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1. 发明授权

US6121336A Surfactants for incorporating silica aerogel in polyurethane foams 失效
标题翻译：用于将二氧化硅气凝胶掺入聚氨酯泡沫中的表面活性剂
公开(公告)号：US6121336A
公开(公告)日：2000-09-19
申请号：US267723
申请日：1994-06-28
申请人： Michael O. Okoroafor , Alan E. Wang , Bulent E. Yoldas
发明人： Michael O. Okoroafor , Alan E. Wang , Bulent E. Yoldas
IPC分类号： C08J9/00
CPC分类号： C08J9/0066 , C08J9/0061 , C08J2375/04 , C08J2483/00
摘要： Polyurethane foams prepared using polysiloxane/polyoxyalkylene surfactants, preferably blended with a viscosity modifying agent, particularly in combination with particulate silica, especially silica aerogel, exhibit improved thermal insulating capacity, as measured by K-factor, and improved closed cell content, without increasing the density of the polyurethane foam.
摘要翻译：使用聚硅氧烷/聚氧化烯表面活性剂制备的聚氨酯泡沫，优选与粘度改进剂共混，特别是与颗粒二氧化硅，特别是二氧化硅气凝胶组合，表现出改善的隔热能力，如通过K因子测量的，并且改善闭孔含量，而不增加聚氨酯泡沫的密度。

2. 发明授权

US5746992A Silica aerogel produced under subcritical conditions 失效
标题翻译：在亚临界条件下生产的二氧化硅气凝胶
公开(公告)号：US5746992A
公开(公告)日：1998-05-05
申请号：US539461
申请日：1995-10-05
申请人： Bulent E. Yoldas , Michael O. Okoroafor
发明人： Bulent E. Yoldas , Michael O. Okoroafor
IPC分类号： C01B33/158
CPC分类号： C01B33/1585
摘要： Liquid comprising from 93 to 100 percent by weight alcohol is removed from silica alcogel at subcritical temperature to produce silica aerogel. The silica aerogel produced by the method of the present invention not only has high porosity, but in most instances it also has a narrow distribution of small pore sizes. The silica aerogel is preferably reduced in size so as to form particulate silica aerogel.
摘要翻译：在亚临界温度下从二氧化硅凝胶上除去包含93-100重量％醇的液体，生成二氧化硅气凝胶。通过本发明的方法制备的二氧化硅气凝胶不仅具有高孔隙率，而且在大多数情况下也具有狭窄的小孔径分布。二氧化硅气凝胶的尺寸优选减小以形成颗粒状二氧化硅气凝胶。

3. 发明授权

US5691392A Stable particulate dispersions 失效
标题翻译：稳定的颗粒分散体
公开(公告)号：US5691392A
公开(公告)日：1997-11-25
申请号：US795736
申请日：1997-02-05
申请人： Michael O. Okoroafor , William H. McDonald , Alan E. Wang
发明人： Michael O. Okoroafor , William H. McDonald , Alan E. Wang
IPC分类号： C08J9/00 , C08G18/00
CPC分类号： C08J9/0066 , C08J9/0023 , C08J2375/04 , Y10S516/01
摘要： A composition comprising a particulate dispersion of from 50% to 98.9% by weight of a siloxane-polyoxyalkylene copolymer surfactant, from 1% to 49.9% by weight of a nonionic organic surfactant other than the siloxane-polyoxyalkylene copolymer surfactant and from 0.1% to 25% by weight, based on the total weight of the composition, of a particulate material having a particle size of less than 20 microns, is described. A method of preparing such a composition, and polyurethane and polyisocyanurate foams containing such a composition are also described. The nonionic organic surfactant is preferably an ethoxylated nonylphenol. The particulate material is preferably a hydrophobic precipitated silica. The composition of the invention is useful as an additive in the preparation of rigid polyurethane and polyisocyanurate foams.
摘要翻译：一种组合物，其包含50至98.9重量％的硅氧烷 - 聚氧化烯共聚物表面活性剂，1重量％至49.9重量％的除硅氧烷 - 聚氧化烯共聚物表面活性剂之外的非离子有机表面活性剂和0.1至25重量％描述了基于组合物总重量的重量％的粒径小于20微米的颗粒材料。还描述了制备这种组合物的方法，以及含有这种组合物的聚氨酯和聚异氰脲酸酯泡沫。非离子有机表面活性剂优选为乙氧基化壬基酚。颗粒材料优选为疏水性沉淀二氧化硅。本发明的组合物可用作制备硬质聚氨酯和聚异氰脲酸酯泡沫体中的添加剂。

