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1. 发明授权

US6074588A Mold releasing agent, cured film obtained therefrom and molding method using said mold releasing agent 失效
标题翻译：脱模剂，由此获得的固化膜和使用该脱模剂的成型方法
公开(公告)号：US6074588A
公开(公告)日：2000-06-13
申请号：US646374
申请日：1996-05-15
申请人： Masayuki Yamana , Tomohiro Hosomi , Hirotoshi Sakashita , Masato Kashiwagi
发明人： Masayuki Yamana , Tomohiro Hosomi , Hirotoshi Sakashita , Masato Kashiwagi
IPC分类号： B29C33/64 , C10M105/00 , C10M105/76 , C10M111/04 , B29C41/02
CPC分类号： C10M105/76 , B29C33/64 , C10M105/00 , C10M111/04 , C10M2203/003 , C10M2211/0406 , C10M2211/042 , C10M2211/0425 , C10M2211/0445 , C10M2211/06 , C10M2213/00 , C10M2213/023 , C10M2213/04 , C10M2213/043 , C10M2213/06 , C10M2213/0606 , C10M2213/0623 , C10M2227/00 , C10M2227/02 , C10M2227/025 , C10M2227/04 , C10M2227/045 , C10M2229/025 , C10M2229/0405 , C10M2229/041 , C10M2229/0415 , C10M2229/042 , C10M2229/0425 , C10M2229/0435 , C10M2229/0445 , C10M2229/045 , C10M2229/0455 , C10M2229/046 , C10M2229/0465 , C10M2229/047 , C10M2229/0475 , C10M2229/048 , C10M2229/0485 , C10M2229/0505 , C10M2229/051 , C10M2229/0515 , C10M2229/052 , C10M2229/0525 , C10M2229/053 , C10M2229/0535 , C10M2229/0545 , C10N2240/00 , C10N2240/22 , C10N2240/30 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： A mold releasing agent comprising a silicon-containing compound represented by the formula:R.sup.1.sub.n SiR.sup.2.sub.4-nwherein R.sup.1 is ##STR1## (R.sup.3 and R.sup.4 are a hydrocarbon group having 1 to 4 carbon atoms), R.sup.2 is a hydrocarbon group having 1 to 4 carbon atoms or a halogenated hydrocarbon group having 1 to 4 carbon atoms, n is 3 or 4, and a silicon- and/or fluorine-containing compound having at least two hydroxyl groups or alkoxyl groups in one molecule. The mold releasing agent of the present invention is excellent in mold releasing property, has a long life, provides a good surface finishing of molded article, and has no influence on secondary processability.
摘要翻译： PCT No.PCT / JP94 / 01961 Sec。 371日期：1996年5月15日 102（e）日期1996年5月15日PCT 1994年11月18日PCT PCT。第WO95 / 14750号公报日期：1995年6月1日，包含由下式表示的含硅化合物的脱模剂：R1nSiR24-n，R1为（R3和R4为碳原子数为1〜4的烃基），R2为1〜4的烃基碳原子或碳原子数为1〜4的卤代烃基，n为3或4，在1分子中含有至少2个羟基或烷氧基的硅和/或含氟化合物。本发明的脱模剂脱模性优异，使用寿命长，成型品表面精加工性良好，二次加工性无影响。

