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1. 发明授权

US06214173B1 On-site manufacture of ultra-high-purity nitric acid 失效
标题翻译：现场制造超高纯度硝酸
公开(公告)号：US06214173B1
公开(公告)日：2001-04-10
申请号：US08759213
申请日：1996-12-05
申请人： Mindi Xu , Wallace I. Yuan , Tracey Jacksier , Hwa-Chi Wang , Joe G. Hoffman , R. Scot Clark
发明人： Mindi Xu , Wallace I. Yuan , Tracey Jacksier , Hwa-Chi Wang , Joe G. Hoffman , R. Scot Clark
IPC分类号： B01D300
CPC分类号： C01B21/46 , B01D3/143 , B01D3/34
摘要： Provided is a novel on-site system and method for providing ultra-high-purity nitric acid to a point of use. The system includes a source of nitric acid at a concentration greater than 68 wt %; a reflux distillation column having an inlet in communication with the nitric acid source for introducing nitric acid into the column, a reboiler, and a condensate outlet to provide a flow of nitric acid condensate from the column; a reservoir in communication with the condensate outlet for receiving the flow of nitric acid condensate; and piping for delivering nitric acid from the reservoir to a point of use. The system and method can be used as an on-site subsystem, in a semiconductor device fabrication facility for supplying the nitric acid condensate to points of use in the semiconductor device fabrication facility.
摘要翻译：提供了一种用于在使用点提供超高纯度硝酸的新型现场系统和方法。该系统包括浓度大于68重量％的硝酸源; 回流蒸馏塔，其具有与硝酸源连通以将硝酸引入塔中的入口，再沸器和冷凝物出口，以从塔中提供硝酸冷凝物流; 与冷凝水出口连通的用于接收硝酸冷凝物流的储存器; 以及用于将硝酸从储存器输送到使用点的管道。该系统和方法可以用作半导体器件制造设备中的现场子系统，用于将硝酸冷凝物供应到半导体器件制造设备中的使用点。

2. 发明申请

US20110100088A1 Articles Of Manufacture Containing Increased Stability Low Concentration Gases And Methods Of Making And Using The Same 有权
标题翻译：含有增加稳定性的低浓度气体制造物品及其制造和使用方法
公开(公告)号：US20110100088A1
公开(公告)日：2011-05-05
申请号：US12912289
申请日：2010-10-26
申请人： Robert Benesch , Malik Haouchine , Tracey Jacksier
发明人： Robert Benesch , Malik Haouchine , Tracey Jacksier
IPC分类号： G01N33/00
CPC分类号： C23C16/045 , F17C1/10 , F17C3/12 , Y10T436/100833 , Y10T436/156666 , Y10T436/18 , Y10T436/182 , Y10T436/184 , Y10T436/186 , Y10T436/188
摘要： Articles of manufacture and methods of making and using same concern a container having an internal space and a passivated internal metal surface. The container contains a composition of an acid gas and a balance gas contained within the internal space and in contact with the passivated internal metal surface. The stability of the acid gas concentration over time is enhanced.
摘要翻译：制造方法和制造和使用方法涉及具有内部空间和钝化的内部金属表面的容器。容器包含酸性气体和平衡气体的组成，该组合物包含在内部空间内并与钝化的内部金属表面接触。随着时间的推移，酸性气体浓度的稳定性得到提高。

