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1. 发明专利

JP2015042635A 脂肪族ジオールの製造方法有权
标题翻译：二氧化钛的生产方法
公开(公告)号：JP2015042635A
公开(公告)日：2015-03-05
申请号：JP2014150122
申请日：2014-07-23
申请人：三菱化学株式会社 , Mitsubishi Chemicals Corp
发明人： TANIGUCHI SHOHEI , IZAWA YUSUKE , UTSUNOMIYA MASARU
IPC分类号： C07C29/90 , C07C29/94 , C07C31/20
摘要：【課題】バイオマス資源由来のアセタールを含む脂肪族ジオールを工業的規模で精製して得る際に、触媒劣化の懸念が少ない、工業的に有利な脂肪族ジオールの製造方法を提供する。【解決手段】原料として、脂肪族ジオール、炭素原子数5及び/又は炭素原子数6のアルデヒド並びに下記式(I)で示されるアセタールの混合物を精製し、生成物として、脂肪族ジオールを得る脂肪族ジオールの製造方法において、該混合物中の式(I)で示されるアセタールを周期表の第8〜11族に属する金属を含む固体触媒の存在下で水素化反応を行うことにより下記式(I)ので示されるアセタールの濃度を低減する際に、該混合物に対して含窒素化合物が0.05〜20.0wtppm存在する脂肪族ジオールの製造方法。【選択図】なし
摘要翻译：要解决的问题：为了提供具有较少的催化剂降解焦虑的工业上有利的脂肪族二醇的生产方法，在工业规模上从生物质资源中纯化包含缩醛的脂肪族二醇。解决方案：在脂族二醇生产方法中获得通过纯化脂族二醇，具有5个和/或6个碳原子的醛和由式（I）表示的缩醛的混合物作为产物的脂肪族二醇，具有含氮化合物的脂族二醇与0.05〜通过式（I）表示的缩醛浓度的降低，相对于混合物为20.0重量ppm，是通过在混合物中在由含有金属的固体催化剂属于周期表第8-11组。

2. 发明专利

JP2014166990A METHOD FOR PRODUCING CARBOXYLIC ACID ANHYDRIDE AND METHOD FOR PRODUCING γ-BUTYROLACTONE 有权
标题翻译：生产羧酸酐的方法及生产γ-丁氧基酮的方法
公开(公告)号：JP2014166990A
公开(公告)日：2014-09-11
申请号：JP2014012507
申请日：2014-01-27
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： TANIGUCHI SHOHEI , KONISHI NORIKAZU , IZAWA YUSUKE , UTSUNOMIYA MASARU , IWADE SHINJI
IPC分类号： C07D307/60 , C07B61/00 , C07D307/33
摘要： PROBLEM TO BE SOLVED: To provide an industrially advantageous method for efficiently forming carboxylic acid anhydride by dehydration condensation reaction with a catalyst using carboxylic acid, and to obtain succinic anhydride at yield higher than the conventional case owing to the promoted reaction in accordance with the invention.SOLUTION: Provided is a method for producing carboxylic acid anhydride characterized in that, when carboxylic acid anhydride is formed by bringing dicarboxylic acid as raw material into dehydration condensation reaction, the dehydration condensation reaction is performed in the presence of an organic phosphor compound. It is preferable that the dicarboxylic acid as raw material being succinic acid, the carboxylic acid anhydride being succinic acid anhydride and the organic phosphorous compound being a phosphine compound.
摘要翻译：要解决的问题：为了提供通过使用羧酸与催化剂脱水缩合反应有效形成羧酸酐的工业上有利的方法，并且由于根据本发明的促进反应而获得比常规情况更高的琥珀酸酐解决方案：提供一种制备羧酸酐的方法，其特征在于当通过将二羧酸作为原料进行脱水缩合反应形成羧酸酐时，脱水缩合反应在有机荧光体化合物的存在下进行。作为原料的二羧酸为琥珀酸，羧酸酐为琥珀酸酐，有机磷化合物为膦化合物为佳。

