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1. 发明申请

US20060199940A1 Method of preparing polycarbonate resin 有权
公开(公告)号：US20060199940A1
公开(公告)日：2006-09-07
申请号：US11368568
申请日：2006-03-06
申请人： Jong Kim , Boo Woo , Sung Park , Mijeung Hong
发明人： Jong Kim , Boo Woo , Sung Park , Mijeung Hong
IPC分类号： C08G64/00
CPC分类号： C08G64/14 , C08G64/42
摘要： A method of preparing a polycarbonate resin having improved thermal stability is provided. The method includes: mixing polycarbonate having hydroxy terminal groups and a end terminator, a compound of formula (1) (refer to the detailed description section) at normal temperature and pressure to obtain a mixture; and performing a melt reaction on the mixture at 250-320° C. and reduced pressure to highly reduce the final concentration of the hydroxy terminal groups of the polycarbonate resin.

2. 发明申请

US20060100413A1 Method of producing modified polycarbonate using spray-crystallizing method 有权
标题翻译：使用喷雾结晶法制备改性聚碳酸酯的方法
公开(公告)号：US20060100413A1
公开(公告)日：2006-05-11
申请号：US11268192
申请日：2005-11-07
申请人： Mijeung Hong , Jong Kim , Sung Park , Boo Woo
发明人： Mijeung Hong , Jong Kim , Sung Park , Boo Woo
IPC分类号： C08G64/00
CPC分类号： C08G64/20 , C08G64/186 , C08G64/205 , C08G64/307
摘要： Provided is a method of producing a high-molecular weight modified polycarbonate resin. The method includes a melt condensation polymerization process in which transesterification and quick condensation polymerization are sequentially performed, a spray crystallization process, and a solid state polymerization process. When this method is used, solid state polymerization can be performed without additional drying, milling and fractionation processes so that the operation time and costs are highly reduced. In addition, crystallinity and size of crystallized modified polycarbonate particles can be efficiently controlled to produce a high-molecular weight modified polycarbonate having uniform physical properties in the solid state polymerization.
摘要翻译：提供高分子量改性聚碳酸酯树脂的制造方法。该方法包括依次进行酯交换和快速缩聚的熔融缩聚方法，喷雾结晶法和固态聚合法。当使用该方法时，可以进行固态聚合而不需要额外的干燥，研磨和分馏过程，从而高度降低操作时间和成本。此外，可以有效地控制结晶化聚碳酸酯颗粒的结晶度和尺寸，以制备在固态聚合中具有均匀物理性能的高分子量改性聚碳酸酯。

3. 发明授权

US07495065B2 Method of preparing polycarbonate resin 有权
标题翻译：聚碳酸酯树脂的制备方法
公开(公告)号：US07495065B2
公开(公告)日：2009-02-24
申请号：US11368568
申请日：2006-03-06
申请人： Jong Hun Kim , Boo Gon Woo , Sung Kyou Park , Mijeung Hong
发明人： Jong Hun Kim , Boo Gon Woo , Sung Kyou Park , Mijeung Hong
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： C08G64/14 , C08G64/42
摘要： A method of preparing a polycarbonate resin having improved thermal stability is provided. The method includes: mixing polycarbonate having hydroxy terminal groups and a end terminator, a compound of formula (1) (refer to the detailed description section) at normal temperature and pressure to obtain a mixture; and performing a melt reaction on the mixture at 250-320° C. and reduced pressure to highly reduce the final concentration of the hydroxy terminal groups of the polycarbonate resin.
摘要翻译：提供了制备具有改进的热稳定性的聚碳酸酯树脂的方法。该方法包括：在常温常压下混合具有羟基末端基团的聚碳酸酯和末端终止剂，式（1）化合物（详细描述部分），得到混合物; 并在250-320℃下对该混合物进行熔融反应并减压以高度降低聚碳酸酯树脂的羟基端基的最终浓度。

