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1. 发明授权

US06765084B2 Production process for ethylene oxide resin 有权
标题翻译：环氧乙烷树脂的生产工艺
公开(公告)号：US06765084B2
公开(公告)日：2004-07-20
申请号：US10335807
申请日：2003-01-02
申请人： Michiyuki Kono , Manabu Kikuta , Masahito Nishiura , Fumihide Tamura , Shigetaka Takamiya , Taketo Toba
发明人： Michiyuki Kono , Manabu Kikuta , Masahito Nishiura , Fumihide Tamura , Shigetaka Takamiya , Taketo Toba
IPC分类号： C08G600
CPC分类号： B01D3/06 , B01D1/225 , C08G65/30
摘要： The present invention provides a novel production process for an ethylene oxide resin, in which, when the ethylene oxide resin is obtained, it is arranged that the resin should contain no antistatic agent, and further its water content is also easily controlled in not more than a definite amount, and the thermal damage of the above resin is prevented, and besides, the reduction of the cost can also be actualized. The production process for an ethylene oxide resin, according to the present invention, comprises the step of carrying out devolatilization of a solvent from a polymerization reaction liquid containing the solvent, thereby obtaining the ethylene oxide resin; with the production process being characterized by arranging that: after the devolatilization, the resin should have a solvent concentration of 0.01 to 30 weight % and a water content of not more than 200 ppm, and the resin should contain no antistatic agent.
摘要翻译：本发明提供一种新型的环氧乙烷树脂的制造方法，其中，当得到环氧乙烷树脂时，树脂不含抗静电剂，其含水量也容易控制在不超过一定量，并且防止了上述树脂的热损伤，并且还可以实现成本的降低。根据本发明的环氧乙烷树脂的制备方法包括从含有溶剂的聚合反应液中进行溶剂脱挥发分的步骤，得到环氧乙烷树脂; 其制造方法的特征在于：在脱挥发分后，树脂的溶剂浓度为0.01〜30重量％，水含量不大于200ppm，树脂不含抗静电剂。

2. 发明授权

US06864353B2 Production process for ethylene oxide copolymer 有权
标题翻译：环氧乙烷共聚物的生产工艺
公开(公告)号：US06864353B2
公开(公告)日：2005-03-08
申请号：US10336421
申请日：2003-01-03
申请人： Michiyuki Kono , Manabu Kikuta , Masahito Nishiura , Fumihide Tamura , Taketo Toba , Shigetaka Takamiya , Koichiro Saeki , Kazuo Takei , Toshiaki Kuriyama , Masashi Yukitake
发明人： Michiyuki Kono , Manabu Kikuta , Masahito Nishiura , Fumihide Tamura , Taketo Toba , Shigetaka Takamiya , Koichiro Saeki , Kazuo Takei , Toshiaki Kuriyama , Masashi Yukitake
IPC分类号： C08G65/14 , C08G65/26 , C08G65/34
CPC分类号： C08G65/14 , C08G65/2696
摘要： The present invention provides a production process, in which, when an ethylene oxide copolymer is obtained, conditions for obtaining this copolymer having a desirable molecular weight with ease and good reproducibility are provided. The production process for an ethylene oxide copolymer, according to the present invention, comprises the step of carrying out polymerization of a monomer mixture under stirring in a solvent, thereby obtaining the ethylene oxide copolymer, wherein the monomer mixture includes ethylene oxide and a substituted oxirane compound of a structural formula (1) as essential raw materials; with the production process being characterized in that the stirring is carried out by a stirring power of not less than 0.6 kW/m3.
摘要翻译：本发明提供一种制备方法，其中当获得环氧乙烷共聚物时，提供了获得具有所需分子量并且具有良好重现性的共聚物的条件。根据本发明的环氧乙烷共聚物的制备方法包括在溶剂中在搅拌下进行单体混合物聚合的步骤，从而得到环氧乙烷共聚物，其中单体混合物包括环氧乙烷和取代的环氧乙烷结构式（1）的化合物作为必需的原料; 其制造方法的特征在于通过不低于0.6kW / m 3的搅拌功率进行搅拌。