4. 发明授权

US5753735A Stable particulate dispersions 失效
标题翻译：稳定的颗粒分散体
公开(公告)号：US5753735A
公开(公告)日：1998-05-19
申请号：US876945
申请日：1997-06-16
申请人： Michael O. Okoroafor , William H. McDonald , Alan E. Wang
发明人： Michael O. Okoroafor , William H. McDonald , Alan E. Wang
IPC分类号： C08J9/00 , C08K5/54 , B01J13/00
CPC分类号： C08J9/0066 , C08J9/0023 , C08J2375/04 , Y10S516/01
摘要： A composition comprising a particulate dispersion of from 50% to 98.9% by weight of a siloxane-polyoxyalkylene copolymer surfactant, from 1% to 49.9% by weight of a nonionic organic surfactant other than the siloxane-polyoxyalkylene copolymer surfactant and from 0.1% to 25% by weight, based on the total weight of the composition, of a particulate material having a particle size of less than 20 microns, is described. A method of preparing such a composition, and polyurethane and polyisocyanurate foams containing such a composition are also described. The nonionic organic surfactant is preferably an ethoxylated nonylphenol. The particulate material is preferably a hydrophobic precipitated silica. The composition of the invention is useful as an additive in the preparation of rigid polyurethane and polyisocyanurate foams.
摘要翻译：一种组合物，其包含50至98.9重量％的硅氧烷 - 聚氧化烯共聚物表面活性剂，1重量％至49.9重量％的除硅氧烷 - 聚氧化烯共聚物表面活性剂之外的非离子有机表面活性剂和0.1至25重量％描述了基于组合物总重量的重量％的粒径小于20微米的颗粒材料。还描述了制备这种组合物的方法，以及含有这种组合物的聚氨酯和聚异氰脲酸酯泡沫。非离子有机表面活性剂优选为乙氧基化壬基酚。颗粒材料优选为疏水性沉淀二氧化硅。本发明的组合物可用作制备刚性聚氨酯和聚异氰脲酸酯泡沫的添加剂。

5. 发明授权

US07087698B1 Method of preparing an optical polymerizate 有权
标题翻译：光聚合物的制备方法
公开(公告)号：US07087698B1
公开(公告)日：2006-08-08
申请号：US09695325
申请日：2000-10-25
申请人： Michael O. Okoroafor , Robert A. Smith
发明人： Michael O. Okoroafor , Robert A. Smith
IPC分类号： C08G18/10 , C08G18/32 , C08G18/38 , C08G18/46 , C08G18/72
CPC分类号： C08G18/758 , C08G18/324 , C08G18/3876 , C08G18/7642 , Y10S348/902 , Y10T428/31551
摘要： The present invention is directed to a novel method of preparing a polymerizate, which includes the step of polymerizing a two-component composition, which includes: a first component containing at least one polycyanate reactant having at least two functional groups selected from isocyanate, isothiocyanate and combinations thereof, the polycyanate reactant being the reaction product of: a polythiol monomer having at least two thiol groups; and a polycyanate monomer having at least two functional groups selected from isocyanate, isothiocyanate and combinations thereof; and a second component containing at least one polyamine reactant having at least two functional groups selected from primary amine, secondary amine and combinations thereof. The present invention is also directed to polymerizates prepared according to the method of the present invention. The present invention is further directed to photochromic articles that may be prepared from the polymerizates of the present invention.
摘要翻译：本发明涉及一种制备聚合物的新方法，其包括聚合双组分组合物的步骤，其包括：含有至少一种选自异氰酸酯，异硫氰酸酯和至少两种官能团的聚氰酸酯反应物的第一组分，聚氰酸酯反应物是以下物质的反应产物：具有至少两个硫醇基团的多硫醇单体; 和具有至少两个选自异氰酸酯，异硫氰酸酯及其组合的官能团的聚氰酸酯单体; 和含有至少一种具有至少两个选自伯胺，仲胺及其组合的官能团的多胺反应物的第二组分。本发明还涉及根据本发明的方法制备的聚合物。本发明还涉及可由本发明的聚合物制备的光致变色制品。

