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1. 发明申请

US20100040653A1 Intercalated layered silicate 失效
标题翻译：插层式硅酸盐
公开(公告)号：US20100040653A1
公开(公告)日：2010-02-18
申请号：US11667424
申请日：2005-12-02
申请人： Michael D. Grah , Michael L. Becraft , Drew V. Speer , Gary W. Beall , Jeremy Bartels
发明人： Michael D. Grah , Michael L. Becraft , Drew V. Speer , Gary W. Beall , Jeremy Bartels
IPC分类号： A61K9/00 , B32B7/10 , C08K3/34 , A61K8/02 , B65D85/00
CPC分类号： C08K9/04 , C01B33/44 , C08K3/34 , C08K5/06 , C08K5/103 , C08K5/175 , Y10T428/265
摘要： An intercalated layered silicate comprises a layered silicate and an intercalating agent sorbed between the silicate layers of the layered silicate. The amount of intercalating agent is effective to provide an average interlayer spacing between the silicate layers of at least about 20 Å. The intercalating agent has a formula selected from formulas I through VII described herein. The intercalated layered silicate may be exfoliated by mixing it with a matrix medium and adding sufficient energy to form a dispersed-particle composition. A packaging film, such as a food packaging film, may comprise the dispersed-particle composition
摘要翻译：嵌层的层状硅酸盐包括层状硅酸盐和吸附在层状硅酸盐的硅酸盐层之间的嵌入剂。嵌入剂的量有效地提供至少约为的硅酸盐层之间的平均层间距。插层剂具有选自本文所述的式I至VII的式。插层的层状硅酸盐可以通过将其与基质介质混合并加入足够的能量以形成分散颗粒组合物而被剥离。包装膜，例如食品包装膜，可以包含分散颗粒组合物

2. 发明授权

US08568808B2 Intercalated layered silicate 失效
标题翻译：插层式硅酸盐
公开(公告)号：US08568808B2
公开(公告)日：2013-10-29
申请号：US11667424
申请日：2005-12-02
申请人： Michael D. Grah , Michael L. Becraft , Drew V. Speer , Gary W. Beall , Jeremy Bartels
发明人： Michael D. Grah , Michael L. Becraft , Drew V. Speer , Gary W. Beall , Jeremy Bartels
IPC分类号： C04B14/00 , C09C1/28 , C08K3/34 , A61K8/04 , A61K9/10 , C09D11/00 , C10M169/04 , B65D85/72
CPC分类号： C08K9/04 , C01B33/44 , C08K3/34 , C08K5/06 , C08K5/103 , C08K5/175 , Y10T428/265
摘要： An intercalated layered silicate comprises a layered silicate and an intercalating agent sorbed between the silicate layers of the layered silicate. The amount of intercalating agent is effective to provide an average interlayer spacing between the silicate layers of at least about 20 Å. The intercalating agent has a formula selected from formulas I through VII described herein. The intercalated layered silicate may be exfoliated by mixing it with a matrix medium and adding sufficient energy to form a dispersed-particle composition. A packaging film, such as a food packaging film, may comprise the dispersed-particle composition.
摘要翻译：嵌层的层状硅酸盐包括层状硅酸盐和吸附在层状硅酸盐的硅酸盐层之间的嵌入剂。嵌入剂的量有效地提供至少约为的硅酸盐层之间的平均层间距。插层剂具有选自本文所述的式I至VII的式。插层的层状硅酸盐可以通过将其与基质介质混合并加入足够的能量以形成分散颗粒组合物而被剥离。包装膜，例如食品包装膜，可以包含分散颗粒组合物。