3. 发明专利

JP2013032341A Method of producing 1,4-butanediol 有权
标题翻译：生产1,4-丁二醇的方法
公开(公告)号：JP2013032341A
公开(公告)日：2013-02-14
申请号：JP2012144393
申请日：2012-06-27
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： KONISHI NORIKAZU , IZAWA YUSUKE , UTSUNOMIYA MASARU
IPC分类号： C07C29/94 , C07C29/80 , C07C31/20
摘要： PROBLEM TO BE SOLVED: To provide an industrially advantageous method of producing 1,4-butanediol (1,4-BG) for producing stably the 1,4-BG of high quality excellent as a THF production raw material.SOLUTION: The method of producing the 1,4-butanediol is constituted to bring crude 1,4-butanediol containing 70.0 wt.% or more and less than 99.4 wt.% of 1,4-butanediol, and having 7.01 or more of pH, into contact with an acid, and to obtain refined 1,4-butanediol having 5.5 or more to 6.99 or less of pH, by distilling an obtained crude 1,4-butanediol-containing liquid.
摘要翻译：待解决的问题：提供一种用于生产1,4-丁二醇（1,4-BG）的工业上有利的方法，用于稳定地生产作为THF生产原料的高质量的1,4-BG。解决方案：制备1,4-丁二醇的方法是使含有70.0重量％以上且小于99.4重量％的1,4-丁二醇的粗1,4-丁二醇，并具有7.01或更多的pH与酸接触，通过蒸馏得到的粗1,4-丁二醇的液体，得到pH 5.5以上至6.99以下的精制1,4-丁二醇。版权所有（C）2013，JPO＆INPIT

4. 发明专利

JP2007302938A Method of separating metal 审中-公开
标题翻译：分离金属的方法
公开(公告)号：JP2007302938A
公开(公告)日：2007-11-22
申请号：JP2006132034
申请日：2006-05-10
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： IZAWA YUSUKE , UTSUNOMIYA MASARU , TAKAHASHI KAZUNARI
IPC分类号： C22B11/00 , B01J31/40 , B01J38/00 , B01J45/00 , C02F1/42 , C07B61/00 , C07C67/333 , C07C69/16 , C22B3/42
CPC分类号： Y02P10/234 , Y02P20/584
摘要： PROBLEM TO BE SOLVED: To provide a method of separating metal from solution of metal containing a trivalent phosphorus compound. SOLUTION: In the method for removing metal components from the solution of metal containing a trivalent phosphorus compound and one or more elements among ruthenium, rhodium, palladium, iridium and platinum, the solution is brought into contact with a polyamine-type chelate resin. It is preferable that the trivalent compound is a phosphorus compound containing phosphorus-oxygen bonds. Further, it is preferable to adjust the pH of the solution of metal to 5 to 10 before the solution of metal is circulated through the polyamine-type chelate resin. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供从含有三价磷化合物的金属溶液中分离金属的方法。解决方案：在从含有三价磷化合物和钌，铑，钯，铱和铂中的一种或多种元素的金属溶液中除去金属组分的方法中，使溶液与多胺型螯合物树脂。优选三价化合物是含有磷 - 氧键的磷化合物。此外，优选在金属溶液循环通过多胺型螯合树脂之前将金属溶液的pH调节至5至10。版权所有（C）2008，JPO＆INPIT

5. 发明专利

JP2014141548A Method for producing polyurethane 有权
标题翻译：生产聚氨酯的方法
公开(公告)号：JP2014141548A
公开(公告)日：2014-08-07
申请号：JP2013009446
申请日：2013-01-22
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： IZAWA YUSUKE , TANAKA KOTA , NAKAGAWA YOKO , UTSUNOMIYA MASARU , OHARA TERUHIKO
IPC分类号： C08G18/42
摘要： PROBLEM TO BE SOLVED: To improve the reaction velocity when polyester polyol is reacted with an isocyanate compound to produce polyurethane and to improve the tensile strength, elastic recovery rate or the like of the obtained polyurethane.SOLUTION: A method for producing polyurethane comprises a step of reacting the polyester polyol with the isocyanate compound in the presence of sugar and/or a derivative thereof. The present amount of the sugar and/or the derivative thereof is determined to be 0.1-80 ppm by weight of the total amount of a polyhydroxy compound in a reaction system and the sugar and/or the derivative thereof. When the polyester polyol is produced by an esterification reaction or an ester interchange reaction of dicarboxylic acid and/or a derivative thereof with a dihydroxy compound, the obtained polyester polyol contains the sugar and/or the derivative thereof since the dihydroxy compound contains the sugar and/or the derivative thereof.
摘要翻译：要解决的问题：为了提高聚酯多元醇与异氰酸酯化合物反应以产生聚氨酯并提高所得聚氨酯的拉伸强度，弹性回复率等时的反应速度。溶液：聚氨酯的制造方法包括步骤在糖和/或其衍生物的存在下使聚酯多元醇与异氰酸酯化合物反应。糖和/或其衍生物的当量被确定为反应体系中多羟基化合物的总量的0.1-80重量ppm，其糖和/或其衍生物。当通过酯化反应或二羧酸和/或其衍生物与二羟基化合物的酯交换反应制备聚酯多元醇时，所得聚酯多元醇含有糖和/或其衍生物，因为二羟基化合物含有糖和 /或其衍生物。