3. 发明申请

US20060276620A1 Process for manufacturing a pellet-shaped nonionic alkylene oxide resin 审中-公开
标题翻译：丸状非离子型环氧烷树脂的制造方法
公开(公告)号：US20060276620A1
公开(公告)日：2006-12-07
申请号：US11442188
申请日：2006-05-25
申请人： Fumihide Tamura , Izuho Okada , Hideo Wakami , Taketo Toba , Makoto Mizushima , Shigetaka Takamiya , Shinichi Horo , Michiyuki Kono , Manabu Kikuta , Masaki Tezuka , Hiroshi Tanaka , Takao Yokohashi
发明人： Fumihide Tamura , Izuho Okada , Hideo Wakami , Taketo Toba , Makoto Mizushima , Shigetaka Takamiya , Shinichi Horo , Michiyuki Kono , Manabu Kikuta , Masaki Tezuka , Hiroshi Tanaka , Takao Yokohashi
IPC分类号： C08F6/10
CPC分类号： C08J3/12 , C08G65/30 , C08J2371/02
摘要： An object of the present invention is to provide a manufacturing process by which a pellet-shaped nonionic alkylene oxide resin can be obtained in a manner which is excellent in stability, economical efficiency and productivity and easy, wherein the pellet-shaped nonionic alkylene oxide resin, as a high-molecular material useful in a variety of applications, has a suitable molecular weight Mw and physical properties and is also excellent in the stability of the physical properties and further is also excellent in the handling property after the manufacture. As a means of achieving this object, the process for manufacturing a pellet-shaped nonionic alkylene oxide resin, according to the present invention, comprises the steps of: obtaining a nonionic alkylene oxide resin having fluidity by volatilizing a solvent from a nonionic alkylene oxide resin solution obtained in advance by solution polymerization; and then pelletizing the nonionic alkylene oxide resin having fluidity.
摘要翻译：本发明的目的是提供一种以稳定性，经济效率和生产率优异的方式获得丸状非离子环氧烷烃树脂的制备方法，其中颗粒状非离子环氧烷树脂作为可用于各种应用的高分子材料，具有合适的分子量Mw和物理性质，并且物理性能的稳定性也优异，并且在制造后的处理性也优异。作为实现该目的的手段，根据本发明的颗粒状非离子性环氧烷烃树脂的制造方法包括以下步骤：通过使来自非离子性环氧烷树脂的溶剂挥发而获得具有流动性的非离子环氧烷烃树脂溶液聚合预先得到的溶液; 然后造粒具有流动性的非离子环氧烷烃树脂。

4. 发明申请

US20050245410A1 Water soluble nonionic alkylene oxide resin, and production process therefor 审中-公开
标题翻译：水溶性非离子环氧烷树脂及其制备方法
公开(公告)号：US20050245410A1
公开(公告)日：2005-11-03
申请号：US11061893
申请日：2005-02-18
申请人： Masaki Tezuka , Hiroshi Tanaka , Takao Yokohashi , Takao Nishihata , Manabu Kikuta , Michiyuki Kono , Tetsuya Higashizaki , Kazuo Takei , Taketo Toba , Toshiaki Kuriyama , Izuho Okada , Fumihide Tamura , Ritsuo Kitada , Shigetaka Takamiya , Jun Iwamura , Takanori Murakami , Hiromoto Katsuyama , Teruki Matsushita
发明人： Masaki Tezuka , Hiroshi Tanaka , Takao Yokohashi , Takao Nishihata , Manabu Kikuta , Michiyuki Kono , Tetsuya Higashizaki , Kazuo Takei , Taketo Toba , Toshiaki Kuriyama , Izuho Okada , Fumihide Tamura , Ritsuo Kitada , Shigetaka Takamiya , Jun Iwamura , Takanori Murakami , Hiromoto Katsuyama , Teruki Matsushita
IPC分类号： B29B9/04 , C08G65/30 , C08G65/46 , C08J3/12 , C08L71/02 , C11D17/00
CPC分类号： C08J3/12 , B29B9/04 , C08G65/30 , C08J2371/00 , C08L71/02
摘要： The residual amount of a solvent in a water soluble nonionic alkylene oxide resin is decreased in an apparatus including an evaporation vessel and a stirring blade which scrapes-up and coats resin solution onto the inner wall surface of the evaporation vessel. A water soluble nonionic alkylene oxide resin having a crystallization temperature of 10 to 60° C. is extruded to a predetermined thickness in a molten state, the extruded molten resin is brought into contact with a metal surface which is at the crystallization temperature (Tc) or lower, and the thereby solidified resin may be cut into pellets. The resin pellets preferably are of rectangular shape and prescribed dimensions. The resin may be pulverized in a pulverizer by shearing force between a rotary blade and a fixed blade. In the pulverizer, grains smaller than a predetermined size pass through the screen, while larger grains are again pulverized.
摘要翻译：在包括蒸发容器和搅拌叶片的装置中，水溶性非离子环氧烷烃树脂中的溶剂的残留量减少，所述搅拌叶片刮擦并将树脂溶液涂覆在蒸发容器的内壁表面上。将结晶温度为10〜60℃的水溶性非离子性环氧烷树脂在熔融状态下挤出至规定厚度，使熔融树脂与结晶化温度（Tc）的金属表面接触，或更低，并且由此固化的树脂可以切成颗粒。树脂颗粒优选为矩形形状和规定尺寸。树脂可以通过旋转叶片和固定叶片之间的剪切力在粉碎机中粉碎。在粉碎机中，小于预定尺寸的颗粒通过筛网，而较大的颗粒再次被粉碎。

