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1. 发明申请

US20130018214A1 CATALYST COMPOSITION FOR OLIGOMERIZATION OF ETHYLENE AND PROCESSES OF OLIGOMERIZATION 审中-公开
标题翻译：乙烯低聚化催化剂组合物及其低分子化方法
公开(公告)号：US20130018214A1
公开(公告)日：2013-01-17
申请号：US13637976
申请日：2011-03-30
申请人： Mingfang Zheng , Weizhen Li , Huaijie Wang , Jun Liu , Haiying Zhang , Yu Zhou , Tonglin Li , Lan Zhao , Jilong Wang , Hongfei Wu , Yuling Piao , Junlong Sui
发明人： Mingfang Zheng , Weizhen Li , Huaijie Wang , Jun Liu , Haiying Zhang , Yu Zhou , Tonglin Li , Lan Zhao , Jilong Wang , Hongfei Wu , Yuling Piao , Junlong Sui
IPC分类号： B01J31/12 , C07C2/26
CPC分类号： C08F10/02 , B01J31/143 , B01J31/183 , B01J2231/20 , B01J2531/842 , B01J2531/845 , B01J2531/847 , C07C2/32 , C07C2531/14 , C07C2531/22 , C08F110/02 , Y02P20/52 , C08F4/7042 , C08F2500/02 , C07C11/02 , C08F210/02
摘要： The present invention provides a catalyst composition for the ethylene oligomerization, which comprises 2-imino-1,10-phenanthroline coordinated iron (II), cobalt (II) or nickel (II) chloride as main catalyst and triethylaluminum as cocatalyst. The present invention also provides a process for oligomerization of ethylene is provided, wherein a catalyst composition comprising 2-imino-1,10-phenanthroline coordinated iron (II), cobalt (II) or nickel (II) chloride as main catalyst and triethylaluminum as cocatalyst is used, and the molar ratio of aluminum in the cocatalyst to central metal in the main catalyst ranges from 30 to less than 200. According to the present invention, another process for oligomerization of ethylene is also provided, wherein a catalyst composition comprising 2-imino-1,10-phenanthroline coordinated iron (II), cobalt (II) or nickel (II) chloride as main catalyst and triethylaluminum as cocatalyst is used, and the temperature of ethylene oligomerization ranges from −10 to 19° C. According to the present invention, the price of cocatalyst i.e. triethylaluminum, is low, just a fraction of that of methylaluminoxane, the amount of cocatalyst is therefore significantly reduced, with the catalytic activity is still acceptable, thus the cost of ethylene oligomerization is significantly reduced. In view of both the catalytic activity and the cost, the present invention is highly applicable in industry.
摘要翻译：本发明提供了一种用于乙烯低聚的催化剂组合物，其包含2-亚氨基-1,10-菲咯啉配位的铁（II），钴（II）或氯化镍（II）作为主要催化剂，三乙基铝作为助催化剂。本发明还提供了一种乙烯低聚方法，其中包含2-亚氨基-1,10-菲咯啉配位的铁（II），钴（II）或氯化镍（II）作为主要催化剂的催化剂组合物和三乙基铝作为助催化剂，主催化剂中助催化剂与中心金属之间的铝的摩尔比为30至小于200.根据本发明，还提供了另一种乙烯低聚方法，其中催化剂组合物包含2 - 亚氨基-1,10-菲咯啉配位的铁（II），钴（II）或氯化镍（II）为主催化剂，三乙基铝为助催化剂，乙烯齐聚温度为-10〜19℃。对于本发明，助催化剂即三乙基铝的价格低，仅仅是甲基铝氧烷的一部分，因此助催化剂的量显着降低，催化活性为仍然是可接受的，因此乙烯低聚的成本显着降低。鉴于催化活性和成本两方面，本发明在工业上是高度适用的。