6. 发明授权

US07098290B1 Method of preparing an optical polymerizate 有权
标题翻译：光聚合物的制备方法
公开(公告)号：US07098290B1
公开(公告)日：2006-08-29
申请号：US09695332
申请日：2000-10-25
申请人： Michael O. Okoroafor , Robert A. Smith , Rifat Tabakovic , Marvin J. Graham , Robert D. Herold
发明人： Michael O. Okoroafor , Robert A. Smith , Rifat Tabakovic , Marvin J. Graham , Robert D. Herold
IPC分类号： C08G18/10 , C08G18/32 , C08G18/38 , C08G18/46 , C08G18/72
CPC分类号： C08G18/3876 , C08G18/324 , C08G18/4277 , C08G18/758 , C08G18/7642 , C08G18/765 , Y10S348/902 , Y10T428/31551
摘要： The present invention is directed to a novel method of preparing a polymerizate, which includes the step of polymerizing a two-component composition, which includes: a first component containing at least one polycyanate reactant having at least two functional groups selected from isocyanate, isothiocyanate and combinations thereof, the polycyanate reactant being the reaction product of: a polythiol monomer having at least two thiol groups; and a polycyanate monomer having at least two functional groups selected from isocyanate, isothiocyanate and combinations thereof; and a second component containing at least one polyamine reactant having at least two functional groups selected from primary amine, secondary amine and combinations thereof. The molar equivalent ratio of (NCO+NCS) groups from the first component to (—NH2+—NH—) groups from the second component is from 0.5 to 100. The present invention is also directed to polymerizates prepared according to the method of the present invention. The present invention is further directed to photochromic articles that may be prepared from the polymerizates of the present invention.
摘要翻译：本发明涉及一种制备聚合物的新方法，其包括聚合双组分组合物的步骤，其包括：含有至少一种具有至少两个选自异氰酸酯，异硫氰酸酯的官能团的聚氰酸酯反应物的第一组分和聚氰酸酯反应物是以下物质的反应产物：具有至少两个硫醇基团的多硫醇单体; 和具有至少两个选自异氰酸酯，异硫氰酸酯及其组合的官能团的聚氰酸酯单体; 和含有至少一种具有至少两个选自伯胺，仲胺及其组合的官能团的多胺反应物的第二组分。来自第二组分的来自第一组分的（NCO + NCS）基团与（-NH 2 N + N - NH-）基团的摩尔当量比为0.5至100.本发明还涉及根据本发明的方法制备的聚合物。本发明还涉及可由本发明的聚合物制备的光致变色制品。

7. 发明授权

US06631021B2 Polyfunctional thiirane compounds 失效
公开(公告)号：US06631021B2
公开(公告)日：2003-10-07
申请号：US09793886
申请日：2001-02-28
申请人： Robert A. Smith , Michael O. Okoroafor , Marvin J. Graham
发明人： Robert A. Smith , Michael O. Okoroafor , Marvin J. Graham
IPC分类号： C08G7532
CPC分类号： C07D331/02
摘要： Describes novel polyfunctional thiiranes. Also described are polymerizable compositions comprising such novel polyfunctional thiiranes, and polymerizates, e.g., optical lenses, prepared therefrom. The described polymerizates may have a refractive index of at least 1.6, and an Abbe number of at least 27.

8. 发明授权

US06342571B1 High refractive index optical resin composition 失效
$High refractive index optical resin composition$
标题翻译：高折射率光学树脂组合物
公开(公告)号：US06342571B1
公开(公告)日：2002-01-29
申请号：US09377805
申请日：1999-08-20
申请人： Robert A. Smith , Michael O. Okoroafor , Robert D. Herold , T. Edwin Freeman
发明人： Robert A. Smith , Michael O. Okoroafor , Robert D. Herold , T. Edwin Freeman
IPC分类号： C08F22020
CPC分类号： C08F222/24
摘要： Polymerizable compositions comprising: (a) a mixture of thio(meth)acrylate functional monomers comprising, (a)(i) a first thio(meth)acrylate functional monomer, e.g., bis(thiomethacrylate)-1,2-ethylene, and (a)(ii) a second thio(meth)acrylate functional monomer, which is chain extended; (b) an aromatic monomer having at least two vinyl groups, e.g., divinyl benzene; (c) a polythiol monomer having at least two thiol groups, e.g., pentaerythritol tetrakis(3-mercaptopropionate); and (d) a comonomer selected from, (d)(i) an anhydride monomer having at least one ethylenically unsaturated group, e.g., methacrylic anhydride; (d) (ii) a monomer having at least three (meth)acryloyl groups, e.g., pentaerythritol tetrakis(acrylate); and (d)(iii) mixtures of monomers (d)(i) and (d)(ii). A polymerizate of the polymerizable composition has a refractive index of at least 1.57 and an Abbe number of at least 33.
摘要翻译：可聚合组合物包括：（a）硫代（甲基）丙烯酸酯官能单体的混合物，其包含（a）（i）第一硫代（甲基）丙烯酸酯官能单体，例如双（硫代甲基丙烯酸酯）-1,2-亚乙基和（ a）（ii）链延伸的第二硫代（甲基）丙烯酸酯官能单体; （b）具有至少两个乙烯基的芳族单体，例如二乙烯基苯; （c）具有至少两个硫醇基的多硫醇单体，例如季戊四醇四（3-巯基丙酸酯）; 和（d）选自（d）（i）具有至少一个烯属不饱和基团的酸酐单体的共聚单体，例如甲基丙烯酸酐; （d）（ii）具有至少三个（甲基）丙烯酰基的单体，例如季戊四醇四（丙烯酸酯）; 和（d）（iii）单体（d）（i）和（d）（ii）的混合物。聚合性组合物的聚合物的折射率为至少1.57，阿贝数为33以上。