2. 发明授权

US5804674A Mold release agent, cured film obtained from said mold release agent, and molding method using said mold release agent 失效
标题翻译：脱模剂，由脱模剂得到的固化膜，以及使用脱模剂的成型方法
公开(公告)号：US5804674A
公开(公告)日：1998-09-08
申请号：US809449
申请日：1997-04-21
申请人： Masayuki Yamana , Yasushi Nakamae , Hirotoshi Sakashita , Masato Kashiwagi
发明人： Masayuki Yamana , Yasushi Nakamae , Hirotoshi Sakashita , Masato Kashiwagi
IPC分类号： B29C33/60 , B29C33/64 , C07F7/10 , C07F7/21 , C08L33/04 , C08L33/16 , C08L83/04 , C08F8/00
CPC分类号： B29C33/60 , B29C33/64
摘要： A mold release agent containing (A) a silane compound, (B) a silicon and/or fluorine-containing compound having at least two hydroxyl groups or alkoxy groups in one molecule and (C) a polymer of a perfluoroalkyl group-containing (meth)acrylate ester gives a long mold release life and a good surface finishing property of a molded article, and does not exert a harmful influence on fabricability such as painting and adhesion of the molded article.
摘要翻译： PCT No.PCT / JP95 / 02146 Sec。 371日期1997年04月21日 102（e）1997年4月21日PCT PCT 1995年10月19日PCT公布。公开号WO96 / 12600 PCT 日期1996年5月2日一种脱模剂，其含有（A）硅烷化合物，（B）在一个分子中具有至少两个羟基或烷氧基的硅和/或含氟化合物，（C）全氟烷基的聚合物（甲基）丙烯酸酯具有长的脱模寿命和良好的模塑制品的表面精加工性，并且不会对成型制品的涂装和粘附等可制造性产生有害影响。

3. 发明授权

US5734001A Fluorosilicone compound and composition containing the same 失效
标题翻译：氟硅氧烷化合物及其组合物
公开(公告)号：US5734001A
公开(公告)日：1998-03-31
申请号：US737498
申请日：1996-11-20
申请人： Fumihiko Yamaguchi , Tatsuya Otsuka , Masayuki Yamana , Masato Kashiwagi , Hirotoshi Sakashita
发明人： Fumihiko Yamaguchi , Tatsuya Otsuka , Masayuki Yamana , Masato Kashiwagi , Hirotoshi Sakashita
IPC分类号： B29C33/64 , C08G77/24 , C08G77/385 , C08L83/08 , C09D5/16 , C09D183/08 , C09K3/10 , D06M15/657
CPC分类号： D06M15/657 , B29C33/64 , C08G77/385 , C08L83/08 , C09D183/08 , C09D5/1675 , C09K3/1018 , D06M7/00 , D06M2200/40
摘要： A novel fluorosilicone compound having at least two hydroxyl groups in its molecule and a curable composition containing such a compound and a commercially available general purpose curing agent; the compound is used suitably for a lubricant and a fiber treating agent, and the curable composition is used suitably for a mold releasing agent, a water- and oil-repelling agent, a stain-proof coating agent, a non-tackifying coating agent, a coating agent for optical use and a sealant.
摘要翻译： PCT No.PCT / JP95 / 01008 Sec。 371日期1996年11月20日 102（e）1996年11月20日PCT PCT 1995年5月25日PCT公布。 WO95 / 33001 PCT出版物日期：1995年12月7日在其分子中具有至少两个羟基的新型氟硅酮化合物和含有这种化合物的可固化组合物和市售通用固化剂; 该化合物适合用于润滑剂和纤维处理剂，并且该固化性组合物适用于脱模剂，拒水拒油剂，防污涂料，非增粘涂料，用于光学用途的涂料剂和密封剂。

