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1. 发明授权

US06538102B1 Method for producing sulfur-containing polymers 失效
标题翻译：含硫聚合物的生产方法
公开(公告)号：US06538102B1
公开(公告)日：2003-03-25
申请号：US09623327
申请日：2001-01-11
申请人： Michael Haubs , Reinhard Wagener , Markus Lehrl
发明人： Michael Haubs , Reinhard Wagener , Markus Lehrl
IPC分类号： C08G7514
CPC分类号： C08G75/025 , C08G75/0254
摘要： The present invention relates to a process for preparing sulfur-containing polymers from at least one sulfide and from at least one aromatic dihalogen compound in at least one solvent, where a) a mixture made from a sulfide and from a solvent is prepared in a first reaction vessel, b) the sulfide and an aromatic dihalogen compound react in a second reaction vessel to form a sulfur-containing polymer, c) the pressure in the second reaction vessel is to some extent or completely released during the reaction, and the emanating vapor mixture is brought into contact with the mixture prepared in step (a).
摘要翻译：本发明涉及一种由至少一种硫化物和至少一种芳族二卤化合物在至少一种溶剂中制备含硫聚合物的方法，其中a）由硫化物和溶剂制成的混合物在第一反应容器，b）硫化物和芳族二卤化合物在第二反应容器中反应以形成含硫聚合物，c）第二反应容器中的压力在一定程度上或在反应期间完全释放，并且发出的蒸汽使混合物与步骤（a）中制备的混合物接触。

2. 发明授权

US06818132B2 Method and device for separating solids from a liquid phase 有权
标题翻译：从液相中分离固体的方法和装置
公开(公告)号：US06818132B2
公开(公告)日：2004-11-16
申请号：US10168269
申请日：2002-10-01
申请人： Michael Haubs , Reinhard Wagener
发明人： Michael Haubs , Reinhard Wagener
IPC分类号： B01D1102
CPC分类号： B01D12/00 , B01D2011/002 , F26B5/005
摘要： The present invention relates to a process and an apparatus for separating separating polymeric from one or more by-products of preparation of the polymer and a first liquid phase, wherein the solid in a first liquid phase is brought into contact with a second liquid phase and the solid is transferred into the second liquid phase. The solid is washed in countercurrent and at least partial displacement washing takes place during the washing of the solid.
摘要翻译：本发明涉及用于将聚合物与聚合物的制备和第一液相的一种或多种副产物分离的方法和装置，其中第一液相中的固体与第二液相接触，将固体转移到第二液相中。将固体以逆流方式洗涤，并且在洗涤固体期间发生至少部分置换洗涤。

3. 发明申请

US20090200153A1 Method for producing and dehydrating cyclic formals 审中-公开
标题翻译：生产和脱水循环甲醛的方法
公开(公告)号：US20090200153A1
公开(公告)日：2009-08-13
申请号：US11665047
申请日：2005-10-06
申请人： Reinhard Wagener , Michael Haubs , Juergen Lingnau , Matthias Göring , Michael Hoffmockel
发明人： Reinhard Wagener , Michael Haubs , Juergen Lingnau , Matthias Göring , Michael Hoffmockel
IPC分类号： B01D61/36
CPC分类号： B01D61/362 , B01D53/22 , C07D317/12
摘要： Processes are described which comprise: (a) providing a mixture comprising a cyclic formal and water, wherein the mixture has a cyclic formal concentration and a water concentration; (b) bringing the mixture into contact with an aqueously selective membrane; (c) creating a pressure differential across the membrane; and (d) obtaining a permeate having a higher water concentration and a lower cyclic formal concentration than the mixture, and a retentate having a lower water concentration and a higher cyclic formal concentration than the mixture.
摘要翻译：描述了方法，其包括：（a）提供包含环状缩甲醛和水的混合物，其中所述混合物具有环形形式浓度和水浓度; （b）使混合物与高选择性的膜接触; （c）跨过膜产生压力差; 和（d）获得具有比混合物更高的水浓度和较低的环状甲醛浓度的渗透物，以及具有比混合物低的水浓度和较高的环状甲醛浓度的滞留物。

4. 发明授权

US5894072A Process for preparing aromatic sulfur-containing polymers 失效
标题翻译：芳香族含硫聚合物的制备方法
公开(公告)号：US5894072A
公开(公告)日：1999-04-13
申请号：US822112
申请日：1997-03-21
申请人： Michael Haubs , Reinhard Wagener
发明人： Michael Haubs , Reinhard Wagener
IPC分类号： C08G75/0254 , C08G75/14
CPC分类号： C08G75/0254
摘要： In a process for preparing aromatic sulfur-containing polymers, the polymer is formed from a prepolymer having halogen end groups. During preparation of the prepolymers, an alkali equivalent and a sulfur equivalent in a ratio of 0.5 to 1:1 is employed in the reaction mixture. The two-step process is particularly suitable for preparing polyphenylene sulfide.
摘要翻译：在制备芳族含硫聚合物的方法中，聚合物由具有卤素端基的预聚物形成。在制备预聚物期间，在反应混合物中使用碱当量和硫当量比为0.5:1:1。两步法特别适用于制备聚苯硫醚。