6. 发明专利

JP2014012663A Method for purifying furfural 有权
标题翻译：净化方法
公开(公告)号：JP2014012663A
公开(公告)日：2014-01-23
申请号：JP2013119856
申请日：2013-06-06
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： KONISHI NORIKAZU , YAMASHITA AKIRA , IZAWA YUSUKE , UTSUNOMIYA MASARU , TSUJI HIDETO
IPC分类号： C07D307/48
摘要： PROBLEM TO BE SOLVED: To provide an industrially advantageous method which, when furfural is purified, suppresses the generation of solids to stably and efficiently distill high-purity furfural from raw material furfural, and produces furan by a decarbonylation reaction of the obtained high-purity furfural.SOLUTION: In a method for purifying furfural, when raw material crude furfural is purified by distilling it to obtain furfural, the raw material crude furfural is brought into contact with an anion exchange resin and/or a basic compound beforehand.
摘要翻译：要解决的问题：提供一种工业上有利的方法，当糠醛被纯化时，抑制固体的产生以从糠醛原料中稳定高效地蒸馏出高纯度糠醛，并通过所得到的高纯度的脱羰反应产生呋喃糠醛。方法：在糠醛纯化方法中，将原料粗糠醇通过蒸馏纯化得到糠醛后，将原料粗糠醛与阴离子交换树脂和/或碱性化合物预先接触。

7. 发明专利

JP2013116881A Method for producing tetrahydrofuran 有权
标题翻译：生产四氢呋喃的方法
公开(公告)号：JP2013116881A
公开(公告)日：2013-06-13
申请号：JP2012149684
申请日：2012-07-03
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： KONISHI NORIKAZU , IZAWA YUSUKE , UTSUNOMIYA MASARU , TANAKA KOTA
IPC分类号： C07D307/08 , C07B61/00
摘要： PROBLEM TO BE SOLVED: To produce tetrahydrofuran stably at high productivity by preventing a solid material from being deposited during a cyclodehydration reaction when the tetrahydrofuran is produced through the cyclodehydration reaction of 1,4-butanediol by using an acid catalyst having a pKa value of no greater than 4.SOLUTION: The present invention is a method for producing tetrahydrofuran by means of a cyclodehydration reaction of 1,4-butanediol in the presence of an acid catalyst having a pKa value of no greater than 4 in a reaction vessel, wherein a starting material liquid containing 1,4-butanediol made available to the reaction contains 0.01-0.35 wt.% of 2-(4-hydroxybutoxy)-tetrahydrofuran and 1-1,000 wt.ppm inclusive by concentration of nitrogen atoms of at least either of an amine and amide.
摘要翻译：待解决的问题：通过使用具有pKa的酸催化剂通过1,4-丁二醇的环化脱水反应制备四氢呋喃时，通过防止在环化脱水反应期间固体材料沉积来以高生产率稳定地生产四氢呋喃值不大于4.解决方案：本发明是通过1,4-丁二醇在pKa值不大于4的酸催化剂存在下，通过1,4-丁二醇的环化脱水反应生产四氢呋喃的方法反应容器，其中含有可用于该反应的1,4-丁二醇的原料液体含有0.01-0.35重量％的2-（4-羟基丁氧基）四氢呋喃和1-1000重量ppm的含氮浓度的氮原子的胺和酰胺中的至少一种。版权所有（C）2013，JPO＆INPIT