3. 发明授权

US07850790B2 Reactive gases with concentrations of increased stability and processes for manufacturing same 有权
标题翻译：活性气体的浓度增加，稳定性和制造方法相同
公开(公告)号：US07850790B2
公开(公告)日：2010-12-14
申请号：US12416556
申请日：2009-04-01
申请人： Tracey Jacksier , Robert Benesch , Malik Haouchine
发明人： Tracey Jacksier , Robert Benesch , Malik Haouchine
IPC分类号： C23C16/00 , B65D85/00
CPC分类号： C23C16/045 , B08B9/22 , B08B9/28 , B08B2203/005 , C23C16/402 , C23G5/00 , F17C1/10 , F17C3/12 , F17C2201/0104 , F17C2201/0128 , F17C2201/052 , F17C2203/0604 , F17C2203/0636 , F17C2203/0639 , F17C2203/0643 , F17C2203/0646 , F17C2203/0648 , F17C2205/0323 , F17C2209/2172 , F17C2209/232 , F17C2221/037 , F17C2223/0123 , F17C2223/013 , F17C2223/0146 , F17C2223/0153 , F17C2260/053
摘要： Methods of passivating a metal surface are described, the methods comprising the steps of exposing the metal surface to a silicon-containing passivation material, evacuating the metal surface, exposing the treated surface to a gas composition, having a concentration of reactive gas that is greater than an intended reactive gas concentration of gas to be transported by the metal surface, evacuating the metal surface to remove substantially all of the gas composition to enable maintenance of an increased shelf-life, low concentration reactive gas at an intended concentration, and exposing the metal surface to the reactive gas at the intended reactive gas concentration. Manufactured products, high stability fluids, and methods of making same are also described.
摘要翻译：描述了钝化金属表面的方法，所述方法包括以下步骤：将金属表面暴露于含硅钝化材料，抽空金属表面，将经处理的表面暴露于气体组合物，反应气体的浓度较大比通过金属表面输送的气体的预期反应气体浓度，抽真空金属表面以去除基本上所有的气体组合物，以便维持预期浓度的增加的保质期低浓度反应气体，并使金属表面以反应气体的浓度反应。还描述了制造产品，高稳定性流体及其制备方法。

4. 发明授权

US06468446B1 Generation of metal-carbonyl standards for the calibration of spectroscopic systems 失效
标题翻译：生成用于校准光谱系统的金属 - 羰基标准品
公开(公告)号：US06468446B1
公开(公告)日：2002-10-22
申请号：US09657395
申请日：2000-09-08
申请人： Tracey Jacksier , Reha Tepe , David N. Vassallo
发明人： Tracey Jacksier , Reha Tepe , David N. Vassallo
IPC分类号： C09K300
CPC分类号： C01G49/16 , C01G1/04 , C01G53/02 , G01N21/278
摘要： Methods and apparatus for preparing gaseous compositions comprising a metal carbonyl, preferably at ppm concentration, are disclosed. The methods comprise placing metal, preferably in the form of filings, of the metal carbonyl to be produced into a first test vessel at a first temperature, and then pressurizing the first test vessel with a gas comprising carbon monoxide from a carbon monoxide source vessel. The contents of the first vessel are then heated to a second temperature and at a rate sufficient to initiate metal carbonyl formation, thereby forming a gas composition comprising a metal carbonyl. The reaction is then quenched by transferring some of the gas composition comprising a metal carbonyl from the first test vessel to a second test vessel which is at a third temperature, the third temperature being lower than the second temperature. Finally, the gas composition is diluted in the second test vessel with an inert gas (preferably argon) from an inert gas source container.
摘要翻译：公开了用于制备包含金属羰基，优选以ppm浓度的气态组合物的方法和设备。所述方法包括将待生产的金属羰基的金属（优选以填料形式）置于第一温度下的第一试验容器中，然后用包含一氧化碳源容器的一氧化碳的气体对第一试验容器加压。然后将第一容器的内容物加热到第二温度并以足以引发金属羰基生成的速率，从而形成包含羰基金属的气体组合物。然后通过将一些包含金属羰基的气体组合物从第一测试容器转移到处于第三温度，第三温度低于第二温度的第二测试容器来淬灭反应。最后，将惰性气体（优选氩气）从惰性气体源容器中稀释到第二测试容器中。

5. 发明授权

US07837806B2 Articles of manufacture containing increased stability low concentration gases and methods of making and using the same 有权
公开(公告)号：US07837806B2
公开(公告)日：2010-11-23
申请号：US12352925
申请日：2009-01-13
申请人： Robert Benesch , Malik Haouchine , Tracey Jacksier
发明人： Robert Benesch , Malik Haouchine , Tracey Jacksier
IPC分类号： C23C16/00 , B65D85/00
CPC分类号： C23C16/045 , F17C1/10 , F17C3/12 , Y10T436/100833 , Y10T436/156666 , Y10T436/18 , Y10T436/182 , Y10T436/184 , Y10T436/186 , Y10T436/188
摘要： Articles of manufacture and methods of making and using same concern a container having an internal space and a passivated internal metal surface. The container contains a composition of an acid gas and a balance gas contained within the internal space and in contact with the passivated internal metal surface. The stability of the acid gas concentration over time is enhanced.

