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1. 发明授权

US08969451B2 Method of producing base compound for liquid fluoroelastomer 有权
标题翻译：制备液态含氟弹性体基础化合物的方法
公开(公告)号：US08969451B2
公开(公告)日：2015-03-03
申请号：US13468233
申请日：2012-05-10
申请人： Mikio Shiono , Shinichi Ide , Yujiro Taira
发明人： Mikio Shiono , Shinichi Ide , Yujiro Taira
IPC分类号： C07F7/10 , B32B9/04 , C08K9/06 , C08J3/20 , C08J3/22 , C08L69/00 , C08G65/00 , C08L71/02
CPC分类号： C08K9/06 , C08G65/007 , C08G2650/48 , C08J3/203 , C08J3/226 , C08J2329/10 , C08J2371/00 , C08K3/04 , C08K3/34 , C08K2201/011 , C08L69/00 , C08L83/10 , C08L71/02
摘要： A method of producing a base compound for a liquid fluoroelastomer which is unaffected by the storage state of the added silica powder, and yields minimal fluctuation in the viscosity between production lots. Specifically, a method of producing a base compound for a liquid fluoroelastomer containing: (A) a linear fluoropolyether compound having at least two alkenyl groups within each molecule and having a perfluoroalkyl ether structure within the main chain, and (B) a hydrophobic silica powder, the method including: (1) heating the component (A) under normal pressure at a temperature of 50 to 100 ° C., (2) adding 20 to 60 parts by mass of the component (B) to 100 parts by mass of the component (A) that has been heated in step (1) while performing kneading to obtain a kneaded product, and (3) kneading the kneaded product obtained in step (2) at a temperature exceeding 100° C., either under conditions of heat and reduced pressure or under conditions of heat and pressure.
摘要翻译：一种制备用于液体含氟弹性体的基础化合物的方法，其不受添加的二氧化硅粉末的储存状态的影响，并且在生产批次之间产生最小的粘度波动。具体地说，一种制备液态含氟弹性体的碱性化合物的方法，该方法包括：（A）在每个分子内具有至少两个烯基并且在主链内具有全氟烷基醚结构的直链含氟聚醚化合物，和（B）疏水性二氧化硅粉末该方法包括：（1）在常压下在50〜100℃的温度下加热组分（A），（2）将20〜60质量份的组分（B）加入到100质量份在步骤（1）中加热的组分（A），同时进行捏合以获得捏合产物，和（3）在超过100℃的温度下将步骤（2）中获得的捏合产物捏合，热和减压或在热和压力条件下。

2. 发明授权

US08299196B2 Adhesive composition 有权
标题翻译：粘合剂组合物
公开(公告)号：US08299196B2
公开(公告)日：2012-10-30
申请号：US13085510
申请日：2011-04-13
申请人： Mikio Shiono , Noriyuki Koike
发明人： Mikio Shiono , Noriyuki Koike
IPC分类号： C08G77/08
CPC分类号： C09D183/08 , C08G77/24 , C08L71/02
摘要： An adhesive composition is provided comprising (A) a fluorinated amide compound containing at least two vinyl groups and having a polyfluoro structure, (B) a fluorinated organosilicon compound containing a fluorinated organic group, at least two SiH groups, and an alkyl, aryl or aralkyl group, and (C) a platinum catalyst, and (D) an organosiloxane containing a SiH group and an epoxy and/or trialkoxysilyl group. The composition is cured on brief heating into a product which achieves adhesion to various substrates and has solvent resistance, chemical resistance, heat resistance, low-temperature properties, low moisture permeability, electric insulation, and acid resistance.
摘要翻译：提供一种粘合剂组合物，其包含（A）含有至少两个乙烯基并具有多氟结构的氟化酰胺化合物，（B）含氟化有机基团的氟化有机硅化合物，至少两个SiH基团和烷基，芳基或芳族烷基，（C）铂催化剂，（D）含有SiH基和环氧基和/或三烷氧基甲硅烷基的有机硅氧烷。该组合物在短暂加热下固化成实现对各种基材的粘合性的产品，并具有耐溶剂性，耐化学性，耐热性，低温性，低透湿性，电绝缘性和耐酸性。

