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1. 发明授权

US6048953A Curable liquid resin composition 失效
标题翻译：可固化液体树脂组合物
公开(公告)号：US6048953A
公开(公告)日：2000-04-11
申请号：US000474
申请日：1998-02-03
申请人： Miki Kawashima , Kunio Horiuchi , Hiroaki Tanaka
发明人： Miki Kawashima , Kunio Horiuchi , Hiroaki Tanaka
IPC分类号： C08F265/06 , C08L55/00 , C09D4/02 , C09D4/06 , C09D11/10 , C09D155/00 , C08F220/10 , C08F220/18
CPC分类号： C09D155/005 , C08F265/06 , C08L55/005 , C09D11/101 , C09D4/06
摘要： A curable liquid resin composition containing 100 parts by weight of the following (meth)acrylic liquid resin (A) and 1 to 1,000 parts by weight of a (meth)acrylic monomer (B) having an unsaturated double bond in its molecule and having a number average molecular weight of 1,000 or less, the (meth)acrylic liquid resin (A) being a liquid resin which is obtained by polymerizing monomers containing an alkyl (meth)acrylate monomer (a-1-1) of the formula (1),CH.sub.2 C(R.sup.1)COO--R.sup.2 (1)wherein R.sup.1 is a hydrogen atom or CH.sub.3 and R.sup.2 is an alkyl group,and/or an alkylene glycol (meth)acrylate monomer (a-1-2) of the formula (2),CH.sub.2 .dbd.C(R.sup.1)COO(C.sub.n H.sub.2n O).sub.m R.sup.3(2)wherein R.sup.1 is a hydrogen atom or CH.sub.3, R.sup.3 is an alkyl group or a phenyl group, n is an integer of 1 to 3, and m is an integer of 3 to 25, and other polymerizable vinyl monomer (a-2), an average of molecular weights of all the monomers being 100 to 1,500, the liquid resin having a number average molecular weight of 10,000 to 200,000 and a viscosity of 1 to 10,000 poise (measured at 50.degree. C.), or a modified product of the above liquid resin, the curable liquid resin composition can form a film as a film-forming material or as a resin for an adhesive without using a solvent and give a cured film.
摘要翻译： PCT No.PCT / JP97 / 01871 Sec。 371日期1998年2月3日 102（e）1998年2月3日PCT 1997年6月2日PCT公布。出版物WO97 / 46601 日期1997年12月11日含有100重量份以下（甲基）丙烯酸系液态树脂（A）和1〜1000重量份具有不饱和双键的（甲基）丙烯酸系单体（B）的固化性液态树脂组合物其分子的数均分子量为1000以下，作为液状树脂的（甲基）丙烯酸系液态树脂（A）是将含有（甲基）丙烯酸烷基酯单体（a-1-1）的单体式（1），其中R1是氢原子或CH3，R2是烷基的CH2（R）COO-R2（1），和/或亚烷基二醇（甲基）丙烯酸酯单体（a-1-2）式（2）中，CH 2 = C（R 1）COO（C n H 2n O）m R 3（2）其中R 1为氢原子或CH 3，R 3为烷基或苯基，n为1〜3的整数， m为3〜25的整数，其它的聚合性乙烯基单体（a-2），所有单体的分子量平均为100〜1500，数均分子量为10,000〜200,000的液态树脂和vi 1〜10,000泊（50℃测定）的光泽度或上述液态树脂的改性物，可固化型液态树脂组合物可以形成作为成膜材料的膜或粘合剂用树脂，而不使用溶剂，得到固化膜。

2. 发明授权

US5576405A Liquid-resin, process for the production thereof and its use 失效
标题翻译：液体树脂，其生产方法及其用途
公开(公告)号：US5576405A
公开(公告)日：1996-11-19
申请号：US257050
申请日：1994-06-08
申请人： Miki Kawashima , Kunio Horiuchi
发明人： Miki Kawashima , Kunio Horiuchi
IPC分类号： C08F220/18 , C08F220/10 , C08F212/06 , C08F220/44 , C07G69/73
CPC分类号： C08F220/18
摘要： A liquid resin having a number average molecular weight of 10,000 to 200,000 and a viscosity, measured at 50.degree. C., of 500 to 30,000 cps, obtained by the copolymerization of a composition containing(a) 35 to 98% by weight of a monomer of the formula,CH.sub.2 .dbd.C(R.sup.1)COOR.sup.2wherein R.sup.1 is a hydrogen or methyl and R.sup.2 is a hydrocarbon group having 4 to 22 carbon atoms,(b) 2 to 40% by weight of a polymerizable unsaturated carboxylic acid, and(c) 0 to 60% by weight of other polymerizable vinyl monomer.
摘要翻译：通过共聚含有（a）35〜98重量％的单体的组合物得到的数均分子量为10,000〜200,000的液态树脂和在50℃下测定的500〜30,000cps的粘度，其中R 1为氢或甲基，R 2为碳原子数为4〜22的烃基，（b）2〜40重量％的聚合性不饱和羧酸，（c） 0〜60重量％的其他可聚合乙烯基单体。