6. 发明授权

US06992282B2 Use of a nebulizer to add gas to eliminate metal deposition on the sampling orifices of an inductively coupled plasma mass spectrometer 失效
标题翻译：使用雾化器添加气体以消除电感耦合等离子体质谱仪的采样孔上的金属沉积
公开(公告)号：US06992282B2
公开(公告)日：2006-01-31
申请号：US10242954
申请日：2002-09-13
申请人： Tracey Jacksier , Janet Graehling , Farouk Kimour
发明人： Tracey Jacksier , Janet Graehling , Farouk Kimour
IPC分类号： B05D5/03 , H01J49/26 , B01D59/44
CPC分类号： H01J49/105 , Y10T436/25875
摘要： Use of a nebulizer add-gas to reduce metal deposition on the sampling orifices of an inductively coupled plasma mass spectrometer (“ICP-MS”) is disclosed. Specifically, dilute mixtures of Sulfur Hexafluoride (SF6) in an inert gas have been used to reduce transition metal deposition on the sampling orifices of an ICP-MS, thereby greatly enhancing the stability of the ICP-MS sensitivity over time without corroding the internal parts and/or chemically attacking the cones of the ICP-MS.
摘要翻译：公开了使用雾化器附加气体来减少电感耦合等离子体质谱仪（“ICP-MS”）的采样孔上的金属沉积。具体来说，已经使用惰性气体中的六氟化硫（SF 6 S 6）的稀释混合物来减少ICP-MS的取样孔上的过渡金属沉积，从而大大提高ICP-MS的稳定性敏感性随时间而不腐蚀内部部件和/或化学侵蚀ICP-MS的锥体。

7. 发明申请

US20050257856A1 Reactive gases with concentrations of increased stability and processes for manufacturing same 有权
标题翻译：活性气体的浓度增加，稳定性和制造方法相同
公开(公告)号：US20050257856A1
公开(公告)日：2005-11-24
申请号：US11114953
申请日：2005-04-25
申请人： Tracey Jacksier , Robert Benesch , Malik Haouchine
发明人： Tracey Jacksier , Robert Benesch , Malik Haouchine
IPC分类号： C23C16/04 , C23C16/40 , C23C22/82 , F17C3/12
CPC分类号： C23C16/045 , B08B9/22 , B08B9/28 , B08B2203/005 , C23C16/402 , C23G5/00 , F17C1/10 , F17C3/12 , F17C2201/0104 , F17C2201/0128 , F17C2201/052 , F17C2203/0604 , F17C2203/0636 , F17C2203/0639 , F17C2203/0643 , F17C2203/0646 , F17C2203/0648 , F17C2205/0323 , F17C2209/2172 , F17C2209/232 , F17C2221/037 , F17C2223/0123 , F17C2223/013 , F17C2223/0146 , F17C2223/0153 , F17C2260/053
摘要： Methods of passivating a metal surface are described, the methods comprising the steps of exposing the metal surface to a silicon-containing passivation material, evacuating the metal surface, exposing the treated surface to a gas composition, having a concentration of reactive gas that is greater than an intended reactive gas concentration of gas to be transported by the metal surface, evacuating the metal surface to remove substantially all of the gas composition to enable maintenance of an increased shelf-life, low concentration reactive gas at an intended concentration, and exposing the metal surface to the reactive gas at the intended reactive gas concentration. Manufactured products, high stability fluids, and methods of making same are also described.
摘要翻译：描述了钝化金属表面的方法，所述方法包括以下步骤：将金属表面暴露于含硅钝化材料，抽空金属表面，将经处理的表面暴露于气体组合物，反应气体的浓度较大比通过金属表面输送的气体的预期反应气体浓度，抽真空金属表面以去除基本上所有的气体组合物，以便维持预期浓度的增加的保质期低浓度反应气体，并使金属表面以反应气体的浓度反应。还描述了制造产品，高稳定性流体及其制备方法。

