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1. 发明申请

US20070225469A1 Polyester Resin and Process for Production Thereof 审中-公开
标题翻译：聚酯树脂及其生产工艺
公开(公告)号：US20070225469A1
公开(公告)日：2007-09-27
申请号：US11568872
申请日：2005-05-11
申请人： Minako Akita , Atsushi Kasai , Tomohiko Tanaka
发明人： Minako Akita , Atsushi Kasai , Tomohiko Tanaka
IPC分类号： C08G63/18 , C08G63/78
CPC分类号： C08G63/82 , C08G63/199
摘要： To provide a polyester resin having 1,4-CHDA as the main dicarboxylic acid units, having isomerization of trans-1,4-CHDA suppressed in the esterification and polyconsensation reactions and having a high melting point and excellent heat resistance, and a process for its production. A polyester resin obtainable by preparing an oligomer by an esterification reaction of a dicarboxylic acid component containing 1,4-cyclohexane dicarboxylic acid as the main component, with a diol component, and polycondensing this oligomer in the presence of a polycondensation catalyst; and a process for producing a polyester resin characterized in that the esterification reaction is carried out by means of a basic compound, and then, the polycondensation reaction is carried out by means of a polycondensation catalyst. In the resent invention, T0 and Tp satisfy 0≦{(T0−Tp)/T0}×100≦12 where T0 is the mol % of the trans form in the 1,4-cyclohexane dicarboxylic acid contained in the starting material, and Tp is the mol % of the trans form in the 1,4-cyclohexane dicarboxylic acid units contained in the obtainable polyester resin.
摘要翻译：为了提供具有1,4-CHDA作为主要二羧酸单元的聚酯树脂，其在酯化和多缩合反应中抑制反式-1,4- -CHDA异构化并具有高熔点和优异的耐热性，其生产。通过以1,4-环己烷二羧酸为主要成分的二羧酸成分的酯化反应制备低聚物和二醇成分得到的聚酯树脂，并在缩聚催化剂的存在下使该低聚物缩聚; 以及一种生产聚酯树脂的方法，其特征在于通过碱性化合物进行酯化反应，然后缩聚反应通过缩聚催化剂进行。在本发明中，T0和Tp满足0 <= {（T0-Tp）/ T0}×100 <= 12其中T0是起始材料中所含的1,4-环己烷二羧酸中的反式摩尔％ Tp是所得聚酯树脂中所含的1,4-环己烷二羧酸单元中的反式摩尔％。

2. 发明授权

US08865855B2 Polycarbonate copolymer and method of producing the same 有权
标题翻译：聚碳酸酯共聚物及其制造方法
公开(公告)号：US08865855B2
公开(公告)日：2014-10-21
申请号：US12305660
申请日：2007-06-14
申请人： Michiaki Fuji , Minako Akita , Tomohiko Tanaka
发明人： Michiaki Fuji , Minako Akita , Tomohiko Tanaka
IPC分类号： C08G64/00 , C08G64/30 , C08G64/02
CPC分类号： C08G64/06 , C08G64/0208 , C08G64/305 , C08L69/005 , C08L2666/18
摘要： The problem to be solved by the present invention is to provide a polycarbonate copolymer containing a plant-derived raw material, which is excellent in the mechanical strength and heat-resistant and assured of small refractive index, large Abbe number, small birefringence and excellent transparency. The present invention provides a polycarbonate copolymer containing a constitutional unit derived from a dihydroxy compound represented by the following formula (1) and a constitutional unit derived from an alicyclic dihydroxy compound, wherein the Abbe number is 50 or more and the 5% thermal reduction temperature is 340° C. or more; and a method of producing this polycarbonate copolymer by reacting a dihydroxy compound represented by the following formula (1) and an alicyclic hydroxy compound with a carbonic acid diester in the presence of a polymerization catalyst.
摘要翻译：本发明要解决的问题是提供一种含有植物来源的原料的聚碳酸酯共聚物，其机械强度和耐热性优异，确保小折射率，大的阿贝数，小双折射和优异的透明性。本发明提供含有由下式（1）表示的二羟基化合物的结构单元和来自脂环族二羟基化合物的结构单元的聚碳酸酯共聚物，其中阿贝数为50以上，热降解温度为5％为340℃以上; 以及通过在聚合催化剂存在下使由下式（1）表示的二羟基化合物与脂环族羟基化合物与碳酸二酯反应制备该聚碳酸酯共聚物的方法。

