldJurgen MeyerKlaus Deller
    • C04B35/645
    • C03B19/06C03B19/066C03B32/005
    • A method for producing ultra-high purity, optical quality, glass articles is disclosed which involves: 1. compacting metaloxide or metal loidoxide to granules having a mean particle size of less than about 1 millimeter; 2. optionally fully sintering the granules to produce high purity, artificial sand; 3. casting the granulesar artificial sand by conventional techniques, such as, slip casting, to form a high density, porous, green body; 4. optionally drying and partially sintering the green body; 5. optionally fully sintering the green body under vacuum, and 6. optionally hot isostatic pressing the fully sintered green body whereby the metal oxide or metalloid oxides is a pyrogenic silicon dioxide powder with a BET surface area of 30 to 90 m2/g, a DBP index of 80 or less, a mean aggregate area of less than 25000 nm2 and a mean aggregate circumference of less than 1000 nm, wherein at least 70% of the aggregates have a circumference of less than 1300 nm or a high-purity pyrogenically prepared silicon dioxide having metal contents of less than 0.2 μg/g.
    • 公开了一种生产超高纯度,光学品质的玻璃制品的方法,其包括:1.将金属氧化物或金属氧化物压制成具有小于约1毫米的平均粒度的颗粒; 2.可选地完全烧结颗粒以产生高纯度人造砂; 3.通过常规技术如滑移浇注铸造颗粒状人造砂,形成高密度,多孔,生坯; 4.可选地干燥和部分烧结生坯; 5.可选地,在真空下完全烧结生坯,以及6.任选地热等静压压完全烧结的生坯,由此金属氧化物或准金属氧化物是BET表面积为30至90m 2 / g的致热二氧化硅粉末, DBP指数为80以下,平均聚集面积小于25000nm 2,平均聚集体周长小于1000nm,其中至少70%的聚集体具有小于1300nm的圆周或高纯度热解法制备 金属含量小于0.2mug / g的二氧化硅。