8. 发明专利

JP2010184877A Method for producing carbonyl compound 审中-公开
标题翻译：生产碳化合物的方法
公开(公告)号：JP2010184877A
公开(公告)日：2010-08-26
申请号：JP2009028721
申请日：2009-02-10
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： IZAWA YUSUKE , UTSUNOMIYA MASARU
IPC分类号： C07D307/33 , C07B61/00
摘要： PROBLEM TO BE SOLVED: To suppress formation of a high-boiling compound and to efficiently produce a carbonyl compound or gamma-butyrolactone in a high yield in producing a carbonyl compound by a dehydrogenation reaction of a raw material alcohol, in more detail, in producing gamma-butyrolactone by a dehydrogenation reaction of 1,4-butanediol.
SOLUTION: In the method for producing the carbonyl compound by dehydrogenation reaction of the raw material alcohol in the presence of a catalyst, an oligomer is made to exist in a reaction system at the beginning of the reaction.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：为了抑制高沸点化合物的形成，并且通过原料醇的脱氢反应来生产羰基化合物，以高产率有效地制备羰基化合物或γ-丁内酯，更详细地说，通过1,4-丁二醇的脱氢反应制备γ-丁内酯。解决方案：在催化剂存在下，通过原料醇的脱氢反应生产羰基化合物的方法中，在反应开始时使反应体系中存在低聚物。版权所有（C）2010，JPO＆INPIT

9. 发明专利

JP2009023928A Method for producing unsaturated alcohol 审中-公开
标题翻译：生产不饱和醇的方法
公开(公告)号：JP2009023928A
公开(公告)日：2009-02-05
申请号：JP2007187522
申请日：2007-07-18
申请人： Chiba Univ , Mitsubishi Chemicals Corp , 三菱化学株式会社 , 国立大学法人千葉大学
发明人： IZAWA YUSUKE , TAKAHASHI KAZUNARI , SATO TOMOJI , KOFUNE MIKA
IPC分类号： C07C29/60 , B01J23/10 , C07B61/00 , C07C33/025
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method for efficiently producing an unsaturated alcohol by a dehydration reaction of an alcohol by suppressing the formation of byproducts. SOLUTION: Provided is a method for producing an unsaturated alcohol from a raw material alcohol by the dehydration reaction in the presence of a catalyst, which comprises an oxide of at least one kind of yttrium group rare earth metals selected from the group consisting of holmium, yttrium, erbium, thulium and lutetium, and has been prepared through firing at 800-1,500°C. COPYRIGHT: (C)2009,JPO&INPIT

10. 发明专利

JP2007039400A Method for producing allyl compound 审中-公开
标题翻译：生产全合成化合物的方法
公开(公告)号：JP2007039400A
公开(公告)日：2007-02-15
申请号：JP2005227246
申请日：2005-08-04
申请人： Mitsubishi Chemicals Corp , 三菱化学株式会社
发明人： IZAWA YUSUKE , UTSUNOMIYA MASARU , TAKAHASHI KAZUNARI
IPC分类号： C07C67/333 , C07B61/00 , C07C29/09 , C07C31/20 , C07C69/16
摘要： PROBLEM TO BE SOLVED: To provide an industrially advantageous isomerization method of a diacetoxyallyl compound by which the isomerization of the diacetoxyallyl compound can be carried out with a smaller amount of a used catalyst.
SOLUTION: The method for producing the allyl compound represented by general formula (b) comprises isomerizing a raw material allyl compound represented by general formula (a) in the presence of a catalyst comprising a group 8-10 transition metal compound and a phosphite ligand, phosphines and tertiary amines. [In the formula (a), R
a to R
e are each independently selected from the group consisting of a hydrogen atom, an alkyl group, an aryl group, an alkoxy group, an aryloxy group, an acyl group, an acyloxy group, a hydroxy group, an amino group, an alkylthio group and an arylthio group; and X is an electron-attracting group]. [In the general formula (b), R
a to R
e , and X are the same as the R
a to the R
e , and the X in the general formula (a)].
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供一种工业上有利的二烯氧基甲酰基化合物的异构化方法，通过该方法可以用较少量的使用的催化剂进行二乙烯氧基甲基化合物的异构化。解决方案：由通式（b）表示的烯丙基化合物的制备方法包括：在包含8-10族过渡金属化合物的催化剂存在下使由通式（a）表示的原料烯丙基化合物异构化，亚磷酸酯配体，膦和叔胺。 [式（a）中，R a 至R e 各自独立地选自氢原子，烷基，芳基，烷氧基基团，芳氧基，酰基，酰氧基，羟基，氨基，烷硫基和芳硫基; X是吸电子基团]。在通式（b）中，R a 至R e ，X与R R a 相同 > e ，通式（a）中的X）。版权所有（C）2007，JPO＆INPIT

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