3. 发明授权

US08110065B2 Heat-curable fluoropolyether adhesive composition and bonding method 有权
标题翻译：可热固化的氟聚醚粘合剂组合物和粘合方法
公开(公告)号：US08110065B2
公开(公告)日：2012-02-07
申请号：US12124556
申请日：2008-05-21
申请人： Hidenori Koshikawa , Mikio Shiono , Hiroyasu Hara , Takashi Aketa
发明人： Hidenori Koshikawa , Mikio Shiono , Hiroyasu Hara , Takashi Aketa
IPC分类号： C04B37/00 , C09J7/02 , C08F283/00 , C08F283/12 , C08G77/00 , C08G77/38 , C08L83/00
CPC分类号： C08G65/007 , C08G2650/48 , C08K5/0025 , C08L83/00 , C08L83/08 , C08L2666/34 , C09J171/02
摘要： A heat-curable fluoropolyether adhesive composition comprising (A) a linear polyfluoro compound having at least two alkenyl groups and a perfluoropolyether structure, (B) a fluorinated organohydrogensiloxane having at least two SiH groups, (C) a platinum group metal catalyst, (D) an organosiloxane having at least one SiH group and at least one epoxy and/or trialkoxysilyl group, and (E) a compound having at least two allyloxycarbonyl groups can be cured to metal and plastic substrates by heating at a temperature from 20° C. to less than 100° C.
摘要翻译：一种可热固化的氟聚醚粘合剂组合物，其包含（A）具有至少两个烯基和全氟聚醚结构的线性多氟化合物，（B）具有至少两个SiH基团的氟化有机氢硅氧烷，（C）铂族金属催化剂，（D ）具有至少一个SiH基团和至少一个环氧基和/或三烷氧基甲硅烷基的有机硅氧烷，和（E）具有至少两个烯丙氧基羰基的化合物可以通过在20℃的温度下加热固化到金属和塑料基材上。至小于100℃

4. 发明授权

US07851066B2 Curable fluoropolyether composition and integral molded resin/rubber articles 有权
标题翻译：可固化的氟聚醚组合物和整体模塑树脂/橡胶制品
公开(公告)号：US07851066B2
公开(公告)日：2010-12-14
申请号：US12124436
申请日：2008-05-21
申请人： Hiromasa Yamaguchi , Mikio Shiono
发明人： Hiromasa Yamaguchi , Mikio Shiono
IPC分类号： B32B9/04
CPC分类号： C08G65/007 , C08G65/336 , C08G77/12 , C08G77/24 , C08G2650/48 , C08L71/02 , C08L83/04 , C08L2205/02 , Y10T428/31663 , Y10T428/31786 , C08L83/00
摘要： Curable fluoropolyether compositions comprising (a) a polyfluorodialkenyl compound, (b) a fluorinated organohydrogenpolysiloxane, (c) a platinum catalyst, (d) hydrophobic silica powder, (e) a tackifier in the form of a specific silicon compound, and (f) an organosiloxane having a SiH group, an epoxy and/or trialkoxysilyl group, and a perfluoroalkyl or perfluoropolyether group cure to thermoplastic resins to form a durable tight bond at a low temperature within a short time and are readily releasable from metal molds.
摘要翻译：固化氟聚醚组合物，其包含（a）多氟二烯基化合物，（b）氟化有机氢聚硅氧烷，（c）铂催化剂，（d）疏水性二氧化硅粉末，（e）特定硅化合物形式的增粘剂，和（f）具有SiH基团，环氧基和/或三烷氧基甲硅烷基的有机硅氧烷和全氟烷基或全氟聚醚基固化成热塑性树脂，以在短时间内在低温下形成耐久的紧密结合，并且容易从金属模上释放。

5. 发明申请

US20090130318A1 METHOD FOR BONDING POLYAMIDE RESIN AND FLUOROELASTOMER 审中-公开
标题翻译：用于粘结聚酰胺树脂和氟橡胶的方法
公开(公告)号：US20090130318A1
公开(公告)日：2009-05-21
申请号：US12265328
申请日：2008-11-05
申请人： Mikio Shiono , Kenichi Fukuda , Shinichi Sato
发明人： Mikio Shiono , Kenichi Fukuda , Shinichi Sato
IPC分类号： B05D3/02
CPC分类号： C09J5/02 , C08J5/122 , C08J2327/12 , C08J2377/00 , C09J2421/008 , C09J2427/008 , C09J2477/008
摘要： A bond between fluoroelastomer and polyamide resin is established by applying a silane-based primer composition to a surface of polyamide resin, heat treating at 100-200° C., applying a liquid fluoroelastomer composition to the primer coat at room temperature to 100° C., and heat curing at 100-200° C. for bonding the fluoroelastomer to the polyamide resin. The bond between fluoroelastomer and polyamide resin is maintained over a long period of time even in transmission oils.
摘要翻译：通过将硅烷类底漆组合物涂布在聚酰胺树脂的表面上，在100〜200℃下进行热处理，将液态含氟弹性体组合物在室温〜100℃下涂布在底涂层上，建立了含氟弹性体和聚酰胺树脂之间的键并在100-200℃下热固化，以将含氟弹性体粘合到聚酰胺树脂上。含氟弹性体和聚酰胺树脂之间的粘合剂即使在变速箱油中也能长期保持。