2. 发明授权

US09266982B2 N ortho acyl substituted nitrogen-containing heterocyclic compound and process for preparing aminal iron (II) complexes thereof 有权
标题翻译： N邻酰基取代的含氮杂环化合物及其制备其中的二胺铁（II）配合物的方法
公开(公告)号：US09266982B2
公开(公告)日：2016-02-23
申请号：US13991044
申请日：2011-12-01
申请人： Jun Liu , Mingfang Zheng , Weizhen Li , Haiying Zhang , Huaijie Wang , Yu Zhou , Tonglin Li , Lan Zhao , Hongfei Wu , Mingjun Xie , Chunhong Wu , Zhiguang Jia , Yanping Qi , Jilong Wang
发明人： Jun Liu , Mingfang Zheng , Weizhen Li , Haiying Zhang , Huaijie Wang , Yu Zhou , Tonglin Li , Lan Zhao , Hongfei Wu , Mingjun Xie , Chunhong Wu , Zhiguang Jia , Yanping Qi , Jilong Wang
IPC分类号： C07D471/04 , C07D211/70 , C07D211/82 , C07D213/46 , C08F110/02 , B01J31/18 , C07C2/32 , C07D213/127 , C07F15/02
CPC分类号： C08F110/02 , B01J31/183 , B01J2231/20 , B01J2531/0241 , B01J2531/842 , C07C2/32 , C07D213/127 , C07D471/04 , C07F15/025 , C07C11/02
摘要： Provided are a process for preparing an N ortho acyl substituted nitrogen-containing heterocyclic compound and an aminal iron (II) complex thereof, and the use of the complexes obtained by the process in an olefin oligomerization catalyst. The N ortho acyl substituted nitrogen-containing heterocyclic compound in the present invention is for example 2-acyl-1,10-phenanthroline or 2,6-diacetyl pyridine as shown in formula b, and the N ortho acyl substituted nitrogen-containing heterocyclic compound in the present invention is produced by a reaction of a precursor thereof in a substituted or unsubstituted nitrobenzene. Preferably the precursor shown in formula I in the present invention is produced by 1,10-phenanthroline reacting with trialkyl aluminum, or a halogenoalkyl aluminum RnAIXm, or a substituted or unsubstituted benzyl lithium Ph′CH2Li, followed by hydrolysis. The preparation method provided in the present invention has a few synthetic steps, an easy process, a low toxic effect, and reduces the preparation costs of the catalyst, and has a promising outlook in the industrial application.
摘要翻译：提供了制备N-邻酰基取代的含氮杂环化合物和其亚胺铁（II）络合物的方法，以及通过该方法在烯烃低聚催化剂中获得的络合物的用途。本发明中的N-邻酰基取代的含氮杂环化合物例如如式b所示的2-酰基-1,10-菲咯啉或2,6-二乙酰基吡啶，并且N-邻酰基取代的含氮杂环化合物在本发明中通过其前体在取代或未取代的硝基苯中的反应来制备。优选地，本发明中式I所示的前体是通过与三烷基铝或卤代烷基铝RnAIXm或取代或未取代的苄基锂Ph'CH2Li反应的1,10-菲咯啉然后水解制备的。本发明提供的制备方法具有几个合成步骤，易操作，低毒性，降低催化剂的制备成本，在工业应用前景看好。

3. 发明申请

US20130267708A1 N ORTHO ACYL SUBSTITUTED NITROGEN-CONTAINING HETEROCYCLIC COMPOUND AND PROCESS FOR PREPARING AMINAL IRON (II) COMPLEXES THEREOF 有权
标题翻译： N ORTHO ACYL取代的含氮杂环化合物及其制备方法（II）其复合物
公开(公告)号：US20130267708A1
公开(公告)日：2013-10-10
申请号：US13991044
申请日：2011-12-01
申请人： Jun Liu , Mingfang Zheng , Weizhen Li , Haiying Zhang , Huaijie Wang , Yu Zhou , Tonglin Li , Lan Zhao , Hongfei Wu , Wingjun Xie , Chunhong Wu , Zhiguang Jia , Qi Yanping , Jilong Wang
发明人： Jun Liu , Mingfang Zheng , Weizhen Li , Haiying Zhang , Huaijie Wang , Yu Zhou , Tonglin Li , Lan Zhao , Hongfei Wu , Wingjun Xie , Chunhong Wu , Zhiguang Jia , Qi Yanping , Jilong Wang
IPC分类号： C08F110/02
CPC分类号： C08F110/02 , B01J31/183 , B01J2231/20 , B01J2531/0241 , B01J2531/842 , C07C2/32 , C07D213/127 , C07D471/04 , C07F15/025 , C07C11/02
摘要： Provided are a process for preparing an N ortho acyl substituted nitrogen-containing heterocyclic compound and an aminal iron (II) complex thereof, and the use of the complexes obtained by the process in an olefin oligomerization catalyst. The N ortho acyl substituted nitrogen-containing heterocyclic compound in the present invention is for example 2-acyl-1,10-phenanthroline or 2,6-diacetyl pyridine as shown in formula b, and the N ortho acyl substituted nitrogen-containing heterocyclic compound in the present invention is produced by a reaction of a precursor thereof in a substituted or unsubstituted nitrobenzene. Preferably the precursor shown in formula I in the present invention is produced by 1,10-phenanthroline reacting with trialkyl aluminum, or a halogenoalkyl aluminum RnAlXm, or a substituted or unsubstituted benzyl lithium 2Li, followed by hydrolysis. The preparation method provided in the present invention has a few synthetic steps, an easy process, a low toxic effect, and reduces the preparation costs of the catalyst, and has a promising outlook in the industrial application.
摘要翻译：提供了制备N-邻酰基取代的含氮杂环化合物和其亚胺铁（II）络合物的方法，以及通过该方法在烯烃低聚催化剂中获得的络合物的用途。本发明中的N-邻酰基取代的含氮杂环化合物例如如式b所示的2-酰基-1,10-菲咯啉或2,6-二乙酰基吡啶，并且N-邻酰基取代的含氮杂环化合物在本发明中通过其前体在取代或未取代的硝基苯中的反应来制备。优选地，本发明中式I所示的前体是通过与三烷基铝或卤代烷基铝RnAlXm或取代或未取代的苄基锂2Li反应的1,10-菲咯啉然后水解制备的。本发明提供的制备方法具有几个合成步骤，易操作，低毒性，降低催化剂的制备成本，在工业应用前景看好。

