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    • 1. 发明授权
    • Preparation of dialkyl (N-cyanoimido)carbonates from dialkyl
imidocarbonates and cyanogen halides
    • 由二烷基亚氨基碳酸酯和氰卤化物制备二烷基(N-氰基亚氨基)碳酸酯
    • US5237084A
    • 1993-08-17
    • US823518
    • 1992-01-21
    • Michael A. OliverWard H. Oliver
    • Michael A. OliverWard H. Oliver
    • C07C271/68
    • C07C271/68
    • Dialkyl (N-cyanoimido) carbonates are prepared in good yield in a non-aqueous solvent by a process which comprises either (a) adding a cyanogen halide at a controlled rate to a reactor containing an unsubstituted or substituted dialkyl imidocarbonate, an inorganic base and/or a trialkyl amine, or (b) by adding a trialkyl amine to a solution of the unsubstituted or substituted dialkyl imidocarbonate and a cyanogen halide. The dialkyl imidocarbonate precursors are prepared by using a stoichiometric ratio (2:1) of alcohol to cyanogen halide in the presence of an acid acceptor and in a non-aqueous solvent.Dialkyl (N-cyanoimido)carbonates are useful as intermediates for pesticides and pharmaceuticals.
    • 在非水溶剂中通过以下方法制备二烷基(N-氰基亚氨基)碳酸酯,该方法包括(a)以受控的速率将氰卤化物加入到含有未取代或取代的亚氨基碳酸二烷基酯的无机碱的反应器中, /或三烷基胺,或(b)通过将三烷基胺加入到未取代或取代的酰亚胺碳酸二烷基酯和氰卤化物的溶液中。 通过在酸受体和非水溶剂的存在下,使用化学计量比(2:1)的醇与氰卤化物来制备二烷基亚氨碳酸酯前体。 二烷基(N-氰基亚氨基)碳酸酯可用作农药和药物的中间体。
    • 3. 发明授权
    • Scissor jet cleaning device
    • 剪式喷射清洗装置
    • US5638845A
    • 1997-06-17
    • US555165
    • 1995-11-08
    • Michael A. OliverJohn W. Mincy
    • Michael A. OliverJohn W. Mincy
    • B05B13/06B08B3/02B08B9/093B63B57/02
    • B63B57/02B08B9/093B08B9/0936B05B13/0627
    • A scissor jet cleaning device (10) for cleaning the interior of a tank (12) through a dome (14) on the tank (12) of a tanker (16). The device (10) comprises a support arm (18) that is adjustable in length. An assembly (20) is mounted to the dome (14) and is connected to a first side of the support arm (18), for extending and retracting the support arm (18) within the tank (12). A double spray nozzle head (22) is mounted in a rotatable manner to a second side of the support arm (18). A facility (24) is for fluidly connecting the double spray nozzle head (22) to pressurized cleaning fluid, so as to clean the interior of the tank (12). A structure (26) is connected to the extending and retracting assembly (20), for rotating the support arm (18) in its retracted position 180 degrees, so that the double spray nozzle head (22) can clean the interior of the tank (12) in an opposite direction.
    • 一种用于通过罐车(16)的罐(12)上的圆顶(14)清洁罐(12)的内部的剪刀喷射清洁装置(10)。 装置(10)包括长度可调节的支撑臂(18)。 组件(20)安装在圆顶(14)上,并连接到支撑臂(18)的第一侧,用于使罐(12)内的支撑臂(18)伸展和缩回。 双喷嘴头(22)以可旋转的方式安装到支撑臂(18)的第二侧。 设备(24)用于将双喷嘴头(22)流体连接到加压清洗流体,以便清洁罐(12)的内部。 结构(26)连接到延伸和缩回组件(20),用于将支撑臂(18)在其缩回位置旋转180度,使得双喷嘴头(22)可以清洁罐的内部 12)在相反的方向。