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1. 发明授权

US6143266A Method for producing crystalline inorganic builders 有权
标题翻译：生产结晶无机助洗剂的方法
公开(公告)号：US6143266A
公开(公告)日：2000-11-07
申请号：US125815
申请日：1998-08-26
申请人： Mikio Sakaguchi , Ichiro Sakamoto , Kazuhiro Otsuka , Masaharu Jyono
发明人： Mikio Sakaguchi , Ichiro Sakamoto , Kazuhiro Otsuka , Masaharu Jyono
IPC分类号： C01B33/36 , C01B33/38 , C11D3/12 , C01B33/24 , C01B33/20 , C01B33/32
CPC分类号： C01B33/38 , C01B33/36 , C11D3/1273
摘要： A method for producing a crystalline inorganic builder having the following composition in its anhydrous form: xM.sub.2 O.ySiO.sub.2.zMeO, wherein x, y and z are numerical values satisfying the following relationships: y/x is 1.0 to 4.0, z/y is not more than 1.0, M stands for Na and K, K/Na is 0.01 to 2.0, and Me stands for Ca and/or Mg, the method comprising the steps of (a) adding water, a Na-containing compound, a K-containing compound, and at least one member of Ca-containing compounds and Mg-containing compounds to silica sand, to give a mixture; (b) subjecting the resulting mixture to a hydrothermal treatment; and (c) baking the resulting treated mixture. Also, a method for producing a crystalline inorganic builder having the following composition in its anhydrous form: xM.sub.2 O.ySiO.sub.2, wherein x and y are numerical values satisfying the following relationships: y/x is 1.0 to 4.0, M stands for Na and K, K/Na is 0.01 to 2.0, the method comprising the steps of (a) adding water, a Na-containing compound, a K-containing compound to silica sand, to give a mixture; (b) subjecting the resulting mixture to a hydrothermal treatment; and (c) baking the resulting treated mixture.
摘要翻译： PCT No.PCT / JP98 / 00147 Sec。 371日期：1998年8月26日 102（e）1998年8月26日PCT 1998年1月14日PCT PCT。公开号WO98 / 31631 日期1998年7月23日制备无水形式的具有以下组成的结晶无机助洗剂的方法：xM2O.ySiO2.zMeO，其中x，y和z是满足以下关系的数值：y / x为1.0〜4.0， z / y不大于1.0，M代表Na和K，K / Na为0.01至2.0，Me代表Ca和/或Mg，该方法包括以下步骤：（a）加入水，含Na 化合物，含钾化合物，以及至少一种含Ca化合物和含Mg化合物的硅砂，得到混合物; （b）对所得混合物进行水热处理; 和（c）烘烤得到的处理过的混合物。另外，制备具有以下无机形式的结晶无机助洗剂的方法：xM2O.ySiO2，其中x和y为满足以下关系的数值：y / x为1.0〜4.0，M为Na和K， K / Na为0.01〜2.0，该方法包括以下步骤：（a）将水，含Na化合物，含K化合物加入硅砂中，得到混合物; （b）对所得混合物进行水热处理; 和（c）烘烤得到的处理过的混合物。