5. 发明申请

US20050197485A1 Process for production of ethylene oxide copolymer 审中-公开
标题翻译：生产环氧乙烷共聚物的方法
公开(公告)号：US20050197485A1
公开(公告)日：2005-09-08
申请号：US11051168
申请日：2005-02-05
申请人： Koichiro Saeki , Kazuo Takei , Toshiaki Kuriyama , Masashi Yukitake , Taketo Toba , Makoto Mizushima , Michiyuki Kono , Manabu Kikuta , Masahito Nishiura
发明人： Koichiro Saeki , Kazuo Takei , Toshiaki Kuriyama , Masashi Yukitake , Taketo Toba , Makoto Mizushima , Michiyuki Kono , Manabu Kikuta , Masahito Nishiura
IPC分类号： C08G65/02 , C08G18/48 , C08G65/08 , C08G65/14 , C08G65/26 , C08G65/34
CPC分类号： C08G65/2696 , C08G18/4837 , C08G65/08
摘要： An object of the present invention is to provide a process which can produce, easily and with good productivity and reproducibility, an ethylene oxide copolymer provided with desired compositional ratios of monomers and a desired molecular weight and further with a desired melting point. As a means of achieving this object, a process according to the present invention for production of an ethylene oxide copolymer is a process comprising a step of polymerizing a monomer mixture including ethylene oxide as a main component, thereby producing the ethylene oxide copolymer, with the process being characterized in that the polymerization step includes at least one step each of the following steps: a step in which only the ethylene oxide is supplied to thus polymerize it; and a step in which the ethylene oxide and another monomer are supplied to thus polymerize them.
摘要翻译：本发明的一个目的是提供一种可以制备具有期望组成比的单体和所需分子量并进一步具有所需熔点的环氧乙烷共聚物，能够容易地且具有良好的生产率和再现性的方法。作为实现该目的的手段，根据本发明的环氧乙烷共聚物的制造方法是包括使包含环氧乙烷作为主要成分的单体混合物聚合的步骤，从而制备环氧乙烷共聚物，方法的特征在于聚合步骤包括以下步骤中的至少一个步骤：仅供给环氧乙烷以使其聚合的步骤; 并且提供环氧乙烷和其它单体从而聚合它们的步骤。

6. 发明授权

US07354984B2 Method for drying nonionic alkylene oxide-type water-soluble resin, method for packaging it, and method for transporting it 有权
标题翻译：非离子环氧烷型水溶性树脂的干燥方法，包装方法及其运送方法
公开(公告)号：US07354984B2
公开(公告)日：2008-04-08
申请号：US11062151
申请日：2005-02-18
申请人： Michiyuki Kono , Manabu Kikuta , Masaki Tezuka , Hiroshi Tanaka , Takao Yokohashi , Takao Nishihata , Kazuhiko Murata , Taketo Toba , Fumihide Tamura , Ritsuo Kitada
发明人： Michiyuki Kono , Manabu Kikuta , Masaki Tezuka , Hiroshi Tanaka , Takao Yokohashi , Takao Nishihata , Kazuhiko Murata , Taketo Toba , Fumihide Tamura , Ritsuo Kitada
IPC分类号： C08G18/08
CPC分类号： C08G65/30 , Y10T428/1348
摘要： To efficiently dry it, a nonionic alkylene oxide-type water-soluble resin is put into a container, then the container is degassed to a prescribed vacuum degree which is maintained while a dry gas having a dew point not higher than prescribed is introduced into the container at a rate not lower than prescribed. Minor volatiles are efficiently removed from the resin in an evaporation tank having a stirring blade. For protecting the dried resin from water, a dry gas is introduced into and air is purged from an empty packaging container whereafter the resin is charged into the container is sealed. By controlling solvent content and visocity of the resin and loading it into a temperature-controlled transportation container and/or unloading it out of the transportation container by the use of a pump, good subsquent processability of the resin and prevention of deterioration thereof are ensured.
摘要翻译：为了有效地将其干燥，将非离子型环氧烷烃型水溶性树脂放入容器中，然后将容器脱气到规定的真空度，将具有不高于露点的干燥气体导入到容器以不低于规定的速度。在具有搅拌叶片的蒸发罐中有效地从树脂中除去少量挥发物。为了将干燥的树脂从水中保护，将干燥的气体引入空气中并从空的包装容器中清除空气，然后将树脂装入容器中进行密封。通过控制树脂的溶剂含量和粘度，并将其装载到温度控制的运输容器中和/或通过使用泵将其卸载出运输容器，确保树脂的良好的加工性和防止其变质。