3. 发明授权

US5686545A Liquid resin, process for the production thereof and its use 失效
标题翻译：液体树脂，其生产方法及其用途
公开(公告)号：US5686545A
公开(公告)日：1997-11-11
申请号：US691017
申请日：1996-08-05
申请人： Miki Kawashima , Kunio Horiuchi
发明人： Miki Kawashima , Kunio Horiuchi
IPC分类号： C08F220/18 , C08F220/10 , C08F212/06 , C08F220/44 , C07G69/73
CPC分类号： C08F220/18
摘要： A liquid resin having a number average molecular weight of 10,000 to 200,000 and a viscosity, measured at 50.degree. C., of 500 to 30,000 cps, obtained by the copolymerization of a composition containing (a) 35 to 98% by weight of a monomer of the formula, CH.sub.2 =C(R.sup.1)COOR.sup.2 wherein R.sup.1 is hydrogen or methyl and R.sup.2 is a hydrocarbon group having 4 to 22 carbon atoms, (b) 2 to 40% by weight of a polymerizable unsaturated carboxylic acid, and (c) 0 to 60% by weight of other polymerizable vinyl monomer.
摘要翻译：通过共聚含有（a）35〜98重量％的单体的组合物得到的数均分子量为10,000〜200,000的液态树脂和在50℃下测定的500〜30,000cps的粘度，其中R 1为氢或甲基，R 2为碳原子数为4〜22的烃基，（b）2〜40重量％的聚合性不饱和羧酸，（c） 0〜60重量％的其他可聚合乙烯基单体。

4. 发明授权

US5668244A Liquid polyesters from cyclic acid anhydrides 失效
标题翻译：来自环状酸酐的液体聚酯
公开(公告)号：US5668244A
公开(公告)日：1997-09-16
申请号：US491366
申请日：1995-06-16
申请人： Miki Kawashima , Takeo Yamaguchi , Kunio Horiuchi , Hiromi Uchida
发明人： Miki Kawashima , Takeo Yamaguchi , Kunio Horiuchi , Hiromi Uchida
IPC分类号： C08G63/42 , C08G63/58
CPC分类号： C08G63/42 , C08G63/58
摘要： A liquid polyester obtained by reacting a cyclic acid anhydride (A) containing at least 10 mol % of one of specific cyclic acid anhydrides with an epoxy compound (B) in a cyclic acid anhydride (A):epoxy compound (B) molar ratio of 10:8-10:12, can be applied with a conventionally generally used film-forming machine such as a roll coater or a printing machine, can easily give a film-forming material such as a solvent-free coating composition or ink and a curable liquid resin for use as an adhesive, is a low-temperature curing liquid polyester useful as a compatibilizer, a surface-tension modifier, a pigment dispersing agent and a metal chelating agent, and is curable in air in the presence of a relatively small amount of a catalyst.
摘要翻译：将在环状酸酐（A）中含有至少10mol％的特定环状酸酐与环氧化合物（B）的环状酸酐（A）：环氧化合物（B）的摩尔比 10：8-10：12可以用常规使用的成膜机如辊涂机或印刷机进行涂布，可以容易地得到诸如无溶剂的涂料组合物或油墨的成膜材料和用作粘合剂的可固化液体树脂是用作增容剂的低温固化液体聚酯，表面张力改性剂，颜料分散剂和金属螯合剂，并且可在相对较小的存在下在空气中固化催化剂量。