4. 发明授权

US09290801B2 Detection method of micro-RNA with high specificity 有权
标题翻译：具有高特异性的微RNA检测方法
公开(公告)号：US09290801B2
公开(公告)日：2016-03-22
申请号：US14001267
申请日：2011-12-08
申请人： Hongfei Wu , Honghoi Ting , Zuxun Gong , Ruoying Tan
发明人： Hongfei Wu , Honghoi Ting , Zuxun Gong , Ruoying Tan
IPC分类号： C12Q1/68
CPC分类号： C12Q1/686 , C12Q1/6848 , C12Q1/6851 , C12Q2561/113 , C12Q2563/173 , C12Q2525/173 , C12Q2525/207 , C12Q2531/113
摘要： The invention provides a method for detecting miRNA based on polymerase chain reaction comprising EvaGreen dye, and the use of EvaGreen dye in elevating the binding specificity of primers to templates in PCR.
摘要翻译：本发明提供了一种基于包含EvaGreen染料的聚合酶链反应检测miRNA的方法，以及使用EvaGreen染料提高引物对PCR中模板的结合特异性。

5. 发明授权

US08455532B2 Pyrazolyl acrylonitrile compounds and uses thereof 有权
标题翻译：吡唑基丙烯腈化合物及其用途
公开(公告)号：US08455532B2
公开(公告)日：2013-06-04
申请号：US13265010
申请日：2010-04-27
申请人： Bin Li , Haibo Yu , Hong Zhang , Yan Cheng , Yanmei Luo , Lizeng Wang , Hongfei Wu , Man Xu
发明人： Bin Li , Haibo Yu , Hong Zhang , Yan Cheng , Yanmei Luo , Lizeng Wang , Hongfei Wu , Man Xu
IPC分类号： A01N43/56 , C07D231/12
CPC分类号： C07D231/12 , A01N43/56 , A01N53/00 , C07D231/14 , C07D231/16
摘要： A kind of pyrazolyl acrylniitrile compounds represented by the structures of formula I or stereoisomers thereof are disclosed in the present invention. Where in: R1 is selected from the group of substituents consisting of H, C1-C4 alkoxy C1-C2 alkyl, C3-C5 alkenyloxy C1-C2 alkyl, C3-C5 alknyloxy C1-C2 alkyl, C1-C4 alkylthio C1-C2 alkyl, C1-C5 alkyl carbonyl, C3-C8 cycloalkyl carbonyl, C1-C5 alkoxy carbonyl or C1-C5 alkylthio carbonyl; R2 is Cl or methyl; R3 is H, methyl, CN, NO2 or halogen. Or its stereoisomers.The Formula I compounds have high insecticidal activities or acaricidal activities, so they can be used as insecticide or acaricide.
摘要翻译：在本发明中公开了一种由式I结构或其立体异构体表示的吡唑基丙烯腈化合物。其中：R1选自H，C1-C4烷氧基C1-C2烷基，C3-C5烯氧基C1-C2烷基，C3-C5烷氧基C1-C2烷基，C1-C4烷硫基C1-C2烷基，C 1 -C 5烷基羰基，C 3 -C 8环烷基羰基，C 1 -C 5烷氧基羰基或C 1 -C 5烷硫基羰基; R2是Cl或甲基; R3是H，甲基，CN，NO2或卤素。或其立体异构体。式I化合物具有高杀虫活性或杀螨活性，因此可用作杀虫剂或杀螨剂。