3. 发明申请

US20090297568A1 Intercalated layered silicate 审中-公开
标题翻译：插层式硅酸盐
公开(公告)号：US20090297568A1
公开(公告)日：2009-12-03
申请号：US11990734
申请日：2006-08-15
申请人： Michael D. Grah , Michael L. Becraft , Drew V. Speer , Gary W. Beall
发明人： Michael D. Grah , Michael L. Becraft , Drew V. Speer , Gary W. Beall
IPC分类号： A61K8/06 , C08K5/10 , B65D81/00 , B32B9/00
CPC分类号： C01B33/44 , C08K5/10 , C08K9/04 , Y10T428/261
摘要： An intercalated layered silicate comprises a layered silicate and an intercalating agent sorbed between the silicate layers of the layered silicate. The amount of intercalating agent is effective to provide an average interlayer spacing between the silicate layers of at least about 20 Å. The intercalating agent comprises one or more of fatty acid esters of sorbitan, ethoxylated fatty esters of sorbitan, fatty acid esters of glycerol, fatty acid esters of polyglycerol, fatty acid amide waxes, variants of amide waxes, and variants of amides. The intercalated layered silicate may be exfoliated by mixing it with a matrix medium and adding sufficient energy to form a dispersed-particle composition. A packaging film, such as a food packaging film, may comprise the dispersed-particle composition.
摘要翻译：嵌层的层状硅酸盐包括层状硅酸盐和吸附在层状硅酸盐的硅酸盐层之间的嵌入剂。嵌入剂的量有效地提供至少约为的硅酸盐层之间的平均层间距。插层剂包含一种或多种脱水山梨糖醇的脂肪酸酯，脱水山梨醇的乙氧基化脂肪酸酯，甘油的脂肪酸酯，聚甘油的脂肪酸酯，脂肪酸酰胺蜡，酰胺蜡的变体和酰胺的变体。插层的层状硅酸盐可以通过将其与基质介质混合并加入足够的能量以形成分散颗粒组合物而被剥离。包装膜，例如食品包装膜，可以包含分散颗粒组合物。

4. 发明申请

US20090297675A1 Film comprising silicate platelets of exfoliated from phospolipid-intercalated layered silicate 有权
标题翻译：包含从磷脂插层的层状硅酸盐剥离的硅酸盐血小板的膜
公开(公告)号：US20090297675A1
公开(公告)日：2009-12-03
申请号：US11990614
申请日：2006-08-15
申请人： Michael D. Grah , Gary W. Beall
发明人： Michael D. Grah , Gary W. Beall
IPC分类号： B65D81/24 , C08K5/52 , B65D65/40 , C01B33/44
CPC分类号： C01B33/44 , C08K5/10 , C08K9/04 , Y10T428/261
摘要： A packaging film comprises a dispersed-particle composition, which comprises a plurality of particles dispersed in a matrix medium of thermoplastic polymer. The particles comprise silicate platelets. Intercalating agent of one or more phospholipids is sorbed to the silicate platelets.
摘要翻译：包装膜包括分散粒子组合物，其包含分散在热塑性聚合物的基质介质中的多个颗粒。颗粒包括硅酸盐血小板。一种或多种磷脂的插入剂被吸附到硅酸盐血小板上。

5. 发明授权

US08362134B2 Film comprising silicate platelets of exfoliated from phospolipid-intercalated layered silicate 有权
公开(公告)号：US08362134B2
公开(公告)日：2013-01-29
申请号：US11990614
申请日：2006-08-15
申请人： Michael D. Grah , Gary W. Beall
发明人： Michael D. Grah , Gary W. Beall
IPC分类号： C01B33/44 , B65D65/40 , C08K5/52
CPC分类号： C01B33/44 , C08K5/10 , C08K9/04 , Y10T428/261
摘要： A packaging film comprises a dispersed-particle composition, which comprises a plurality of particles dispersed in a matrix medium of thermoplastic polymer. The particles comprise silicate platelets. Intercalating agent of one or more phospholipids is sorbed to the silicate platelets.