5. 发明授权

US6136943A Multi-branched compounds and curable composition 失效
标题翻译：多支化合物和可固化组合物
公开(公告)号：US6136943A
公开(公告)日：2000-10-24
申请号：US144220
申请日：1998-08-31
申请人： Miki Kawashima , Minoru Nakamura , Hiroaki Tanaka
发明人： Miki Kawashima , Minoru Nakamura , Hiroaki Tanaka
IPC分类号： C08G18/32 , C08G18/81 , C08G83/00 , C08L101/00 , C09D201/00
CPC分类号： C08G83/003 , C08G18/3278 , C08G18/8116 , C08G18/8175 , C08L101/005 , C09D201/005
摘要： A multi-branched compound which can give a compound having a relatively high molecular weight but a low viscosity and having excellent coating performances, and can give a solvent-less composition having sufficient coating performances and having a low viscosity sufficient for forming a coating, and which can serve to decrease the amount of a low-molecular-weight compound having performance problems and the multi-branched compound is obtained by reacting a core compound obtained by subjecting (a) a polyamino compound having a molecule containing a primary or secondary amino group and (b-1) an active-hydrogen-containing (meth)acrylic compound in Michael addition reaction with (c) a vinyl-group-containing compound having a functional group reactive with the active hydrogen.
摘要翻译：能够提供具有较高分子量但低粘度且具有优异涂层性能的化合物的多支化化合物，并且可以得到具有足够的涂料性能和低粘度的无溶剂组合物，以形成涂料，这可以减少具有性能问题的低分子量化合物的量，多支化化合物是通过使（a）具有分子中含有伯或仲氨基的聚氨基化合物和（b-1）与迈克尔加成反应中的含活性氢的（甲基）丙烯酸化合物与（c）具有与活性氢反应的官能团的含乙烯基的化合物。

6. 发明授权

US5644010A Curable liquid resin, process for the production thereof and use thereof 失效
标题翻译：可固化液体树脂，其制备方法和用途
公开(公告)号：US5644010A
公开(公告)日：1997-07-01
申请号：US503723
申请日：1995-07-18
申请人： Toru Kurihashi , Miki Kawashima , Takeo Yamaguchi
发明人： Toru Kurihashi , Miki Kawashima , Takeo Yamaguchi
IPC分类号： C08F220/18 , C08F220/28 , C08F224/00 , C07C11/12 , C07C69/54 , C07C233/16 , C08F220/04 , C08F220/10 , C08F220/58 , C08F230/00
CPC分类号： C08F220/18 , C08F220/28 , Y10S106/901
摘要： A curable liquid resin which can give a coating composition capable of forming a film, the curable liquid resin being a copolymer obtained from(A) a monomer of the formula (1) or (2),CH.sub.2 .dbd.C(R.sup.1)COO--R.sup.2 (1)CH.sub.2 .dbd.C(R.sup.3)COO(C.sub.n H.sub.2n O).sub.m--R.sup.4(2)and(B) at least one monomer selected from the group consisting of(B1) a monomer prepared by reacting an ethylenically unsaturated epoxide (a) with a fatty acid (b) of the formula (3)R.sup.5 COOH (3)(B2) a monomer of the formula (4),CH.sub.2 .dbd.C(R.sup.6)CONR.sup.7 R.sup.8 (4)and(B3) a monomer whose molecule has at least two ethylenically unsaturated double bonds.
摘要翻译：一种可以得到能够形成膜的涂料组合物的可固化液体树脂，该可固化液体树脂是由（A）式（1）或（2）的单体获得的共聚物，CH 2 = C（R 1）COO-R 2 （1）CH 2 = C（R 3）COO（C n H 2n O）m -R 4（2）和（B）至少一种选自（B1）通过烯属不饱和环氧化物（a）与式（3）的脂肪酸（b）R5COOH（3）（B2）式（4）的单体，CH2 = C（R6）CONR7R8（4）和（B3）分子具有至少两个烯属不饱和双键。