8. 发明授权

US10058824B2 Method and apparatus for dynamic gas mixture production 有权
公开(公告)号：US10058824B2
公开(公告)日：2018-08-28
申请号：US14344373
申请日：2012-08-17
申请人： Johann Ponzgraz , David Kihumbu , Tracey Jacksier , Denis Muller
发明人： Johann Ponzgraz , David Kihumbu , Tracey Jacksier , Denis Muller
IPC分类号： B01F3/02 , B01F5/04 , B01F15/02
CPC分类号： B01F3/026 , B01F3/02 , B01F5/04 , B01F5/0456 , B01F15/0201
摘要： The present invention relates to a method for producing and delivering a gas mixture having a selected composition of a first gas and at least one second gas, comprising the following steps: (a) providing a main gas flow comprising the first gas in a main conduit, (b) separating the main gas flow into a first plurality of secondary gas flows, (c) guiding each secondary gas flow through a secondary conduit, (d) adding at least one second gas to at least one of the first plurality of secondary gas flows in the respective secondary conduit through a delivering conduit, said delivering conduit protruding into the secondary conduit, and (e) combining the first plurality of secondary gas flows to the gas mixture. With the technical teaching of the present invention a dynamic gas bottle filling is possible wherein the second gas components may have a concentration form some ppb to percent.

9. 发明申请

US20120210872A1 REMOVAL OF KRYPTON AND XENON IMPURITIES FROM ARGON BY MOF ADSORBENT 有权
标题翻译：从阿尔贡通过财政部门移除KRYPTON和轩尼诗的罪犯
公开(公告)号：US20120210872A1
公开(公告)日：2012-08-23
申请号：US13504508
申请日：2010-10-29
申请人： Yanyu Duan , Tracey Jacksier
发明人： Yanyu Duan , Tracey Jacksier
IPC分类号： B01D53/04
CPC分类号： B01J20/22 , B01J20/226 , B01J20/34 , B01J20/3425 , B01J20/3458 , B01J20/3483 , B01J2220/62 , C01B23/0057 , C01B23/0073 , C01B2210/0034 , C01B2210/0084 , C01B2210/0085
摘要： Disclosed is a system and method for removing trace levels of krypton and xenon from argon by using metal organic framework (MOF) adsorbents.
摘要翻译：公开了一种通过使用金属有机骨架（MOF）吸附剂从氩气中除去痕量氪和氙的系统和方法。

10. 发明申请

US20090223594A1 Reactive Gases With Concentrations Of Increased Stability And Processes For Manufacturing Same 有权
标题翻译：具有增加稳定性和加工浓度的反应性气体制造相同
公开(公告)号：US20090223594A1
公开(公告)日：2009-09-10
申请号：US12416556
申请日：2009-04-01
申请人： Tracey Jacksier , Robert Benesch , Malik Haouchine
发明人： Tracey Jacksier , Robert Benesch , Malik Haouchine
IPC分类号： B65B31/02 , C23C16/00 , B65B3/04
CPC分类号： C23C16/045 , B08B9/22 , B08B9/28 , B08B2203/005 , C23C16/402 , C23G5/00 , F17C1/10 , F17C3/12 , F17C2201/0104 , F17C2201/0128 , F17C2201/052 , F17C2203/0604 , F17C2203/0636 , F17C2203/0639 , F17C2203/0643 , F17C2203/0646 , F17C2203/0648 , F17C2205/0323 , F17C2209/2172 , F17C2209/232 , F17C2221/037 , F17C2223/0123 , F17C2223/013 , F17C2223/0146 , F17C2223/0153 , F17C2260/053
摘要： Methods of passivating a metal surface are described, the methods comprising the steps of exposing the metal surface to a silicon-containing passivation material, evacuating the metal surface, exposing the treated surface to a gas composition, having a concentration of reactive gas that is greater than an intended reactive gas concentration of gas to be transported by the metal surface, evacuating the metal surface to remove substantially all of the gas composition to enable maintenance of an increased shelf-life, low concentration reactive gas at an intended concentration, and exposing the metal surface to the reactive gas at the intended reactive gas concentration. Manufactured products, high stability fluids, and methods of making same are also described.
摘要翻译：描述了钝化金属表面的方法，所述方法包括以下步骤：将金属表面暴露于含硅钝化材料，抽空金属表面，将经处理的表面暴露于气体组合物，反应气体的浓度较大比通过金属表面输送的气体的预期反应气体浓度，抽真空金属表面以去除基本上所有的气体组合物，以便维持预期浓度的增加的保质期低浓度反应气体，并使金属表面以反应气体的浓度反应。还描述了制造产品，高稳定性流体及其制备方法。

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