5. 发明申请

US20080272052A1 Method for Producing and Dewatering Cyclic Formals 审中-公开
标题翻译：循环形式的生产和脱水方法
公开(公告)号：US20080272052A1
公开(公告)日：2008-11-06
申请号：US11665028
申请日：2005-10-06
申请人： Reinhard Wagener , Michael Haubs , Juergen Lingnau , Matthias Goring , Michael Hoffmockel
发明人： Reinhard Wagener , Michael Haubs , Juergen Lingnau , Matthias Goring , Michael Hoffmockel
IPC分类号： B01D61/36 , C07D317/12
CPC分类号： B01D61/362 , B01D53/22 , C07D317/12
摘要： Processes are described which comprise: (a) providing a mixture comprising a cyclic formal and water, wherein the mixture has a cyclic formal concentration and a water concentration; (b) bringing the mixture into contact with an organically selective membrane; (c) creating a pressure differential across the membrane; and (d) obtaining a permeate having a lower water concentration and a higher cyclic formal concentration than the mixture, and a retentate having a higher water concentration and a lower cyclic formal concentration than the mixture.
摘要翻译：描述了方法，其包括：（a）提供包含环状缩甲醛和水的混合物，其中所述混合物具有环形形式浓度和水浓度; （b）使混合物与有机选择性膜接触; （c）跨过膜产生压力差; 和（d）获得具有比混合物低的水浓度和较高的环状甲醛浓度的渗透物，以及具有比混合物更高的水浓度和更低的环状甲醛浓度的渗余物。

6. 发明授权

US06350852B1 Process for producing sulfur-containing polymers by polymerizing prepolymers and monomers 有权
标题翻译：通过聚合预聚物和单体生产含硫聚合物的方法
公开(公告)号：US06350852B1
公开(公告)日：2002-02-26
申请号：US09202255
申请日：1999-02-10
申请人： Michael Haubs , Reinhard Wagener
发明人： Michael Haubs , Reinhard Wagener
IPC分类号： C08G7502
CPC分类号： C08G75/0254
摘要： The process for preparing sulfur-containing polymers, in particular polyarylene sulfides, from at least one sulfide and at least one aromatic dihalogen compound, in a solvent, is carried out in the steps: a) a mixture of aromatic dihalogen compound and sulfide is polymerized, b) aromatic dihalogen compound and sulfide are added to the polymerized mixture and c) the reaction mixture is polymerized further. The sulfur-containing polymers prepared by the process are distinguished by high purity and good mechanical properties.
摘要翻译：在溶剂中由至少一种硫化物和至少一种芳族二卤化合物制备含硫聚合物，特别是聚亚芳基硫醚的方法，是在以下步骤中进行：a）将芳族二卤化合物与硫化物的混合物聚合，b）将芳族二卤化合物和硫化物加入聚合的混合物中，c）进一步聚合反应混合物。通过该方法制备的含硫聚合物的特征在于高纯度和良好的机械性能。

7. 发明授权

US5905137A Process for preparing sulfur-containing polymers 失效
标题翻译：制备含硫聚合物的方法
公开(公告)号：US5905137A
公开(公告)日：1999-05-18
申请号：US752060
申请日：1996-11-19
申请人： Michael Haubs , Reinhard Wagener , Afif Nesheiwat
发明人： Michael Haubs , Reinhard Wagener , Afif Nesheiwat
IPC分类号： C08G75/02 , C08G75/14
CPC分类号： C08G75/0254
摘要： The present invention relates to a process for preparing sulfur-containing polymers from at least one sulfide and at least one aromatic dihalo compound in a solvent, which comprisesa) reacting the sulfide with a stoichiometric excess of aromatic dihalo compound,b) largely removing the excess aromatic dihalo compound andc) further polymerizing the mixture.
摘要翻译：本发明涉及一种在溶剂中由至少一种硫化物和至少一种芳族二卤代化合物制备含硫聚合物的方法，该方法包括：a）使硫化物与化学计量过量的芳族二卤代化合物反应，b）过量的芳族二卤化合物和c）进一步聚合该混合物。