6. 发明授权

US4864003A Block-graft polymer and process for producing it 失效
标题翻译：嵌段聚合物及其制备方法
公开(公告)号：US4864003A
公开(公告)日：1989-09-05
申请号：US229738
申请日：1988-08-01
申请人： Teruo Fujimoto , Mikio Shiono , Osamu Watanabe , Koichi Ito
发明人： Teruo Fujimoto , Mikio Shiono , Osamu Watanabe , Koichi Ito
IPC分类号： C08F293/00 , C08F8/44 , C08F275/00 , C08F285/00 , C08F287/00 , C08F290/00 , C08F297/00 , C08F297/02 , C08F299/00 , C08G65/02 , C08G65/08 , C08G77/42 , C08G77/442 , C08G81/02
CPC分类号： C08G81/024 , C08F275/00 , C08F287/00 , C08F297/02 , C08F8/44 , C08G81/021
摘要： Disclosed are a block-graft copolymer comprising a polymer block having a repetitive unit represented by General Formula: ##STR1## wherein A represents an organopolysiloxane chain, a polyalkylene oxide chain, a polyalkylene-imine chain, a polyacrylate chain or a polyacryloyl chain,and a process for producing the same. This block-graft copolymer can have various performances such as an oxygen enrichment performance, an ion concentration property, a capability of forming a complex with a metal salt and a biocompatibility, depending on the kind of graft polymer chains.
摘要翻译：公开了一种嵌段共聚物，其包含具有由通式表示的重复单元的聚合物嵌段：其中A表示有机聚硅氧烷链，聚环氧烷链，聚亚烷基亚胺链，聚丙烯酸酯链或聚丙烯酰基链，以及其制造方法。根据接枝聚合物链的种类，该嵌段共聚物可以具有各种性能，例如富氧性能，离子浓度性质，与金属盐形成络合物的能力和生物相容性。

7. 发明授权

US08860076B2 Optical semiconductor sealing curable composition and optical semiconductor apparatus using this 有权
标题翻译：光半导体密封固化性组合物及其使用的光半导体装置
公开(公告)号：US08860076B2
公开(公告)日：2014-10-14
申请号：US13589364
申请日：2012-08-20
申请人： Hidenori Koshikawa , Mikio Shiono
发明人： Hidenori Koshikawa , Mikio Shiono
IPC分类号： H01L33/00 , H01L33/56 , C08L83/04 , C08G77/12
CPC分类号： C08L83/04 , C08G77/12 , H01L33/56 , H01L2224/45124 , H01L2224/45144 , H01L2224/48091 , H01L2224/48247 , H01L2224/48257 , H01L2224/49107 , C08L71/00 , H01L2924/00014 , H01L2924/00
摘要： There are provided an optical semiconductor sealing curable composition that provides a cured material having excellent transparency, and an optical semiconductor apparatus having an optical semiconductor device sealed using the cured material obtained by curing the optical semiconductor sealing curable composition. There is provided an optical semiconductor sealing curable composition containing: (A) a linear polyfluoro compound; (B) cyclic organosiloxane having an SiH group and a fluorine-containing organic group; (C) a platinum group metal catalyst; (D) cyclic organosiloxane having an SiH group, fluorine-containing organic group, and an epoxy group; and (E) cyclic organosiloxane having an SiH group, a fluorine-containing organic group, and a cyclic carboxylic acid anhydride residue.
摘要翻译：提供了提供透明性优异的固化物的光半导体密封固化性组合物，以及使用通过使光半导体密封固化性组合物固化而得到的固化物密封的光半导体装置的光半导体装置。提供一种光学半导体密封可固化组合物，其包含：（A）线性多氟化合物; （B）具有SiH基和含氟有机基团的环状有机硅氧烷; （C）铂族金属催化剂; （D）具有SiH基的环状有机硅氧烷，含氟有机基团和环氧基团; 和（E）具有SiH基的环状有机硅氧烷，含氟有机基团和环状羧酸酐残基。