2. 发明授权

US06468500B1 Aluminosilicate 有权
标题翻译：硅铝酸盐
公开(公告)号：US06468500B1
公开(公告)日：2002-10-22
申请号：US09530367
申请日：2000-04-28
申请人： Mikio Sakaguchi , Takanori Kotera , Masaharu Jyono , Ichiro Sakamoto
发明人： Mikio Sakaguchi , Takanori Kotera , Masaharu Jyono , Ichiro Sakamoto
IPC分类号： C01B3326
CPC分类号： A61K8/26 , A61K8/22 , A61K2800/28 , A61Q11/00 , A61Q19/10 , C01B33/26 , C09K3/1409 , C11D3/128 , Y10S423/32
摘要： An aluminosilicate in an acicular form, a platy form, or a columnar form and having the composition represented by aM2O.bAl2O3.cSiO2.dRmAn.yH2O, wherein M is at least one of Na and K; R is one or more elements selected from the group consisting of Na, K, Ca and Mg; A is one or more members selected from the group consisting of CO3, SO4, NO3, OH and Cl; a is from 1 to 6; b is from 2 to 8; c is from 2 to 12; d is from 0 to 4; m is from 1 to 2; n is from 1 to 3; and y is from 0 to 32; a polishing agent including the aluminosilicate; and a detergent composition including the aluminosilicate.
摘要翻译：具有针状，板状或柱状的硅铝酸盐，其组成由M 2 O·b Al 2 O 3·cSiO 2·d·R·m·n·H 2 O表示，其中M为Na和K中的至少一种; R是选自Na，K，Ca和Mg中的一种或多种元素; A是选自CO 3，SO 4，NO 3，OH和Cl中的一种或多种; a为1〜6; b为2〜8; c为2〜12; d为0〜4; m为1〜2; n为1〜3; y为0〜32; 包括硅铝酸盐的抛光剂; 和含有硅铝酸盐的洗涤剂组合物。

3. 发明授权

US06027560A Method for producing crystalline, inorganic ion exchange material 失效
标题翻译：生产结晶无机离子交换材料的方法
公开(公告)号：US06027560A
公开(公告)日：2000-02-22
申请号：US913634
申请日：1997-09-19
申请人： Mikio Sakaguchi , Ichiro Sakamoto , Taisuke Aosaki , Kazuhiro Otsuka
发明人： Mikio Sakaguchi , Ichiro Sakamoto , Taisuke Aosaki , Kazuhiro Otsuka
IPC分类号： B01J43/00 , C01B33/20 , C01B33/36 , C11D3/12 , C04B12/04
CPC分类号： C01B33/36
摘要： The method for producing a crystalline, inorganic ion exchange material having the following composition: xM.sub.2 O.ySiO.sub.2.zMeO, wherein x, y and z are numerical values satisfying the relationships of y/x=0.5 to 2.1, preferably 0.5 to 2.0, and z/y=0.001 to 1.0; M stands for Na and K, wherein K/Na is in the range from 0.01 to 1.2; and Me stands for Ca and/or Mg, the method including the steps of adding 1 to 85 parts by weight of water to 100 parts by weight of cullets, wherein the cullets have the following compositon: xM.sub.2 O.ySiO.sub.2 .multidot.zMeO, wherein x, y, z, M, and Me are defined as above, and then baking the resulting mixture.
摘要翻译： PCT No.PCT / JP96 / 00950 Sec。 371日期：1997年9月19日 102（e）1997年9月19日PCT PCT 1996年4月4日PCT公布。公开号WO96 / 33131 日期：1996年10月24日具有以下组成的结晶无机离子交换材料的制造方法：xM2O.ySiO2.zMeO，其中x，y和z是满足y / x = 0.5〜2.1的关系的数值，优选为0.5 至2.0，z / y = 0.001至1.0; M代表Na和K，其中K / Na在0.01至1.2的范围内; Me表示Ca和/或Mg，该方法包括以下步骤：向100重量份的碎玻璃中加入1至85重量份的水，其中所述碎玻璃具有以下组成：xM2O.ySiO2xzMeO，其中x，y， z，M和Me定义如上，然后烘焙所得混合物。