3. 发明申请

US20100190953A1 POLYCARBONATE COPOLYMER AND METHOD OF PRODUCING THE SAME 有权
标题翻译：聚碳酸酯共聚物及其制备方法
公开(公告)号：US20100190953A1
公开(公告)日：2010-07-29
申请号：US12305660
申请日：2007-06-14
申请人： Michiaki Fuji , Minako Akita , Tomohiko Tanaka
发明人： Michiaki Fuji , Minako Akita , Tomohiko Tanaka
IPC分类号： C08G64/00 , C08G65/00
CPC分类号： C08G64/06 , C08G64/0208 , C08G64/305 , C08L69/005 , C08L2666/18
摘要： The object is to provide a polycarbonate copolymer having excellent mechanical strength, good heat resistance, a low refractive index, a large Abbe number, a low berefringence and excellent transparency and containing a plant-derived raw material. Disclosed is a polycarbonate copolymer which comprises a constituent unit derived from a dihydroxy compound represented by the general formula (1) and a constituent unit derived from an alicyclic dihydroxy compound and has an Abbe number of 50 or greater and “a 5% heating weight loss temperature” (a temperature at which the 5% weight loss under heating is observed) of 340° C. or higher. Also disclosed is a process for producing the polycarbonate copolymer by reacting a dihydroxy compound represented by the general formula (1) and an alicyclic dihydroxy compound with a carbonate diester in the presence of a polymerization catalyst.
摘要翻译：本发明的目的是提供具有优异的机械强度，良好的耐热性，低折射率，大的阿贝数，低的光辉度和优异的透明性并且含有植物来源的原料的聚碳酸酯共聚物。公开了一种聚碳酸酯共聚物，其包含衍生自由通式（1）表示的二羟基化合物的结构单元和衍生自脂环族二羟基化合物的结构单元，并且具有50以上的阿贝数和“5％的加热失重温度“（观察到加热时5％重量损失的温度）为340℃以上。还公开了通过在聚合催化剂存在下使由通式（1）表示的二羟基化合物与脂环族二羟基化合物与碳酸二酯反应制备聚碳酸酯共聚物的方法。

4. 发明申请

US20110257362A1 POLYCARBONATE COPOLYMER AND METHOD OF PRODUCING THE SAME 审中-公开
标题翻译：聚碳酸酯共聚物及其制备方法
公开(公告)号：US20110257362A1
公开(公告)日：2011-10-20
申请号：US13172285
申请日：2011-06-29
申请人： Michiaki Fuji , Minako Akita , Tomohiko Tanaka
发明人： Michiaki Fuji , Minako Akita , Tomohiko Tanaka
IPC分类号： C08G64/30
CPC分类号： C08G64/06 , C08G64/0208 , C08G64/305 , C08L69/005 , C08L2666/18
摘要： The problem to be solved by the present invention is to provide a polycarbonate copolymer containing a plant-derived raw material, which is excellent in the mechanical strength and heat-resistant and assured of small refractive index, large Abbe number, small birefringence and excellent transparency. The present invention provides a polycarbonate copolymer containing a constitutional unit derived from a dihydroxy compound represented by the following formula (1) and a constitutional unit derived from an alicyclic dihydroxy compound, wherein the Abbe number is 50 or more and the 5% thermal reduction temperature is 340° C. or more; and a method of producing this polycarbonate copolymer by reacting a dihydroxy compound represented by the following formula (1) and an alicyclic hydroxy compound with a carbonic acid diester in the presence of a polymerization catalyst.
摘要翻译：本发明要解决的问题是提供一种含有植物来源的原料的聚碳酸酯共聚物，其机械强度和耐热性优异，确保小折射率，大的阿贝数，小双折射和优异的透明性。本发明提供含有由下式（1）表示的二羟基化合物的结构单元和来自脂环族二羟基化合物的结构单元的聚碳酸酯共聚物，其中阿贝数为50以上，热降解温度为5％为340℃以上; 以及通过在聚合催化剂存在下使由下式（1）表示的二羟基化合物与脂环族羟基化合物与碳酸二酯反应制备该聚碳酸酯共聚物的方法。