8. 发明授权

US07879450B2 Method for preparing silicone rubber/fluoroelastomer integrated rubber article 有权
标题翻译：硅橡胶/含氟弹性体一体化橡胶制品的制备方法
公开(公告)号：US07879450B2
公开(公告)日：2011-02-01
申请号：US11711659
申请日：2007-02-28
申请人： Takashi Matsuda , Mikio Shiono , Takeshi Hashimoto
发明人： Takashi Matsuda , Mikio Shiono , Takeshi Hashimoto
IPC分类号： B32B9/04 , C08G77/24
CPC分类号： F16J15/108 , C08J7/047 , C08J2383/04 , C08J2471/00 , Y10T428/31663
摘要： A rubber article is manufactured by heat curing a heat-curable silicone rubber composition filled with untreated fumed silica to form a substrate, applying a primer composition comprising a fluoroalkylene or fluoropolyether compound having at least one alkenyl radical and at least one hydrolyzable silyl radical onto the substrate surface, and disposing a heat-curable perfluoropolyether elastomer composition thereon and curing the composition for integration. The integrally molded article has characteristics of both silicone rubber and fluoroelastomer.
摘要翻译：通过将填充有未处理的热解法二氧化硅的可热固化的硅橡胶组合物加热固化以形成基底来制造橡胶制品，将包含具有至少一个烯基的氟代亚烷基或含氟聚醚化合物的底漆组合物和至少一种可水解的甲硅烷基基团底物表面，并在其上设置可热固化的全氟聚醚弹性体组合物，并固化该组合物用于整合。一体成形品具有硅橡胶和含氟弹性体的特征。

9. 发明申请

US20080293859A1 CURABLE FLUOROPOLYETHER COMPOSITION AND INTEGRAL MOLDED RESIN/RUBBER ARTICLES 有权
标题翻译：可固化氟聚乙烯组合物和一体成型树脂/橡胶制品
公开(公告)号：US20080293859A1
公开(公告)日：2008-11-27
申请号：US12124436
申请日：2008-05-21
申请人： Hiromasa Yamaguchi , Mikio Shiono
发明人： Hiromasa Yamaguchi , Mikio Shiono
IPC分类号： C08K5/541
CPC分类号： C08G65/007 , C08G65/336 , C08G77/12 , C08G77/24 , C08G2650/48 , C08L71/02 , C08L83/04 , C08L2205/02 , Y10T428/31663 , Y10T428/31786 , C08L83/00
摘要： Curable fluoropolyether compositions comprising (a) a polyfluorodialkenyl compound, (b) a fluorinated organohydrogenpolysiloxane, (c) a platinum catalyst, (d) hydrophobic silica powder, (e) a tackifier in the form of a specific silicon compound, and (f) an organosiloxane having a SiH group, an epoxy and/or trialkoxysilyl group, and a perfluoroalkyl or perfluoropolyether group cure to thermoplastic resins to form a durable tight bond at a low temperature within a short time and are readily releasable from metal molds.
摘要翻译：固化氟聚醚组合物，其包含（a）多氟二烯基化合物，（b）氟化有机氢聚硅氧烷，（c）铂催化剂，（d）疏水性二氧化硅粉末，（e）特定硅化合物形式的增粘剂，和（f）具有SiH基团，环氧基和/或三烷氧基甲硅烷基的有机硅氧烷和全氟烷基或全氟聚醚基固化成热塑性树脂，以在短时间内在低温下形成耐久的紧密结合，并且容易从金属模上释放。

10. 发明申请

US20080132653A1 Coating composition 有权
标题翻译：涂料组成
公开(公告)号：US20080132653A1
公开(公告)日：2008-06-05
申请号：US11979555
申请日：2007-11-05
申请人： Mikio Shiono , Kenichi Fukuda
发明人： Mikio Shiono , Kenichi Fukuda
IPC分类号： C09D183/05 , C08L83/05 , C08L83/04
CPC分类号： C09D183/04 , C08G65/005 , C08G2650/48 , C08J7/047 , C08J2427/00 , C08K5/02 , C08K5/54 , C09D171/02 , C08L83/00
摘要： A coating composition comprises a fluoroelastomer composition and a diluent solvent consisting of a perfluoroalkyl-substituted aromatic compound and a perfluoro organic compound, the fluoroelastomer composition comprising (A) a linear perfluoropolyether compound, (B) a fluorinated organohydrogensiloxane, (C) a platinum catalyst, and (D) an organopolysiloxane containing an SiH group and an epoxy or trialkoxysilyl group. The composition cures into a fluoroelastomer having excellent characteristics and achieves a firm adhesion to a broad range of substrates by brief heating at relatively low temperatures.
摘要翻译：涂料组合物包含含氟弹性体组合物和由全氟烷基取代的芳族化合物和全氟有机化合物组成的稀释剂溶剂，该含氟弹性体组合物包含（A）直链全氟聚醚化合物，（B）氟化有机氢硅氧烷，（C）铂催化剂，（D）含有SiH基和环氧基或三烷氧基甲硅烷基的有机聚硅氧烷。该组合物固化成具有优异特性的含氟弹性体，并通过在较低温度下短暂加热而实现对宽范围基材的牢固粘附。

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