4. 发明授权

US06537962B1 Composite powder 失效
标题翻译：复合粉
公开(公告)号：US06537962B1
公开(公告)日：2003-03-25
申请号：US09508816
申请日：2000-03-17
申请人： Kazuo Oki , Takashi Miyaji , Kazuhiro Otsuka , Mikio Sakaguchi
发明人： Kazuo Oki , Takashi Miyaji , Kazuhiro Otsuka , Mikio Sakaguchi
IPC分类号： C01B3332
CPC分类号： C11D3/046 , C11D3/08 , C11D3/10
摘要： The present invention pertains to a composite powder comprising (A) an alkali metal silicate particle having an average particle size of from 1 to 500 &mgr;m; and (B) a water-soluble salt particle having an average particle size of from 0.01 to 50 &mgr;m, of which solubility to water at 20° C. is 1 g/100 g or more, wherein the alkali metal silicate particle has a composition formula in an anhydride form represented by: xM2O.ySiO2.zMeO (I) wherein M stands for Na and/or K; Me stands for Ca and/or Mg; y/x is from 0.5 to 4.0; z/x is from 0 to 1.0; and Mg/Ca in MeO is from 0 to 10, and wherein the composite powder has a (A)/(B) weight ratio of from 1/9 to 99/1; and a detergent composition comprising the composite powder. The composite powder is a composite powder having a remarkably enhanced storage stability of the alkali metal silicate without impairing the ion exchange capacity owned by the alkali metal silicate.
摘要翻译：本发明涉及复合粉末，其包含（A）平均粒径为1〜500μm的碱金属硅酸盐颗粒; 和（B）平均粒径为0.01〜50μm的水溶性盐粒子，其在20℃下对水的溶解度为1g / 100g以上，其中，碱金属硅酸盐粒子的组成由下式表示的酸酐形式：xM2O.ySiO2.zMeO（I）其中M代表Na和/或K; 我代表Ca和/或Mg; y / x为0.5〜4.0; z / x为0〜1.0; 和MeO中的Mg / Ca为0至10，并且其中复合粉末的（A）/（B）重量比为1/9至99/1; 以及包含所述复合粉末的洗涤剂组合物。该复合粉末是具有显着增强的碱金属硅酸盐的储存稳定性而不损害碱金属硅酸盐所具有的离子交换能力的复合粉末。

5. 发明授权

US5171572A Barium sulfate and cosmetic compositions comprising same 失效
标题翻译：硫酸钡和包含其的化妆品组合物
公开(公告)号：US5171572A
公开(公告)日：1992-12-15
申请号：US665583
申请日：1991-03-06
申请人： Hiroshi Suganuma , Satoshi Takano , Mikio Sakaguchi , Ichiro Sakamoto , Minoru Iwata , Nariyuki Kurotani , Hideaki Koizumi , Hiroshi Itoh , Risa Maejima
发明人： Hiroshi Suganuma , Satoshi Takano , Mikio Sakaguchi , Ichiro Sakamoto , Minoru Iwata , Nariyuki Kurotani , Hideaki Koizumi , Hiroshi Itoh , Risa Maejima
IPC分类号： A61K8/04 , A61K8/23 , A61Q1/02 , A61Q1/06 , A61Q1/08 , A61Q1/10 , A61Q1/12 , C01F11/46
CPC分类号： C01F11/462 , A61K8/0254 , A61K8/23 , A61Q1/02 , A61Q1/06 , A61Q1/08 , A61Q1/10 , A61Q1/12 , C01P2002/72 , C01P2004/01 , C01P2004/20 , C01P2004/32 , C01P2004/54 , C01P2006/60
摘要： Barium sulfate having a specific crystal structure and optical characteristics is disclosed. The crystals have a plate-like structure of which the aspect ratio is 5-100 and the ratio of the square of the circumference of the plate and the area of the orthogonal projection plane is 20:1-150:1. In a preferred embodiment, a thin film of 25 .mu.m thickness with 20% by weight of the barium sulfate powder concentration has a scattering transmittance of 70% or greater and a total transmittance of 85% or greater. The cosmetic compositions to which the barium sulfate is incorporated exhibits excellent extendibility and adhesion to the skin and can effectively hide the spots or freckles on the skin. The cosmetic composition satisfies both the fine naked skin feeling and the skin covering effect, which have never been satisfied by conventional cosmetic compositions.