5. 发明申请

US20110003101A1 PROCESSES FOR PRODUCING POLYCARBONATE AND MOLDED POLYCARBONATE ARTICLES 有权
标题翻译：生产聚碳酸酯和成型的聚碳酸酯制品的方法
公开(公告)号：US20110003101A1
公开(公告)日：2011-01-06
申请号：US12747724
申请日：2008-12-10
申请人： Michiaki Fuji , Tomohiko Tanaka , Minako Akita
发明人： Michiaki Fuji , Tomohiko Tanaka , Minako Akita
IPC分类号： B32B1/02 , C08G64/00
CPC分类号： G11B7/2534 , C08G64/0208 , C08G64/1608 , C08G64/305 , C08J5/18 , C08J2369/00 , G02B1/041 , C08L69/00
摘要： A subject for the invention relates to processes for producing a polycarbonate containing a plant-derived starting material and to molded articles thereof, the polycarbonate having excellent mechanical strength, heat resistance, a low refractive index, a large Abbe number, low birefringence, and excellent transparency. The invention relates to a process for producing a polycarbonate which includes a step in which one or more dihydroxy compounds including a dihydroxy compound having at least one linking group —CH2—O— in the molecule thereof are reacted with a carbonic acid diester in the presence of a polymerization catalyst, wherein the dihydroxy compound having at least one linking group —CH2—O— in the molecule thereof has a formic acid content lower than 20 ppm. The invention further relates to a molded article constituted of a polycarbonate or a composition of the polycarbonate, the polycarbonate being a polycarbonate which contains constituent units derived from a dihydroxy compound having at least one linking group —CH2—O— in the molecule thereof and has an Abbe number of 50 or larger and a 5% weight loss temperature of 340° C. or higher.
摘要翻译：本发明的主题涉及制备含有植物来源的原料的聚碳酸酯及其成型体的方法，该聚碳酸酯具有优异的机械强度，耐热性，低折射率，大的阿贝数，低双折射率和优异的透明度。本发明涉及一种制备聚碳酸酯的方法，其包括在其存在下使一种或多种包含分子中具有至少一个连接基团-CH 2 -O-的二羟基化合物的二羟基化合物与碳酸二酯反应的步骤，的聚合催化剂，其中分子中具有至少一个连接基团-CH 2 -O-的二羟基化合物的甲酸含量低于20ppm。本发明还涉及由聚碳酸酯或聚碳酸酯的组合物构成的成型品，该聚碳酸酯为聚碳酸酯，该聚碳酸酯含有由分子内具有至少一个连结基团-CH 2 -O-的二羟基化合物衍生的构成单元，阿贝数为50以上，5％重量减轻温度为340℃以上。