4. 发明授权

US06750277B1 Composition and treatment agent 有权
标题翻译：成分和处理剂
公开(公告)号：US06750277B1
公开(公告)日：2004-06-15
申请号：US09355673
申请日：1999-08-19
申请人： Masayuki Yamana , Ikuo Yamamoto , Masato Kashiwagi , Koji Kubota
发明人： Masayuki Yamana , Ikuo Yamamoto , Masato Kashiwagi , Koji Kubota
IPC分类号： C08K504
CPC分类号： C08K5/06 , C08K5/10 , C09K3/18 , D06M15/277 , D06M15/285 , D06M2200/11 , D06M2200/12
摘要： A composition comprising (A) a copolymer which comprises (I) repeating units which are derived from a monomer having a fluoroalkyl group, a carbon-carbon double bond, (II) optional repeating units which are derived from a monomer having at least two urethane or urea bonds and a carbon-carbon double bond, but no fluorine atom, (III) optional repeating units which are derived from a monomer, the homopolymer of which having a glass transition temperature (Tg) of 50° C. or less, (IV) optional repeating units which are derived from a monomer having a hydrophilic group and a carbon-carbon double bond, and (V) optional repeating units which are derived from a monomer having a chlorine atom and a carbon-carbon double bond; and (B) a film-forming auxiliary can impart high water and oil repellency by drying at room temperature (0 to 30° C.) without requiring a heat treatment step.
摘要翻译：一种组合物，其包含（A）共聚物，其包含（I）衍生自具有氟烷基的单体的重复单元，碳 - 碳双键，（II）任选的重复单元，其衍生自具有至少两个氨基甲酸酯的单体或脲键和碳 - 碳双键，但不含氟原子，（III）衍生自单体的任选的重复单元，其均聚物的玻璃化转变温度（Tg）为50℃以下（（Tg） IV）衍生自具有亲水基团和碳 - 碳双键的单体的任选重复单元，和（V）衍生自具有氯原子和碳 - 碳双键的单体的任选的重复单元; 和（B）成膜助剂可以通过在室温（0〜30℃）下干燥而赋予高斥水斥油性，而不需要热处理步骤。

5. 发明申请

US20070293654A1 Water-Repellant/Oil Repellent Composition 有权
标题翻译：防水/防油组成
公开(公告)号：US20070293654A1
公开(公告)日：2007-12-20
申请号：US11660966
申请日：2005-08-02
申请人： Masato Kashiwagi
发明人： Masato Kashiwagi
IPC分类号： C08G61/00
CPC分类号： D06M15/277 , C09D133/16 , C09K3/18 , D06M15/53 , D06M2200/11 , D06M2200/12
摘要： Disclosed is an aqueous water-repellent/oil-repellent composition containing the following components (A), (B) and (C). Fluorine-containing copolymer (A): a copolymer containing a polymerizable monomer (al) having a perfluoroalkyl group with 1-6 carbon atoms or a perfluoroalkenyl group wherein the amount of (al) is not less than 20% by weight relative to the copolymer. Surfactant (B): a surfactant essentially containing a sorbitan ester or an alkylene oxide addition product thereof. Aqueous medium (C): a medium substantially containing water only or water and a water-soluble organic solvent.
摘要翻译：公开了含有以下组分（A），（B）和（C）的水性拒水/拒油组合物。含氟共聚物（A）：含有具有1-6个碳原子的全氟烷基的可聚合单体（a1）或全氟烯基的共聚物，其中（a1）的量相对于共聚物为不小于20重量％。表面活性剂（B）：基本上含有脱水山梨糖醇酯或其烯化氧加成产物的表面活性剂。水性介质（C）：基本上仅含水的介质或水和水溶性有机溶剂。

6. 发明授权

US07560506B2 Water- and oil-repellent composition and process for production thereof 有权
标题翻译：拒水拒油剂组合物及其生产方法
公开(公告)号：US07560506B2
公开(公告)日：2009-07-14
申请号：US11578797
申请日：2005-04-14
申请人： Masato Kashiwagi
发明人： Masato Kashiwagi
IPC分类号： C08L27/12
CPC分类号： C09K3/18 , D06M15/277 , Y10S524/926
摘要： A water- and oil-repellent composition consisting of (A) a fluorine-containing copolymer comprising at least 20% by weight (based on the copolymer) of (a1) units derived from a polymerizable monomer having a C1-6 polyfluoroalkyl group or a polyfluoroalkenyl group, (B) a surfactant component comprising as the essential components (b1) a nonionic surfactant having an HLB value of 12 or below and (b2) a nonionic surfactant having an HLB value of 15 or above, and (C) an aqueous medium substantially consisting of water. This composition is free from operationally or environmentally undesirable solvents and superior to conventional ones in stabilities such as mechanical stability, chemical stability, and long-term shelf stability.
摘要翻译：一种防水防油组合物，由（A）含有共聚物的至少20重量％（基于共聚物）的（a1）衍生自具有C1-6多氟烷基的可聚合单体或（B）含有HLB值为12以下的非离子表面活性剂和（b2）HLB值为15以上的非离子性表面活性剂，（C）水性基本上由水组成的介质。该组合物在机械稳定性，化学稳定性和长期贮存稳定性等稳定性方面没有操作上或环境不理想的溶剂，优于常规溶剂。