6. 发明授权

US5939040A Method for producing crystalline, inorganic ion exchange material 失效
标题翻译：生产结晶无机离子交换材料的方法
公开(公告)号：US5939040A
公开(公告)日：1999-08-17
申请号：US894689
申请日：1997-08-26
申请人： Mikio Sakaguchi , Kazuhiro Otsuka , Taisuke Aosaki
发明人： Mikio Sakaguchi , Kazuhiro Otsuka , Taisuke Aosaki
IPC分类号： B01J41/10 , C01B33/36 , C11D3/08
CPC分类号： C01B33/36
摘要： A method for producing a crystalline, inorganic ion exchange material having the following composition: x.sub.1 K.sub.2 O.x.sub.2 Na.sub.2 O.ySiO.sub.2. zMeO, wherein x.sub.1, x.sub.2, y and z are numerical values satisfying the following relationships: y/(x.sub.1 +x.sub.2)=1.0 to 2.1, z/y=0 to 1.0, x.sub.1 /x.sub.2 =0.01 to 2.0, and Me stands for Ca and/or Mg, the method including the steps of adding and blending one or more alkali metal compounds, or one or more alkali metal compounds and one or more alkaline earth metal compounds in cullets having a composition of SiO.sub.2 /Na.sub.2 O=1.5 to 4.2, and baking the resulting mixture.
摘要翻译： PCT No.PCT / JP96 / 00516 Sec。 371日期：1997年8月26日 102（e）日期1997年8月26日PCT提交1996年3月4日PCT公布。出版物WO96 / 27555 日本1996年9月12日制备具有以下组成的结晶无机离子交换材料的方法：x1K2O.x2Na2O.ySiO2。 zMeO，其中x1，x2，y和z是满足以下关系的数值：y /（x1 + x2）= 1.0〜2.1，z / y = 0〜1.0，x1 / x2 = 0.01〜2.0，Me表示 Ca和/或Mg的方法，包括以下步骤：在SiO 2 / Na 2 O = 1.5至4.2的碎片中加入和掺混一种或多种碱金属化合物或一种或多种碱金属化合物和一种或多种碱土金属化合物，并烘烤得到的混合物。

7. 发明授权

US5656213A Process for the production of carbon-filled ceramic composite material 失效
标题翻译：碳填充陶瓷复合材料生产工艺
公开(公告)号：US5656213A
公开(公告)日：1997-08-12
申请号：US457599
申请日：1995-06-01
申请人： Mikio Sakaguchi , Kazuhiro Otsuka
发明人： Mikio Sakaguchi , Kazuhiro Otsuka
IPC分类号： C04B35/56 , C04B35/565 , C04B35/58 , F16C33/04 , F16C33/16 , C01B31/00
CPC分类号： C04B35/522 , C04B35/117 , C04B35/488 , C04B35/52 , C04B35/524 , C04B35/5611 , C04B35/5622 , C04B35/5626 , C04B35/563 , C04B35/565 , C04B35/58007 , C04B35/58014 , C04B35/58064 , C04B35/58071 , C04B35/58078 , C04B35/581 , C04B35/583 , C04B35/584 , C04B35/591 , C04B35/645 , C04B35/6455 , F16C33/043 , F16C33/16
摘要： A process for producing a carbon-filled ceramic composite material comprising a ceramic matrix and a carbon domain dispersed therein with a carbon domain diameter of from 0.01 to 30 .mu.m and a carbon domain area ratio of from 5 to 70%; comprising the steps of mixing ceramic powder, sintering aids and a carbon source, calcining the mixture at 300.degree.-600.degree. C., granulating the mixture, molding and sintering.
摘要翻译：一种碳填充陶瓷复合材料的制造方法，包括陶瓷基体和分散在其中的碳域直径为0.01〜30μm，碳畴面积率为5〜70％的碳域; 包括将陶瓷粉末，烧结助剂和碳源混合的步骤，在300-600℃下煅烧混合物，将混合物成粒，成型和烧结。