7. 发明申请

US20050211956A1 Method for drying nonionic alkylene oxide-type water-soluble resin, method for packaging it, and method for transporting it 有权
标题翻译：非离子环氧烷型水溶性树脂的干燥方法，包装方法及其运送方法
公开(公告)号：US20050211956A1
公开(公告)日：2005-09-29
申请号：US11062151
申请日：2005-02-18
申请人： Michiyuki Kono , Manabu Kikuta , Masaki Tezuka , Hiroshi Tanaka , Takao Yokohashi , Takao Nishihata , Kazuhiko Murata , Taketo Toba , Fumihide Tamura , Ritsuo Kitada
发明人： Michiyuki Kono , Manabu Kikuta , Masaki Tezuka , Hiroshi Tanaka , Takao Yokohashi , Takao Nishihata , Kazuhiko Murata , Taketo Toba , Fumihide Tamura , Ritsuo Kitada
IPC分类号： C08G65/02 , C08G65/30 , C08G65/34 , C08G65/46 , C11D17/00
CPC分类号： C08G65/30 , Y10T428/1348
摘要： To efficiently dry it, a nonionic alkylene oxide-type water-soluble resin is put into a container, then the container is degassed to a prescribed vacuum degree which is maintained while a dry gas having a dew point not higher than prescribed is introduced into the container at a rate not lower than prescribed. Minor volatiles are efficiently removed from the resin in an evaporation tank having a stirring blade. For protecting the dried resin from water, a dry gas is introduced into and air is purged from an empty packaging container whereafter the resin is charged into the container is sealed. By controlling solvent content and visocity of the resin and loading it into a temperature-controlled transportation container and/or unloading it out of the transportation container by the use of a pump, good subsquent processability of the resin and prevention of deterioration thereof are ensured.
摘要翻译：为了有效地将其干燥，将非离子型环氧烷烃型水溶性树脂放入容器中，然后将容器脱气到规定的真空度，将具有不高于露点的干燥气体导入到容器以不低于规定的速度。在具有搅拌叶片的蒸发罐中有效地从树脂中除去少量挥发物。为了将干燥的树脂从水中保护，将干燥的气体引入空气中并从空的包装容器中清除空气，然后将树脂装入容器中进行密封。通过控制树脂的溶剂含量和粘度，并将其装载到温度控制的运输容器中和/或通过使用泵将其卸载出运输容器，确保树脂的良好的加工性和防止其变质。