7. 发明授权

US07820745B2 Water-repellent/oil-repellent composition 有权
标题翻译：防水/防油组合物
公开(公告)号：US07820745B2
公开(公告)日：2010-10-26
申请号：US11660966
申请日：2005-08-02
申请人： Masato Kashiwagi
发明人： Masato Kashiwagi
IPC分类号： C08K5/1535 , C08G61/00
CPC分类号： D06M15/277 , C09D133/16 , C09K3/18 , D06M15/53 , D06M2200/11 , D06M2200/12
摘要： Disclosed is an aqueous water-repellent/oil-repellent composition containing the following components (A), (B) and (C). Fluorine-containing copolymer (A): a copolymer containing a polymerizable monomer (a1) having a perfluoroalkyl group with 1-6 carbon atoms or a perfluoroalkenyl group wherein the amount of (a1) is not less than 20% by weight relative to the copolymer. Surfactant (B): a surfactant essentially containing a sorbitan ester or an alkylene oxide addition product thereof. Aqueous medium (C): a medium substantially containing water only or water and a water-soluble organic solvent.
摘要翻译：公开了含有以下组分（A），（B）和（C）的水性拒水/拒油组合物。含氟共聚物（A）：含有具有1-6个碳原子的全氟烷基的可聚合单体（a1）或全氟烯基的共聚物，其中（a1）的量相对于共聚物为不小于20重量％。表面活性剂（B）：基本上含有脱水山梨糖醇酯或其烯化氧加成产物的表面活性剂。水性介质（C）：基本上仅含水的介质或水和水溶性有机溶剂。

8. 发明授权

US07709563B2 Aqueous dispersion type fluorine-containing water- and-oil repellent composition having a polymer of a perfluoroalkyl group- containing etheylenically unsaturated monomer, a nonionic surfactant ana cationic surfactant, and preparation and use thereof 有权
标题翻译：具有含全氟烷基的乙烯基不饱和单体的聚合物，非离子表面活性剂阳离子表面活性剂的水分散型含氟斥水斥油剂组合物及其制备及用途
公开(公告)号：US07709563B2
公开(公告)日：2010-05-04
申请号：US10470305
申请日：2002-01-29
申请人： Kouji Kubota , Takuya Yoshioka , Masato Kashiwagi
发明人： Kouji Kubota , Takuya Yoshioka , Masato Kashiwagi
IPC分类号： C08K5/19 , C08K5/06 , C08L27/12 , D06M15/277
CPC分类号： D06M15/263 , C03C17/32 , C03C25/305 , C09K3/18 , D06M15/277 , D06M2101/20 , D06M2200/10 , D06M2200/11 , D06M2200/12
摘要： An aqueous dispersion type fluorine-containing water- and oil-repellent composition containing a polymer of a perfluoroalkyl group-containing ethylenically unsaturated monomer dispersed in an aqueous medium. The composition also contains a nonionic surfactant having an HLB value of at most 11 and a cationic surfactant. A homopolymer of at least one monomer constituting the polymer has Tg of at most 50° C.
摘要翻译：含有分散在水性介质中的含全氟烷基的烯属不饱和单体的聚合物的水分散型含氟防水斥油剂组合物。该组合物还含有HLB值至多为11的非离子表面活性剂和阳离子表面活性剂。构成聚合物的至少一种单体的均聚物的Tg至多为50℃