9. 发明授权

US5976422A Optical resin composition 失效
标题翻译：光学树脂组合物
公开(公告)号：US5976422A
公开(公告)日：1999-11-02
申请号：US37108
申请日：1998-03-09
申请人： Michael O. Okoroafor , Robert D. Herold , Robert A. Smith
发明人： Michael O. Okoroafor , Robert D. Herold , Robert A. Smith
IPC分类号： C08G75/04 , G02B5/23
CPC分类号： C08G75/045 , G02B5/23
摘要： Describes a polymerizable organic composition comprising at least one polymerizable monomer having at least two ethylenically unsaturated groups, e.g., divinyl benzene, and a polythiol monomer represented by the following general formula, ##STR1## wherein R.sub.1 and R.sub.2 are each selected from the group consisting of straight or branched chain alkylene, e.g., methylene or ethylene, cyclic alkylene, phenylene and C.sub.1 -C.sub.9 alkyl substituted phenylene. Optionally, a monoethylenically unsaturated monomer, e.g., phenoxyethyl methacrylate, and/or an anhydride monomer, e.g., methacrylic anhydride, may also be present. Polymerizates prepared from polymerizable organic compositions of the present invention have a refractive index of at least 1.57, an Abbe number of at least 33 and an initial Barcol hardness of at least 1. Also described are photochromic articles prepared from such compositions.
摘要翻译：描述了包含至少一种具有至少两个烯键式不饱和基团的可聚合单体的可聚合有机组合物，例如二乙烯基苯和由以下通式表示的多硫醇单体，其中R 1和R 2各自选自直链或支链链亚烷基，例如亚甲基或亚乙基，环状亚烷基，亚苯基和C 1 -C 9烷基取代的亚苯基。任选地，也可以存在单烯属不饱和单体，例如甲基丙烯酸苯氧基乙酯和/或酸酐单体，例如甲基丙烯酸酐。由本发明的可聚合有机组合物制备的聚合物具有至少1.57的折射率，至少33的阿贝数和至少为1的初始巴醇硬度。还描述了由这些组合物制备的光致变色制品。

10. 发明申请

US20090036639A1 Post-Processing of Polylactic Acid Article 审中-公开
标题翻译：聚乳酸后处理
公开(公告)号：US20090036639A1
公开(公告)日：2009-02-05
申请号：US12181415
申请日：2008-07-29
申请人： Qiuchen Peter Zhang , Michael O. Okoroafor , Xiaoyan Huang , Stuart Michael Ruan Jones , Philip Andrew Dent , Claire Louise Gould
发明人： Qiuchen Peter Zhang , Michael O. Okoroafor , Xiaoyan Huang , Stuart Michael Ruan Jones , Philip Andrew Dent , Claire Louise Gould
IPC分类号： C08G63/08
CPC分类号： A47J31/06 , B29C49/0005 , B29C51/002 , B29C71/02 , C08J7/08 , C08J2367/04
摘要： Methods are provided for making a polylactic acid article. The methods may include the steps of providing an article comprising polylactic acid; supporting the article using a carrier support system; and curing the article with heat. The step of curing the article is effective to improve one or more properties of the article. Articles comprising polylactic acid also are provided having improved properties. Methods also are provided for preparing a beverage including the steps of providing a pod comprising polylactic acid, wherein the pod has been cured with heat while being supported by a carrier support system; placing a beverage material in the pod; placing a hot liquid into the pod; brewing the beverage material and hot liquid in the pod to create a beverage; and removing the beverage from the pod.
摘要翻译：提供制备聚乳酸制品的方法。所述方法可以包括提供包含聚乳酸的制品的步骤; 使用运营商支持系统支持文章; 并用热量固化物品。固化该制品的步骤对于改善制品的一种或多种性质是有效的。提供包含聚乳酸的制品具有改进的性能。提供了用于制备饮料的方法，包括以下步骤：提供包含聚乳酸的荚，其中所述荚已经被热固化，同时由载体支撑系统支撑; 将饮料材料放入荚中; 将热液放入荚内; 在饮料袋中冲泡饮料和热液体以形成饮料; 以及从所述荚中去除所述饮料。

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