6. 发明申请

US20130112925A1 METHOD AND SYSTEM FOR PRODUCING GRAPHENE AND GRAPHENOL 失效
标题翻译：用于生产石墨和石墨烯的方法和系统
公开(公告)号：US20130112925A1
公开(公告)日：2013-05-09
申请号：US13659570
申请日：2012-10-24
申请人： Gary W. Beall
发明人： Gary W. Beall
IPC分类号： C07C37/00
CPC分类号： C07C37/002 , B82Y30/00 , B82Y40/00 , C01B32/184 , C07C2603/54 , C08K5/053 , C07C39/12
摘要： This disclosure includes a process that unexpectedly can produce very inexpensive graphene and a new compound called graphenol in particulate or dispersions in solvents. The process can also produce graphene layers on metallic and nonmetallic substrates. Further, the graphenol and graphene can be utilized to form nanocomposites that yield property improvements exceeding anything reported previously.
摘要翻译：该公开内容包括意外地可以生产非常便宜的石墨烯和称为石墨烯的新化合物的方法，其在溶剂中的颗粒或分散体中。该工艺还可以在金属和非金属基底上生产石墨烯层。此外，可以利用石墨烯和石墨烯来形成纳米复合材料，其产生超过以前报道的任何物质改进。

7. 发明授权

US07772362B2 Treatment method for imparting self-healing and shape memory properties to certain CBDO copolymers 有权
标题翻译：赋予某些CBDO共聚物自我修复和形状记忆性能的处理方法
公开(公告)号：US07772362B2
公开(公告)日：2010-08-10
申请号：US12173186
申请日：2008-07-15
申请人： Gary W. Beall , Jesse R. Hancock , Chad J. Booth
发明人： Gary W. Beall , Jesse R. Hancock , Chad J. Booth
IPC分类号： C08F6/00
CPC分类号： C08G63/88 , C08G63/199
摘要： A method of treating an amorphous CBDO polymer to impart self healing and shape memory properties by heat treatment, and products resulting from such method are described. An amorphous CBDO copolymer may include a copolyester prepared by reacting an aromatic dicarboxylic acid or ester or anhydride thereof, a 2,2,4,4-tetraalkyl-1,3-cyclobutanediol and 1,3-propanediol, 1,4-butanediol, or mixture thereof. The method may include heating said copolymer to a temperature above its glass transition temperature to impart self healing and shape memory properties.
摘要翻译：描述了通过热处理处理无定形CBDO聚合物以赋予自愈和形状记忆特性的方法，并且描述了由这种方法产生的产品。无定形CBDO共聚物可以包括通过使芳族二羧酸或其酯或酸酐，2,2,4,4-四烷基-1,3-环丁二醇和1,3-丙二醇，1,4-丁二醇，或其混合物。该方法可以包括将所述共聚物加热至高于其玻璃化转变温度的温度以赋予自愈合和形状记忆性能。

8. 发明申请

US20090023885A1 TREATMENT METHOD FOR IMPARTING HIGH IMPACT RESISTANCE IN CERTAIN CBDO COPOLYMERS 审中-公开
标题翻译：在某些CBDO共聚物中阻止高抗冲击性的处理方法
公开(公告)号：US20090023885A1
公开(公告)日：2009-01-22
申请号：US12173314
申请日：2008-07-15
申请人： Gary W. Beall , Jesse R. Hancock , Chad J. Booth
发明人： Gary W. Beall , Jesse R. Hancock , Chad J. Booth
IPC分类号： C08G63/16
CPC分类号： C08G63/88 , C08G63/199
摘要： According to the invention, an amorphous CBDO copolymer (as described in U.S. Pat. No. 5,705,575, issued Jan. 6, 1998, which U.S. patent is incorporated herein by reference in its entirety) is treated to impart high impact resistance, also called impact strength.
摘要翻译：根据本发明，处理无定形CBDO共聚物（如美国专利5,705,575（1998年1月6日授权，其全部内容通过引用并入本文作为参考）中所述）以赋予高抗冲击性，也称为冲击强度。