8. 发明授权

US5618783A Synthesized inorganic ion exchange material and detergent composition containing the same 失效
标题翻译：合成的无机离子交换材料和含有它的洗涤剂组合物
公开(公告)号：US5618783A
公开(公告)日：1997-04-08
申请号：US395994
申请日：1995-02-28
申请人： Mikio Sakaguchi , Ichiro Sakamoto , Ryuichi Akagi , Shu Yamaguchi , Masaki Tsumadori
发明人： Mikio Sakaguchi , Ichiro Sakamoto , Ryuichi Akagi , Shu Yamaguchi , Masaki Tsumadori
IPC分类号： B01J39/14 , C01B33/36 , C11D3/12 , C11D7/02 , C11D7/14
CPC分类号： B01J39/14 , C01B33/36 , C11D3/1246
摘要： The synthesized inorganic crystalline ion exchange material has a composition represented by the following general formula in an anhydride form:aX.sub.2 O.bSiO.sub.2.cX'O,wherein X represents Na and K; X' represents Ca, or Ca and Mg; b/a is 1.4 to 2.1; c/a is 0.001 to 0.35; K/Na in X.sub.2 O is 0.09 to 1.11; Mg/Ca in X'O is 0 to 100; and K.sub.2 O/SiO.sub.2 is 0.06 to 0.25. The synthesized inorganic crystalline ion exchange material exhibits main shift peaks at least at 1080.+-.6 cm.sup.-1 in Raman scattering spectra in the range of from 900 to 1200 cm.sup.-1. The inorganic ion exchange material of the present invention is excellent in cationic exchange capacity, cationic exchange speed, and anti-solubility, making it useful to be used for a water softener and an alkalinity adjusting agent in detergents.
摘要翻译：合成的无机结晶离子交换材料具有由以下通式表示的组成，其为酸酐形式：aX2O.bSiO2.cX'O，其中X表示Na和K; X'表示Ca或Ca和Mg; b / a为1.4〜2.1; c / a为0.001〜0.35; X2O中的K / Na为0.09〜1.11; X'O中的Mg / Ca为0〜100; K2O / SiO2为0.06〜0.25。合成的无机结晶离子交换材料在900-1200cm -1范围内的拉曼散射光谱中至少在1080 +/- 6cm -1处显示出主要的偏移峰。本发明的无机离子交换材料的阳离子交换能力，阳离子交换速度，抗溶解性优异，可用于洗涤剂中的软水剂和碱性调节剂。

9. 发明授权

US5427711A Synthesized inorganic ion exchange material and detergent composition containing the same 失效
标题翻译：合成的无机离子交换材料和含有它的洗涤剂组合物
公开(公告)号：US5427711A
公开(公告)日：1995-06-27
申请号：US246711
申请日：1994-05-20
申请人： Mikio Sakaguchi , Ichiro Sakamoto , Mutsumi Kuroda , Masaki Tsumadori , Motomitsu Hasumi , Yuichi Sakamoto , Ryuichi Akagi , Fumio Sai
发明人： Mikio Sakaguchi , Ichiro Sakamoto , Mutsumi Kuroda , Masaki Tsumadori , Motomitsu Hasumi , Yuichi Sakamoto , Ryuichi Akagi , Fumio Sai
IPC分类号： B01J39/08 , B01J39/14 , C01B33/20 , C01B33/36 , C11D3/12 , C11D3/386 , C01B33/24 , C01B33/32 , C11D7/02
CPC分类号： C11D3/38636 , B01J39/085 , B01J39/14 , C01B33/20 , C01B33/36 , C11D3/1246 , C11D3/126
摘要： The synthesized crystalline ion exchange material or a hydrate thereof has a chain structure and a composition represented by the following general formula (A) in an anhydride form:xM.sub.2 O.ySiO.sub.2.zM'O, (A)wherein M represents Na and/or K; M' represents Ca and/or Mg; y/x is 0.5 to 2.0; and z/x is 0.005 to 1.0. The chain structure exhibits at least one main scattering peak at 970.+-.20 cm.sup.-1 in Raman spectra. The detergent composition contains the above synthesized inorganic crystalline ion exchange material. The inorganic ion exchange material of the present invention is excellent in both cationic exchange capacity and anti-solubility, making it useful to be used for a water softener and alkalinity regulator in detergents. The detergent composition of the present invention contains an inorganic ion exchange material which has anti-solubility as well as excellent ion exchange capacity and alkaline capacity, thereby offering excellent washing effects and is suitable for the concentration of detergent.
摘要翻译：合成的结晶离子交换材料或其水合物具有以下通式（A）表示的链状结构和酸酐形式的组成：xM2O.ySiO2.zM'O，（A）其中M表示Na和/或K ; M'表示Ca和/或Mg; y / x为0.5〜2.0; z / x为0.005〜1.0。该链结构在拉曼光谱中显示出970 +/- 20cm-1处的至少一个主散射峰。洗涤剂组合物含有上述合成的无机结晶离子交换材料。本发明的无机离子交换材料的阳离子交换容量和抗溶解性均优异，因此可用于洗涤剂中的软水剂和碱度调节剂。本发明的洗涤剂组合物含有具有抗溶解性以及优异的离子交换容量和碱性能的无机离子交换材料，从而提供优异的洗涤效果，适用于洗涤剂的浓缩。

