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1. 发明专利

JP2008230992A PHOSPHORUS-CONTAINING SULFONE, SULFOXIDE DERIVATIVE AND METHOD FOR PRODUCING PHOSPHORUS-CONTAINING α-KETO ACID USING THE SAME AS INTERMEDIATE 有权
标题翻译：含磷硫化物，硫氧化物衍生物和使用其作为中间产物含有含磷酸的α-酮酸的方法
公开(公告)号：JP2008230992A
公开(公告)日：2008-10-02
申请号：JP2007069959
申请日：2007-03-19
申请人： Meiji Seika Kaisha Ltd , 明治製菓株式会社
发明人： MINOWA NOBUTO , MITOMI MASAAKI
IPC分类号： C07F9/32 , B01J31/12 , C07B61/00 , C07F9/30
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method for efficiently producing 4-(hydroxymethyl-phosphonyl)-2-oxobutanoic acid of an intermediate for producing herbicide L-AMPB. SOLUTION: The method for producing the 4-(hydroxymethyl-phosphonyl)-2-oxobutanoic acid uses a compound represented by formula (5) [wherein, R 1 is an aryl group; R 2 , R 3 and R 4 are each a 1-4C alkyl group; and n is an integer of 1 or 2]. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：待解决的问题：提供一种有效生产除草剂L-AMPB的中间体的4-（羟甲基 - 膦酰基）-2-氧代丁酸的方法。解决方案：制备4-（羟基甲基 - 膦酰基）-2-氧代丁酸的方法使用由式（5）表示的化合物[其中，R“SP”是芳基; R 2 ，R 3 和R 4 分别为1-4C烷基; n为1或2的整数]。版权所有（C）2009，JPO＆INPIT

2. 发明专利

JPS5970696A Novel methylphosphinic acid compound and herbicidal and miticidal agent 失效
标题翻译：新型甲基磷酸化合物和除草剂和微生物剂
公开(公告)号：JPS5970696A
公开(公告)日：1984-04-21
申请号：JP17980082
申请日：1982-10-15
申请人： Meiji Seika Kaisha Ltd
发明人： MINOWA NOBUTO , TACHIBANA KUNITAKA , KIKUCHI TAKAHIKO , WATANABE TETSUO , FUKATSU SHIYUNZOU
IPC分类号： A01N57/20 , C07F9/30
摘要： NEW MATERIAL:The compound of formula I [R
1 is H; R
2 is (substituted) 1W4C alkyl, (substituted) 1W4C alkenyl or (substituted) aryl; M
1 and M
2 are H, metallic cation, (substituted) ammonium cation, or cation derived from choline molecule; m is reciprocal number of the ionic value of M
1 cation; n is reciprocal number of the ionic value of M
2 cation].
EXAMPLE: [(3-Phenylmethyleneamino-3-carboxy)-propyl-1]-methylphosphinic acid disodium salt.
USE: A herbicidal and miticidal agent having low toxicity to man and cattle.
PROCESS: For example, the carbonyl compound of formula III, pereferably an aldehyde, is condensed to the methylphosphine compound of formula II preferably at -10W+50°C for 1W24hr is necessary in the presence of a solvent (preferably a lower alkanol).
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新材料：式I化合物[R 1]为H; R 2是（取代的）1-4C烷基，（取代的）1-4C烯基或（取代的）芳基; M 1和M 2均为H，金属阳离子，（取代的）铵阳离子或衍生自胆碱分子的阳离子; m是M 1离子的离子值的倒数; n是M 2阳离子的离子值的倒数。实施例：[（3-苯基亚甲基氨基-3-羧基） - 丙基] -1-甲基次膦酸二钠盐。用途：对人和牛具有低毒性的除草和杀螨剂。方法：例如，式III的羰基化合物，优选为醛，优选在-10- + 50℃下与式II的甲基膦化合物缩合1-24小时，在溶剂存在下（优选为低级链烷醇）。

3. 发明专利

JPS58198494A Novel compound, its preparation and use 失效
标题翻译：新化合物，其制备和使用
公开(公告)号：JPS58198494A
公开(公告)日：1983-11-18
申请号：JP8058082
申请日：1982-05-13
申请人： Meiji Seika Kaisha Ltd
发明人： MINOWA NOBUTO , TACHIBANA KUNITAKA , FUKATSU SHIYUNZOU , MATSUMOTO KUNIOMI , WATANABE TETSUO
IPC分类号： A01N57/20 , C07F9/30
摘要： NEW MATERIAL:A compound of formula I [R is H, lower alkyl, phenyl; X, Y, Z are H, alkyl or alakaline earth metal; m, n, q are valency of X, Y, Z; A is inorganic or organic acid; e is 0, 1/2, 1].
EXAMPLE: The compound of formula II.
USE: A herbicide with low toxicity to men and animals.
PREPARATION: The reaction between a compound of formula III such as DL-2- amino-4-[(hydroxy)(methyl)phosphinoyl]butyric acid, an aldehyde of R-CHO and a sulfite of Z
1/q HSO
3 is effected to give the compound of formula I .
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：新材料：式I化合物[R为H，低级烷基，苯基; X，Y，Z是H，烷基或碱土金属; m，n，q是X，Y，Z的化合价; A是无机或有机酸; e为0，1/2，1]。实施例：式II化合物。用途：对男性和动物毒性低的除草剂。制备：实施式III化合物如DL- 2-氨基-4 - [（羟基）（甲基）膦酰基]丁酸，R-CHO的醛和Z1 / qHSO3的亚硫酸酯之间的反应，得到式I化合物。