9. 发明授权

US06235533B1 Method of determining the composition of clay deposit 失效
标题翻译：确定粘土沉积物组成的方法
公开(公告)号：US06235533B1
公开(公告)日：2001-05-22
申请号：US09040633
申请日：1998-03-18
申请人： Semeon J. Tsipursky , Don D. Eisenhour , Gary W. Beall , Mark Clarey , James Edwards
发明人： Semeon J. Tsipursky , Don D. Eisenhour , Gary W. Beall , Mark Clarey , James Edwards
IPC分类号： G01N3300
CPC分类号： G01N33/24 , G01N33/383
摘要： A method of determining a quantity of amorphous SiC2-containing impurities in a montmorillonite clay sample comprising the steps of: (a) analyzing the clay sample to determine the weight percent of SiO2 contained in the clay sample; (b) analyzing the clay sample for non-montmorillonite SiO2-containing crystalline components; (c) calculating the weight percent of SiO2 from step (a) that is derived from the montmorillonite and amorphous SiQ2-containing impurities by lowering the weight percent of SiO2 in step (a) based on the non-montmorillonite SiO2-containing crystalline impurities found in step (b); and (d) determining the amorphous SiO2-containing impurity portion of the SiO2 calculated in step (c) by further lowering the amount of SiO2 from step (c) until the amount of montmorillonite-derived SiO2 is consistent with one or more properties of the clay sample, the amount of further lowering being proportional to an amount of amorphous SiO2-containing impurities contained in the clay sample.
摘要翻译：一种测定蒙脱石粘土样品中含无定形SiC 2的杂质的量的方法，包括以下步骤：（a）分析粘土样品以确定粘土样品中所含的SiO 2的重量百分比;（b）分析粘土样品非蒙脱土SiO 2的结晶成分;（c）通过降低步骤（a）中SiO 2的重量百分比来计算源自蒙脱土和含有无定形SiQ 2的杂质的步骤（a）中SiO 2的重量百分比，基于在步骤（b）中发现的非蒙脱石SiO 2结晶杂质; 和（d）通过进一步降低步骤（c）中的SiO 2的量直到由蒙脱石衍生的SiO 2的量与所述SiO 2的一个或多个性质一致来确定在步骤（c）中计算出的SiO 2的无定形SiO 2杂质部分粘土样品，进一步降低的量与粘土样品中所含的无定形SiO 2杂质的量成比例。

10. 发明授权

US5952095A Intercalates and exfoliates formed with long chain (C.sub.10 +) monomeric organic intercalant compounds; and composite materials containing same 失效
标题翻译：由长链（C10 +）单体有机插层剂形成的插层和去角质; 和含有它们的复合材料
公开(公告)号：US5952095A
公开(公告)日：1999-09-14
申请号：US758740
申请日：1996-12-06
申请人： Gary W. Beall , Fernando Serrano , Semeon Tsipursky , Steven J. Engman
发明人： Gary W. Beall , Fernando Serrano , Semeon Tsipursky , Steven J. Engman
IPC分类号： C01B33/44 , C08K7/00 , C08K9/04 , C08L101/00 , C09C1/42 , C09C3/10 , B32B7/00
CPC分类号： C09C1/42 , C01B33/44 , C08K9/04 , C09C3/10 , C01P2002/08 , C01P2002/72 , C01P2002/77 , C01P2004/54 , Y10T428/26
摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer including an alkyl radical having at least 10 carbon atoms and having a dipole moment greater than the dipole moment of water, to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG. (as measured after water removal to a maximum of 5% by weight water), up to about 100 .ANG. and preferably in the range of about 10-45 .ANG., so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix.
摘要翻译：通过使层状材料例如页硅酸盐与包含具有至少10个碳原子的烷基并且具有大于偶极矩的偶极矩的插层单体接触形成的插层，以吸附或插入相邻片晶之间的插入剂单体的分层材料。在相邻的血小板之间吸附足够的嵌入剂单体以将相邻的血小板膨胀至至少约5 ANGSTROM（水除去后测量到最多5％（重量）水）的间隔，最高达约100安培，最好在约10-45安士，使得插入物容易被剥离成单独的血小板。插入的复合物可以与有机液体结合成粘性载体材料，用于递送载体材料或递送活性化合物; 或者插层的复合物可以与基质聚合物组合以形成强的，填充的聚合物基质。

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