7. 发明授权

US5705602A Process for the production of star-like or comb-like branched aliphatic polyamino compound and curable resin composition 失效
标题翻译：制备星形或梳状支链脂族聚氨基化合物和可固化树脂组合物的方法
公开(公告)号：US5705602A
公开(公告)日：1998-01-06
申请号：US801027
申请日：1997-02-19
申请人： Miki Kawashima , Takeo Yamaguchi , Toru Kurihashi , Norifumi Watanabe
发明人： Miki Kawashima , Takeo Yamaguchi , Toru Kurihashi , Norifumi Watanabe
IPC分类号： C08G69/00 , C08G59/50 , C08G73/02 , C08G83/00 , C08L63/00
CPC分类号： C08G83/003 , C08G73/02 , C08G73/028 , C08L63/00
摘要： A star-like or comb-like branched aliphatic polyamino compound for use as a basic catalyst or a curing agent, as an effective thixotropic agent or viscosity adjusting agent for an aqueous medium, as a component for any one of a coating-forming agent, a sealing agent, a molding material and an adhesive resin, or as a substantially solvent-free coating composition, molding material or adhesive resin. The process for the production of the above compound comprises (a) forming an adduct of ammonia or an aliphatic amino compound having an amino group (compound A) with methyl acrylate, adding an alkylenediamine having 2 to 12 carbon atoms to the adduct to carry out an ester-amide exchange reaction (b), thereby obtaining a polyamino compound (B) having a total of 2 to 100 aliphatic primary amino and secondary amino groups per molecule and having a number average molecular weight of 170 to 10,000, and forming an adduct of the polyamino compound (B) with an acrylic acid ester (C) of the formula (1), CH.sub.2 =CHCOO--R.sub.1 (1) wherein R.sub.1 is an alkyl group having 4 to 50 carbon atoms or a group of (C.sub.n H.sub.2n O).sub.m R.sub.2 in which R.sub.2 is an alkyl group having 1 to 5 carbon atoms, n is an integer of 1 to 3 and m is an integer of 1 to 25.
摘要翻译：用作碱性催化剂或固化剂的星状或梳状支链脂族聚氨基化合物作为水性介质的有效触变剂或粘度调节剂，作为涂料形成剂，密封剂，成型材料和粘合剂树脂，或作为基本上无溶剂的涂料组合物，成型材料或粘合剂树脂。制备上述化合物的方法包括（a）将氨或氨基（脂肪族氨基化合物）与丙烯酸甲酯一起形成加合物，向该加合物中加入具有2-12个碳原子的亚烷基二胺进行酯酰胺交换反应（b），从而获得每分子总共具有2至100个脂族伯氨基和仲氨基并且数均分子量为170至10,000的聚氨基化合物（B），并形成加合物的聚氨基化合物（B）与式（1）的丙烯酸酯（C），CH 2 = CHCOO-R 1（1），其中R 1是具有4〜50个碳原子的烷基或（C n H 2n O）m R 2 其中R 2为具有1至5个碳原子的烷基，n为1至3的整数，m为1至25的整数。

8. 发明授权

US06187897B1 Vinyl-group-containing dendrimer and curable composition 失效
标题翻译：含乙烯基的树枝状聚合物和可固化组合物
公开(公告)号：US06187897B1
公开(公告)日：2001-02-13
申请号：US09121868
申请日：1998-07-24
申请人： Miki Kawashima , Minoru Nakamura , Hiroaki Tanaka
发明人： Miki Kawashima , Minoru Nakamura , Hiroaki Tanaka
IPC分类号： C08G6300
CPC分类号： C08G83/003 , C08G18/3278 , C08G18/8116 , C08G18/8175 , C08L101/005 , C09D201/005 , Y10S424/16
摘要： A vinyl-group-containing dendrimer useful in coating and printing and is curable by any one of conventional triggers such as heating, ultraviolet light, infrared light, electron beams and &ggr; rays, the composition comprising a vinyl-group-containing dendrimer (A) comprising a core portion, branching portions, branches and at least 4 terminal portions and having a vinyl group as a terminal portion and a long-chain group and a curable unsaturated-group-containing compound (B), and the composition comprising a vinyl-group-containing dendrimer (A) obtained by reacting a polyfunctional compound (a) having at least three active-hydrogen-containing groups in a terminal per molecule and having at least five active hydrogen atoms per molecule with a long-chain-group-containing compound (b) having a functional group reactive with an active hydrogen atom so as to leave part of the active hydrogen atoms, thereby obtaining a long-chain-group-containing multi-branched compound (X), and reacting the long-chain-containing multi-branched compound (X) with a vinyl-group-containing compound (c) having a functional group reactive with an active hydrogen atom and a curable unsaturated-group-containing compound (B).
摘要翻译：可用于涂布和印刷的含乙烯基的树枝状聚合物并且可通过任何常规触发剂如加热，紫外光，红外光，电子束和γ射线固化，所述组合物包含含乙烯基的树枝状聚合物（A）包含芯部分，支链部分，分支和至少4个末端部分，并且具有乙烯基作为末端部分，长链基团和含固化不饱和基团的化合物（B），并且所述组合物包含乙烯基 - 通过使具有至少三个含有活性氢的基团的多官能化合物（a）在每个分子的末端与每个分子具有至少五个活性氢原子的长链基团反应获得的含基团的树枝状大分子（A）具有与活性氢原子反应的官能团的化合物（b），以留下部分活性氢原子，从而得到含有长链基团的多支化化合物（X），并使具有含活性氢原子的具有官能团的含乙烯基的化合物（c）的长链多支化合物（X）和含有可固化不饱和基团的化合物（B）。

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