6. 发明授权

US08217179B2 Preparation method of phenylcarboxamides 有权
标题翻译：苯甲酰胺的制备方法
公开(公告)号：US08217179B2
公开(公告)日：2012-07-10
申请号：US12918133
申请日：2009-03-30
申请人： Bin Li , Hongfei Wu , Haibo Yu , Huibin Yang
发明人： Bin Li , Hongfei Wu , Haibo Yu , Huibin Yang
IPC分类号： C07D401/04
CPC分类号： C07D401/04
摘要： A preparation method of phenylcarboxamides of formula (I), the reaction scheme of which is as follows: wherein the groups are defined in the description. In this method, 3-halo-1-(3-chloro-2-pyridinyl)-4,5-dihydro-1H-pyrazole-5-carboxylic acid esters (V) as the raw materials are hydrolyzed to obtain carboxylic acids of formula (IV) under a basic condition, and carboxylic acids (IV) are simultaneously acyl halogenated and oxidated to get acyl halide of formula (III), and then without the presence of a acid binging agent, acyl chlorides (III) are reacted with substituted anilines (II) to get phenylcarboxamides of formula (I) in high yield.
摘要翻译：式（I）的苯甲酰胺的制备方法，其反应方案如下：其中这些基团在说明书中定义。在该方法中，将作为原料的3-卤代-1-（3-氯-2-吡啶基）-4,5-二氢-1H-吡唑-5-羧酸酯（V）水解，得到式（Ⅳ），羧酸（Ⅳ）同时进行酰基卤化和氧化，得到式（Ⅳ）的酰卤，然后不存在酸性起始剂，酰基氯（III）与取代的苯胺（II）以高产率得到式（I）的苯基甲酰胺。

7. 发明申请

US20120035236A1 Pyrazolyl Acrylonitrile Compounds and Uses Thereof 有权
标题翻译：吡唑基丙烯腈化合物及其用途
公开(公告)号：US20120035236A1
公开(公告)日：2012-02-09
申请号：US13265010
申请日：2010-04-27
申请人： Bin Li , Haibo Yu , Hong Zhang , Yan Cheng , Yanmie Luo , Lizeng Wang , Hongfei Wu , Man Xu
发明人： Bin Li , Haibo Yu , Hong Zhang , Yan Cheng , Yanmie Luo , Lizeng Wang , Hongfei Wu , Man Xu
IPC分类号： A01N43/56 , A01P7/04 , A01P7/02 , C07D231/12 , C07D231/16
CPC分类号： C07D231/12 , A01N43/56 , A01N53/00 , C07D231/14 , C07D231/16
摘要： A kind of pyrazolyl acrylniitrile compounds represented by the structures of formula I or stereoisomers thereof are disclosed in the present invention. Where in: R1 is selected from the group of substituents consisting of H, C1-C4 alkoxy C1-C2 alkyl, C3-C5 alkenyloxy C1-C2 alkyl, C3-C5 alknyloxy C1-C2 alkyl, C1-C4 alkylthio C1-C2 alkyl, C1-C5 alkyl carbonyl, C3-C8 cycloalkyl carbonyl, C1-C5 alkoxy carbonyl or C1-C5 alkylthio carbonyl; R2 is Cl or methyl; R3 is H, methyl, CN, NO2 or halogen. Or its stereoisomers. The Formula I compounds have high insecticidal activities or acaricidal activities, so they can be used as insecticide or acaricide.
摘要翻译：在本发明中公开了一种由式I结构或其立体异构体表示的吡唑基丙烯腈化合物。其中：R1选自H，C1-C4烷氧基C1-C2烷基，C3-C5烯氧基C1-C2烷基，C3-C5烷氧基C1-C2烷基，C1-C4烷硫基C1-C2烷基，C 1 -C 5烷基羰基，C 3 -C 8环烷基羰基，C 1 -C 5烷氧基羰基或C 1 -C 5烷硫基羰基; R2是Cl或甲基; R3是H，甲基，CN，NO2或卤素。或其立体异构体。式I化合物具有高杀虫活性或杀螨活性，因此可用作杀虫剂或杀螨剂。