6. 发明授权

US09193823B2 Polycarbonate copolymer and method of producing the same 有权
标题翻译：聚碳酸酯共聚物及其制造方法
公开(公告)号：US09193823B2
公开(公告)日：2015-11-24
申请号：US14267003
申请日：2014-05-01
申请人： Michiaki Fuji , Minako Akita , Tomohiko Tanaka
发明人： Michiaki Fuji , Minako Akita , Tomohiko Tanaka
IPC分类号： C08G64/06 , C08L69/00 , C08G64/02 , C08G64/30
CPC分类号： C08G64/06 , C08G64/0208 , C08G64/305 , C08L69/005 , C08L2666/18
摘要： The problem to be solved by the present invention is to provide a polycarbonate copolymer containing a plant-derived raw material, which is excellent in the mechanical strength and heat-resistant and assured of small refractive index, large Abbe number, small birefringence and excellent transparency. The present invention provides a polycarbonate copolymer containing a constitutional unit derived from a dihydroxy compound represented by the following formula (1) and a constitutional unit derived from an alicyclic dihydroxy compound, wherein the Abbe number is 50 or more and the 5% thermal reduction temperature is 340° C. or more; and a method of producing this polycarbonate copolymer by reacting a dihydroxy compound represented by the following formula (1) and an alicyclic hydroxy compound with a carbonic acid diester in the presence of a polymerization catalyst.
摘要翻译：本发明要解决的问题是提供一种含有植物来源的原料的聚碳酸酯共聚物，其机械强度和耐热性优异，确保小折射率，大的阿贝数，小双折射和优异的透明性。本发明提供含有由下式（1）表示的二羟基化合物的结构单元和来自脂环族二羟基化合物的结构单元的聚碳酸酯共聚物，其中阿贝数为50以上，热降解温度为5％为340℃以上; 以及通过在聚合催化剂存在下使由下式（1）表示的二羟基化合物与脂环族羟基化合物与碳酸二酯反应制备该聚碳酸酯共聚物的方法。

7. 发明授权

US08546515B2 Processes for producing polycarbonate and molded polycarbonate articles 有权
标题翻译：生产聚碳酸酯和模制聚碳酸酯制品的方法
公开(公告)号：US08546515B2
公开(公告)日：2013-10-01
申请号：US12747724
申请日：2008-12-10
申请人： Michiaki Fuji , Tomohiko Tanaka , Minako Akita
发明人： Michiaki Fuji , Tomohiko Tanaka , Minako Akita
IPC分类号： C08G63/02 , C08G63/18
CPC分类号： G11B7/2534 , C08G64/0208 , C08G64/1608 , C08G64/305 , C08J5/18 , C08J2369/00 , G02B1/041 , C08L69/00
摘要： A subject for the invention relates to processes for producing a polycarbonate containing a plant-derived starting material and to molded articles thereof, the polycarbonate having excellent mechanical strength, heat resistance, a low refractive index, a large Abbe number, low birefringence, and excellent transparency. The invention relates to a process for producing a polycarbonate which includes a step in which one or more dihydroxy compounds including a dihydroxy compound having at least one linking group —CH2—O— in the molecule thereof are reacted with a carbonic acid diester in the presence of a polymerization catalyst, wherein the dihydroxy compound having at least one linking group —CH2—O— in the molecule thereof has a formic acid content lower than 20 ppm. The invention further relates to a molded article constituted of a polycarbonate or a composition of the polycarbonate, the polycarbonate being a polycarbonate which contains constituent units derived from a dihydroxy compound having at least one linking group —CH2—O— in the molecule thereof and has an Abbe number of 50 or larger and a 5% weight loss temperature of 340° C. or higher.
摘要翻译：本发明的主题涉及制备含有植物来源的原料的聚碳酸酯及其成型体的方法，该聚碳酸酯具有优异的机械强度，耐热性，低折射率，大的阿贝数，低双折射率和优异的透明度。本发明涉及一种制备聚碳酸酯的方法，其包括在其存在下使一种或多种包含分子中具有至少一个连接基团-CH 2 -O-的二羟基化合物的二羟基化合物与碳酸二酯反应的步骤，的聚合催化剂，其中分子中具有至少一个连接基团-CH 2 -O-的二羟基化合物的甲酸含量低于20ppm。本发明还涉及由聚碳酸酯或聚碳酸酯的组合物构成的成型品，该聚碳酸酯为聚碳酸酯，该聚碳酸酯含有由分子内具有至少一个连结基团-CH 2 -O-的二羟基化合物衍生的构成单元，阿贝数为50以上，5％重量减轻温度为340℃以上。

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