8. 发明授权

US06874644B1 Method of and appliance for material separation 失效
标题翻译：材料分离方法和用具
公开(公告)号：US06874644B1
公开(公告)日：2005-04-05
申请号：US09936752
申请日：2000-03-17
申请人： Reinhard Wagener , Michael Haubs
发明人： Reinhard Wagener , Michael Haubs
IPC分类号： B03B5/28 , B01D11/02 , B01J8/00 , B01J8/40 , B03B5/66 , B01D11/04
CPC分类号： B01D11/0246 , B01J8/007 , B01J8/40
摘要： The invention relates to a method of material separation, in which a material, which comprises at least a first material component and a second material component, is introduced, together with a washing fluid, into a container with at least one sedimentation chamber and is subjected to a gravitational field, under influence of the gravitational field in the sedimentation chamber, the first material component is enriched in a sedimentation zone, which is bounded by a base, and the material with the enriched first material component is evacuated from the sedimentation zone via an opening in the base, the material with the enriched first material component being evacuated as a sediment film through the opening in the base, washing fluid flowing transversely onto the sediment film and the washing fluid flowing through the sediment film and, in the process, an at least partial displacement of the remaining second material component taking place from the sediment film. The invention further relates to an appliance, in particular for carrying out the method.
摘要翻译：本发明涉及一种材料分离方法，其中包括至少第一材料组分和第二材料组分的材料与洗涤流体一起被引入具有至少一个沉降室的容器中，并且经受在重力场中，在沉淀室中的重力场的影响下，第一材料成分富集沉积区，其由碱形成，并且具有富集的第一材料成分的材料经由沉淀区经由在基部的开口部分，将富集的第一材料成分的材料通过底部的开口作为沉淀物膜排出，洗涤流体横向流动到沉积物膜上，洗涤流体流过沉积物膜，剩余的第二材料组分至少部分地从沉淀膜中移出。本发明还涉及一种器具，特别是用于实施该方法。

9. 发明授权

US06734282B1 Method and device for separating solids from polymer solutions 有权
标题翻译：从聚合物溶液中分离固体的方法和装置
公开(公告)号：US06734282B1
公开(公告)日：2004-05-11
申请号：US09958365
申请日：2002-01-18
申请人： Reinhard Wagener , Michael Haubs
发明人： Reinhard Wagener , Michael Haubs
IPC分类号： C08F600
CPC分类号： C08G75/0281 , B01D3/24 , B01D21/02 , B01D21/2416 , B01J8/005 , B01J8/007 , C08G75/0213 , C08G75/0254 , C08G75/0277
摘要： The present invention relates to a process for separating a dissolved polymer from solids, wherein the solid is separated off by sedimentation and the sedimented solid is washed in countercurrent with a solvent. The present invention further relates to a process for preparing polymers in a solvent, wherein a) a polymer having a low molecular weight is prepared in solution, b) the solid which is undissolved in the reaction mixture is separated off by sedimentation and c) the mixture which has been freed of the solid is polymerized further until a particular molecular weight has been reached.
摘要翻译：本发明涉及从固体中分离溶解的聚合物的方法，其中通过沉降分离出固体，并将沉淀的固体与溶剂逆流洗涤。本发明还涉及在溶剂中制备聚合物的方法，其中a）在溶液中制备具有低分子量的聚合物，b）在反应混合物中未溶解的固体通过沉降分离，和c）将混合物已经释放出固体，进一步聚合直至达到特定的分子量。

10. 发明申请

US20110077378A1 Oxymethylene Polymers and Process for the Preparation Thereof 有权
标题翻译：亚甲基聚合物及其制备方法
公开(公告)号：US20110077378A1
公开(公告)日：2011-03-31
申请号：US12787698
申请日：2010-05-26
申请人： Michael Haubs , Michael Hoffmockel , Jürgen Lingnau , Robert M. Gronner , Larson Lowell
发明人： Michael Haubs , Michael Hoffmockel , Jürgen Lingnau , Robert M. Gronner , Larson Lowell
IPC分类号： C08G16/00 , C08G65/34
CPC分类号： C08L67/025 , C08G2/06 , C08G2/10 , C08L59/02 , C08L2666/16
摘要： The present invention relates to a process for the preparation of oxymethylene polymers as well as oxymethylene polymers obtainable therefrom. The process includes polymerization of a monomer, which forms —CH2—O— units in the presence of an acetal of formaldehyde or a polyhydric alcohol and an initiator for cationic polymerization. The initiator may be a heteropoly acid or an acid salt thereof which is dissolved in an alkyl ester of a polybasic carboxylic acid.
摘要翻译：本发明涉及一种制备甲醛聚合物的方法以及由其获得的甲醛聚合物。该方法包括在甲醛或多元醇的缩醛和用于阳离子聚合的引发剂的存在下形成-CH 2 -O-单体的单体的聚合。引发剂可以是杂多酸或其酸盐，其溶解在多元羧酸的烷基酯中。

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