8. 发明申请

US20090179670A1 PERFORMANCE INVERSION DETECTION CIRCUIT AND A DESIGN STRUCTURE FOR THE SAME 审中-公开
标题翻译：性能反相检测电路及其设计结构
公开(公告)号：US20090179670A1
公开(公告)日：2009-07-16
申请号：US12014430
申请日：2008-01-15
申请人： Albert M. Chu , John A. Fifield , Daryl M. Seitzer , Hongfei Wu
发明人： Albert M. Chu , John A. Fifield , Daryl M. Seitzer , Hongfei Wu
IPC分类号： H03F3/45
CPC分类号： H03F3/45475 , H03F2200/447 , H03F2203/45586 , H03F2203/45618 , H03F2203/45622
摘要： A circuit containing a parallel connection of a first sub-circuit and a second sub-circuit is provided. The first sub-circuit comprises a serial connection of a first field effect transistor having a first threshold voltage and a first voltage dividing device. The second sub-circuit comprises a serial connection of a second field effect transistor having a second threshold voltage, which is different from the first threshold voltage, and a second voltage dividing device. The voltage between the first field effect transistor and the first voltage dividing device is compared with the voltage between the second field effect transistor and the second voltage dividing device so that a signal may be generated at a temperature at which the ratio of a performance parameter such as on-current between the first and second field effect transistors crosses over a predefined value. The signal may be advantageously employed to actively control circuit characteristics.
摘要翻译：提供了包含第一子电路和第二子电路的并联连接的电路。第一子电路包括具有第一阈值电压的第一场效应晶体管和第一分压装置的串联连接。第二子电路包括具有与第一阈值电压不同的第二阈值电压的第二场效应晶体管的串联连接和第二分压装置。将第一场效应晶体管和第一分压装置之间的电压与第二场效应晶体管和第二分压装置之间的电压进行比较，使得可以在这样的温度下产生信号，因为第一和第二场效应晶体管之间的导通电流跨越预定值。可以有利地使用该信号来主动地控制电路特性。

9. 发明授权

US06545521B2 Low skew, power sequence independent CMOS receiver device 失效
标题翻译：低偏移，电源顺序独立的CMOS接收器件
公开(公告)号：US06545521B2
公开(公告)日：2003-04-08
申请号：US09895778
申请日：2001-06-29
申请人： Bret R. Dale , Joseph A. Iadanza , Douglas W. Stout , Sebastian T. Ventrone , Hongfei Wu
发明人： Bret R. Dale , Joseph A. Iadanza , Douglas W. Stout , Sebastian T. Ventrone , Hongfei Wu
IPC分类号： H03L500
CPC分类号： H04L25/0292 , H03K19/00315 , H04L25/0266 , H04L25/0272
摘要： The present invention provides a receiver device having multiple voltage supplies that allows the output stage of the receiver device to go to a safe state whenever its voltage is disconnected or powered-down, independent of any of its normal control circuits. Furthermore, the isolation of the multiple voltage supplies provides a low skew at the output of the receiver device.
摘要翻译：本发明提供了一种具有多个电压源的接收机设备，每当其电压断开或掉电时，接收机设备的输出级都能够进入安全状态，独立于其任何正常的控制电路。此外，多个电压源的隔离在接收器件的输出处提供低偏移。

10. 发明申请

US20070159225A1 STROBE RECEIVER WITH DIGITAL HIGH-HIGH PROTECT 失效
标题翻译：具有数字高保护功能的接收器
公开(公告)号：US20070159225A1
公开(公告)日：2007-07-12
申请号：US11275537
申请日：2006-01-12
申请人： William Bucossi , Hongfei Wu
发明人： William Bucossi , Hongfei Wu
IPC分类号： G06F1/04
CPC分类号： G06F1/04
摘要： A digital clock generation circuit (and a method for operating the same). The digital clock generation circuit includes a first, a second, a third differential comparator circuits. The first differential comparator circuit receives the positive differential clock signal and a reference voltage, and generates a first output signal. The second differential comparator circuit receives the positive and negative differential clock signal, and generates a second output signal. The third differential comparator circuit receives the reference voltage and the negative differential clock signal, and generates a third output signal. A high-high detecting circuit receives the first output signal, and the third output signal, and generates an Enable signal. The digital clock generation circuit further includes a latch circuit which receives the second output signal, and the Enable signal and generates a digital clock signal. The latch circuit comprises a latch with glitch or noise immunity.
摘要翻译：数字时钟产生电路（及其操作方法）。数字时钟产生电路包括第一，第二，第三差分比较器电路。第一差分比较器电路接收正差分时钟信号和参考电压，并产生第一输出信号。第二差分比较器电路接收正和负差分时钟信号，并产生第二输出信号。第三差分比较器电路接收参考电压和负差分时钟信号，并产生第三输出信号。高电平检测电路接收第一输出信号和第三输出信号，并产生使能信号。数字时钟发生电路还包括接收第二输出信号的锁存电路和使能信号并产生数字时钟信号。锁存电路包括具有毛刺或抗噪声的锁存器。

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