4. 发明专利

JP2009023942A MANUFACTURING METHOD OF PHOSPHORUS-CONTAINING α-AMINO ACID, AND PHOSPHORUS-CONTAINING NITRO DERIVATIVE AS PRODUCTION INTERMEDIATE THEREOF 有权
标题翻译：含有α-氨基酸的含磷酸的制造方法和含有硝基衍生物作为生产中间体的制备方法
公开(公告)号：JP2009023942A
公开(公告)日：2009-02-05
申请号：JP2007188396
申请日：2007-07-19
申请人： Meiji Seika Kaisha Ltd , 明治製菓株式会社
发明人： MINOWA NOBUTO , MITOMI MASAAKI
IPC分类号： C07F9/32 , C07B61/00 , C07F9/30
摘要： PROBLEM TO BE SOLVED: To provide a method for inexpensively manufacturing a herbicide, D, L-2-amino-4-(hydroxymethylphosphinyl)-butanoic acid in a good yield without generating a large amount of a by-product such as a salt under a mild reaction condition.
SOLUTION: The manufacturing method of D, L-2-amino-4-(hydroxymethylphosphinyl)-butanoic acid comprises reducing a nitro group of a compound represented by formula (3) [wherein R
1 is an alkyl group or a chloroethyl group; and R
2 is an alkyl group] to convert it into an amino group followed by deprotection by hydrolysis of a phosphoric ester and a carboxylic ester.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：待解决的问题：提供一种低成本地制造除草剂D，L-2-氨基-4-（羟甲基氧膦基） - 丁酸的方法，而不产生大量的副产物，例如盐在温和的反应条件下。解决方案：D，L-2-氨基-4-（羟甲基氧膦基） - 丁酸的制备方法包括将由式（3）表示的化合物的硝基还原[其中R 1 = 是烷基或氯乙基; 并且R 2为烷基]，将其转化为氨基，然后通过磷酸酯和羧酸酯的水解脱保护。版权所有（C）2009，JPO＆INPIT

5. 发明专利

JPS61137802A Antimicrobial agent, antifungal agent and herbicide 失效
标题翻译：抗菌剂，抗真菌剂和除草剂
公开(公告)号：JPS61137802A
公开(公告)日：1986-06-25
申请号：JP25934784
申请日：1984-12-10
申请人： Meiji Seika Kaisha Ltd , Nippon Terupen Kagaku Kk
发明人： INAGAKI TAKASHI , TAKEUCHI HIROYUKI , MINOWA NOBUTO , MATSUMOTO KUNIOMI , TACHIBANA KUNITAKA , FUKUYASU SHUNKAI , FUKATSU SHUNZO
IPC分类号： A01N37/02
摘要： PURPOSE: An agent useful in the fields of medical treatment, animals, agriculture and industry, showing improved antimicrobial activities against fungi of iatrogenic strain, wood-decomposing mold, slime-constituting microorganism, etc., having further herbicidal activity, comprising a specific terpene acetate compound as an active ingredient.
CONSTITUTION: The titled agent comprising a compound shown by the formula (X is halogen; R is monoterpene, preferably bornyl, isobornyl, menthyl, perillyl, terpinyl, etc.) as an active ingredient. The compound shown by the formula is obtained by dehydration reaction of a halogenoacetic acid with a monoterpene alcohol. The titled agent is used as a solution or ointment for remedying external diseases caused by molds belonging to the genus Candida, for animal use such as pets, domestic animals, etc., for preventing growth of pathogenic bacteria and molds, as a sterilizer or a disinfectant for remedying external diseases, a sterilizer or a disinfectant for seeds, lumber, agricultural and horticultural crops, adhesives, pulp, circulating water for cooling etc., and a herbicide for a wide range of weeds.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：一种在医疗，动物，农业和工业领域有用的药剂，显示出具有进一步除草活性的具有进一步除草活性的医源性菌株，木材分解霉菌，粘液微生物等真菌的抗菌活性的改善，包括特定的萜烯乙酸酯化合物作为活性成分。构成：作为活性成分，含有式（X为卤素，R为单萜，优选为冰片基，异冰片基，薄荷基，环己基，萜烯基等）的化合物。由式表示的化合物是通过卤代乙酸与单萜醇的脱水反应得到的。标题试剂用作解决方案或软膏，用于补救由属于假丝酵母属的霉菌，动物用途如宠物，家畜等引起的外部疾病，用于预防病原菌和霉菌的生长，作为灭菌器或用于补救外部疾病的消毒剂，用于种子，木材，农业和园艺作物的消毒剂或消毒剂，粘合剂，纸浆，用于冷却的循环水等，以及用于广泛杂草的除草剂。

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