8. 发明申请

US20110287325A1 METHOD FOR PREPARING AN ELECTROCHEMICAL CELL HAVING A GEL ELECTROLYTE 有权
标题翻译：用于制备具有凝胶电解质的电化学细胞的方法
公开(公告)号：US20110287325A1
公开(公告)日：2011-11-24
申请号：US12921453
申请日：2009-03-05
申请人： Karim Zaghib , Manabu Kikuta , Martin Dontigny , Abdelbas Guerfi , Michiyuki Kono
发明人： Karim Zaghib , Manabu Kikuta , Martin Dontigny , Abdelbas Guerfi , Michiyuki Kono
IPC分类号： H01M10/056 , H01M4/525 , H01M10/04 , H01M4/583 , H01M4/485 , H01M4/505 , H01M4/40
CPC分类号： H01M10/0565 , H01G11/56 , H01M2300/0085 , Y02E60/12 , Y02E60/13
摘要： The invention relates to a method for manufacturing an electrochemical cell comprising an anode and a cathode separated by a separator and a gel electrolyte. The method comprises the steps of assembling the electrodes and the separator, and injecting a liquid electrolyte composition between the electrodes, the liquid electrolyte composition comprising a polymer, an aprotic liquid solvent and a lithium salt, wherein the polymer in the liquid electrolyte composition has functional groups capable of polymerizing via cationic polymerization, and the cell is submitted to an electrochemical cycling comprising a charging step and a discharging step.
摘要翻译：本发明涉及一种用于制造电化学电池的方法，所述电化学电池包括由隔膜和凝胶电解质分离的阳极和阴极。该方法包括以下步骤：组装电极和分离器，以及在电极之间注入液体电解质组合物，该液体电解质组合物包含聚合物，非质子液体溶剂和锂盐，其中液体电解质组合物中的聚合物具有功能能够通过阳离子聚合聚合的基团，并且电池进行包括充电步骤和放电步骤的电化学循环。

9. 发明申请

US20120115037A1 POLYMER GEL ELECTROLYTE AND POLYMER SECONDARY BATTERY USING SAME 审中-公开
标题翻译：聚合物凝胶电解质和聚合物二次电池使用相同
公开(公告)号：US20120115037A1
公开(公告)日：2012-05-10
申请号：US13382851
申请日：2009-07-09
申请人： Yasutaka Kono , Koji Utsugi , Hiroshi Kobayashi , Hitoshi Ishikawa , Manabu Kikuta , Michiyuki Kono
发明人： Yasutaka Kono , Koji Utsugi , Hiroshi Kobayashi , Hitoshi Ishikawa , Manabu Kikuta , Michiyuki Kono
IPC分类号： H01M10/056
CPC分类号： H01M10/0565 , H01G11/56 , H01M4/485 , H01M4/587 , H01M10/052 , H01M10/0567 , H01M10/0568 , H01M10/0569 , H01M2300/0085 , Y02E60/13
摘要： The present invention provides a polymer gel electrolyte capable of inhibiting the cell expansion of a polymer secondary battery and improving the cycle characteristics and high-temperature storage characteristics of a polymer secondary battery. The present invention relates to a polymer gel electrolyte comprising an aprotic solvent; a supporting salt; a cyclic sulfonic acid ester which includes at least two sulfonyl groups; and a crosslinked polymer obtained by crosslinking a methacrylic acid ester polymer represented by general formula (1) below. In the general formula (1), n meets 1800
摘要翻译：本发明提供能够抑制聚合物二次电池的电池膨胀并提高聚合物二次电池的循环特性和高温保存特性的聚合物凝胶电解质。本发明涉及包含非质子溶剂的聚合物凝胶电解质; 支持盐包括至少两个磺酰基的环状磺酸酯; 和通过下述通式（1）表示的甲基丙烯酸酯聚合物交联得到的交联聚合物。在通式（1）中，n满足1800

10. 发明申请

US20080041438A1 Photoelectric conversion device 审中-公开
标题翻译：光电转换装置
公开(公告)号：US20080041438A1
公开(公告)日：2008-02-21
申请号：US11810903
申请日：2007-06-07
申请人： Yasuteru Saito , Manabu Kikuta , Michiyuki Kono
发明人： Yasuteru Saito , Manabu Kikuta , Michiyuki Kono
IPC分类号： H01L31/042
CPC分类号： H01G9/2031 , H01G9/2018 , H01G9/2059 , Y02E10/542
摘要： Provided is an inexpensive and high-performance photoelectric conversion device of high practicability. The device comprises a semiconductor electrode, a counter electrode and an electrolyte layer held between the two electrodes, in which the electrolyte layer contains a compound of the following general formula (1) as an oxidation-reduction pair therein: (wherein M+represents an organic or inorganic cation; A represents an aromatic, non-aromatic, heteroaromatic or hetero-non-aromatic cyclic compound).
摘要翻译：提供了一种实用性高的廉价且高性能的光电转换装置。该装置包括半导体电极，对电极和保持在两个电极之间的电解质层，其中电解质层包含下列通式（1）的化合物作为氧化还原对：（其中M < +表示有机或无机阳离子; A表示芳族，非芳族，杂芳族或杂 - 非芳族环状化合物）。

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