4. 发明申请

US20060089484A1 Method of preparing polycarbonate resin 有权
标题翻译：聚碳酸酯树脂的制备方法
公开(公告)号：US20060089484A1
公开(公告)日：2006-04-27
申请号：US11255515
申请日：2005-10-21
申请人： Mijeung Hong , Jong Hun Kim , Sung Kyou Park , Boo Gon Woo
发明人： Mijeung Hong , Jong Hun Kim , Sung Kyou Park , Boo Gon Woo
IPC分类号： C08G64/00
CPC分类号： C08G64/307 , C08G64/186 , C08G64/205
摘要： A method of preparing a high molecular weight polycarbonate resin is provided. In the method, a condensation polymerization process is used so that a mole fraction of arylcarbonate existing in a terminated group of a reaction side product having a degree of polymerization of less than 3 obtained as a result of transesterification and in a non-reacted diarylcarbonate is reduced. As a result, a high molecular weight polycarbonate can be obtained by solid state polymerization. A polycarbonate with an identical molecular weight can be produced in a substantially short time, compared with a polycarbonate produced through solid state polymerization without condensation polymerization. In addition, the non-use of a poisonous phosgene contributes to stability. Furthermore, quality polycarbonate may be guaranteed.
摘要翻译：提供了制备高分子量聚碳酸酯树脂的方法。在该方法中，使用缩聚方法，使得存在于作为酯交换反应的结果得到的聚合度小于3的反应副产物的末端基团中的芳基碳酸酯的摩尔分数和未反应的碳酸二芳基酯的摩尔分数为减少结果，可以通过固态聚合获得高分子量聚碳酸酯。与通过不进行缩聚的固相聚合制造的聚碳酸酯相比，可以在短时间内生产具有相同分子量的聚碳酸酯。此外，不使用有毒光气有助于稳定。此外，可以保证质量的聚碳酸酯。

5. 发明授权

US07368521B2 Method of producing modified polycarbonate using spray-crystallizing method 有权
标题翻译：使用喷雾结晶法制备改性聚碳酸酯的方法
公开(公告)号：US07368521B2
公开(公告)日：2008-05-06
申请号：US11268192
申请日：2005-11-07
申请人： Mijeung Hong , Jong Hun Kim , Sung Kyou Park , Boo Gon Woo
发明人： Mijeung Hong , Jong Hun Kim , Sung Kyou Park , Boo Gon Woo
IPC分类号： C08F6/00
CPC分类号： C08G64/20 , C08G64/186 , C08G64/205 , C08G64/307
摘要： Provided is a method of producing a high-molecular weight modified polycarbonate resin. The method includes a melt condensation polymerization process in which transesterification and quick condensation polymerization are sequentially performed, a spray crystallization process, and a solid state polymerization process. When this method is used, solid state polymerization can be performed without additional drying, milling and fractionation processes so that the operation time and costs are highly reduced. In addition, crystallinity and size of crystallized modified polycarbonate particles can be efficiently controlled to produce a high-molecular weight modified polycarbonate having uniform physical properties in the solid state polymerization.
摘要翻译：提供高分子量改性聚碳酸酯树脂的制造方法。该方法包括依次进行酯交换和快速缩聚的熔融缩聚方法，喷雾结晶法和固态聚合法。当使用该方法时，可以进行固态聚合而不需要额外的干燥，研磨和分馏过程，从而高度降低操作时间和成本。此外，可以有效地控制结晶化聚碳酸酯颗粒的结晶度和尺寸，以制备在固态聚合中具有均匀物理性能的高分子量改性聚碳酸酯。

6. 发明授权

US07332559B2 Method of preparing polycarbonate resin 有权
标题翻译：聚碳酸酯树脂的制备方法
公开(公告)号：US07332559B2
公开(公告)日：2008-02-19
申请号：US11255515
申请日：2005-10-21
申请人： Mijeung Hong , Jong Hun Kim , Sung Kyou Park , Boo Gon Woo
发明人： Mijeung Hong , Jong Hun Kim , Sung Kyou Park , Boo Gon Woo
IPC分类号： C08G64/00
CPC分类号： C08G64/307 , C08G64/186 , C08G64/205
摘要： A method of preparing a high molecular weight polycarbonate resin is provided. In the method, a condensation polymerization process is used so that a mole fraction of arylcarbonate existing in a terminated group of a reaction side product having a degree of polymerization of less than 3 obtained as a result of transesterification and in a non-reacted diarylcarbonate is reduced. As a result, a high molecular weight polycarbonate can be obtained by solid state polymerization. A polycarbonate with an identical molecular weight can be produced in a substantially short time, compared with a polycarbonate produced through solid state polymerization without condensation polymerization. In addition, the non-use of a poisonous phosgene contributes to stability. Furthermore, quality polycarbonate may be guaranteed.
摘要翻译：提供了制备高分子量聚碳酸酯树脂的方法。在该方法中，使用缩聚方法，使得存在于作为酯交换反应的结果得到的聚合度小于3的反应副产物的末端基团中的芳基碳酸酯的摩尔分数和未反应的碳酸二芳基酯的摩尔分数为减少结果，可以通过固态聚合获得高分子量聚碳酸酯。与通过不进行缩聚的固相聚合制造的聚碳酸酯相比，可以在短时间内生产具有相同分子量的聚碳酸酯。此外，不使用有毒光气有助于稳定。此外，可以保证质量的聚碳酸酯。

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