10. 发明授权

US5340582A Barium sulfate cosmetic composition 失效
标题翻译：硫酸钡化妆品组合物
公开(公告)号：US5340582A
公开(公告)日：1994-08-23
申请号：US98819
申请日：1993-07-29
申请人： Hiroki Sugasawa , Satoshi Takano , Mikio Sakaguchi , Ichiro Sakamoto , Minoru Iwata , Nariyuki Kurotani , Hideaki Koizumi , Hiroshi Itoh , Risa Maejima
发明人： Hiroki Sugasawa , Satoshi Takano , Mikio Sakaguchi , Ichiro Sakamoto , Minoru Iwata , Nariyuki Kurotani , Hideaki Koizumi , Hiroshi Itoh , Risa Maejima
IPC分类号： A61K8/04 , A61K8/23 , A61Q1/02 , A61Q1/06 , A61Q1/08 , A61Q1/10 , A61Q1/12 , C01F11/46 , A61K7/02
CPC分类号： C01F11/462 , A61K8/0254 , A61K8/23 , A61Q1/02 , A61Q1/06 , A61Q1/08 , A61Q1/10 , A61Q1/12 , C01P2002/72 , C01P2004/01 , C01P2004/20 , C01P2004/32 , C01P2004/54 , C01P2006/60
摘要： Barium sulfate having a specific crystal structure and optical characteristics is disclosed. The crystals have a plate-like structure of which the aspect ratio is 5-100 and the ratio of the square of the circumference of the plate and the area of the orthogonal projection plane is 20:1-150:1. In a preferred embodiment, a thin film of 25 .mu.m thickness with 20% by weight of the barium sulfate powder concentration has a scattering transmittance of 70% or greater and a total transmittance of 85% or greater. The cosmetic compositions to which the barium sulfate is incorporated exhibits excellent extendibility and adhesion to the skin and can effectively hide the spots or freckles on the skin. The cosmetic composition satisfies both the fine naked skin feeling and the skin covering effect, which have never been satisfied by conventional cosmetic compositions.
摘要翻译：公开了具有特定晶体结构和光学特性的硫酸钡。晶体具有长宽比为5-100的平板状结构，并且板的圆周面积与正交投影面的面积的比率为20:1〜150:1。在优选的实施方案中，具有20重量％的硫酸钡粉末浓度的25μm厚的薄膜具有70％以上的散射透射率和85％以上的总透射率。引入硫酸钡的化妆品组合物表现出优异的延展性和对皮肤的粘附性，并能有效地隐藏皮肤上的斑点或雀斑。化妆品组合物既满足了常规化妆品组合物从未满足的细裸裸肤感和皮肤覆盖效果。

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