9. 发明授权

US07217760B2 Water-and-oil repellant composition with improved suitability for cold cure 有权
标题翻译：防水防油组合物具有改进的适用于冷固化的组合物
公开(公告)号：US07217760B2
公开(公告)日：2007-05-15
申请号：US10471179
申请日：2002-03-06
申请人： Takuya Yoshioka , Masato Kashiwagi
发明人： Takuya Yoshioka , Masato Kashiwagi
IPC分类号： D06M15/277 , C08L27/12
CPC分类号： D06M15/277 , C08F212/14 , C08F214/18 , C08F214/182 , C08F220/22 , C08F220/24 , C09K3/18 , D06M15/227 , D06M15/248 , D06M15/263 , D06M15/576 , D06M2200/11 , D06M2200/12 , Y10T428/2967 , C08F2/24 , C08F2/32
摘要： A fluoropolymer-based water-and-oil repellant composition which comprises a copolymer comprising units derived from (a) an ethylenic monomer having a perfluoroalkyl group, (b) an ethylenic monomer having a group comprising an aromatic ring and a halogen atom or halogenomethyl group bonded thereto, and (c) an ethylenic monomer copolymerizable with these. The composition imparts excellent water and oil repellency through cold cure.
摘要翻译：一种含氟聚合物类防水斥油剂组合物，其包含共聚物，所述共聚物包含衍生自（a）具有全氟烷基的烯属单体的单元，（b）具有包含芳环和卤素原子的基团的烯属单体或卤代甲基和（c）可与其共聚的乙烯类单体。该组合物通过冷固化赋予优异的拒水拒油性。

10. 发明申请

US20070088141A1 Water and oil repellent composition and treatment method 有权
标题翻译：防水防油组成及处理方法
公开(公告)号：US20070088141A1
公开(公告)日：2007-04-19
申请号：US11512195
申请日：2006-08-30
申请人： Masato Kashiwagi
发明人： Masato Kashiwagi
IPC分类号： C08F214/18
CPC分类号： C08F214/18
摘要： Disclosed is a water- and oil-repellent agent comprising the following fluorine-containing copolymer (A). The fluorine-containing copolymer (A) comprises: (a1) a fluoroalkyl group-containing polymerizable monomer of the formula: wherein Y is a divalent organic group [for example, an aliphatic group having 1 to 10 carbon atoms, an aromatic or cycloaliphatic group having 6 to 10 carbon atoms, a —SO2N(R1)R2— group (in which R1 is a hydrogen atom or an alkyl group having 1 to 4 carbon atoms, and R2 is an alkylene group having 1 to 10 carbon atoms), a —CON(R1)R2— group (in which R1 is a hydrogen atom or an alkyl group having 1 to 4 carbon atoms, and R2 is an alkylene group having 1 to 10 carbon atoms), or a —CH2CH(OY1)CH2— group (in which Y1 is a hydrogen atom or an acyl group having 1 to 4 carbon atoms)]; and Rf is a linear or branched fluoroalkyl or fluoroalkenyl group having 1 to 6 carbon atoms; and (a2) vinylidene chloride.
摘要翻译：公开了一种防水防油剂，其包含以下含氟共聚物（A）。含氟共聚物（A）包括：（a 1）下式的含氟烷基的可聚合单体：其中Y是二价有机基团[例如，具有1-10个碳原子的脂族基团，芳族或环脂族具有6至10个碳原子的基团，-SO 2 N（R 1）R 2 - （其中R 1）是氢原子或碳原子数为1〜4的烷基，R 2为碳原子数为1〜10的亚烷基），-CON（R 1）基团（其中R 1是氢原子或具有1至4个碳原子的烷基，R 2是氢， / SUP>是具有1至10个碳原子的亚烷基）或-CH 2 CH 2（CH 2）CH 2 - 基团（其中Y 1是氢原子或具有1至4个碳原子的酰基）]; Rf是具有1-6个碳原子的直链或支链氟烷基或氟烯基; 和（a2）偏二氯乙烯。

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