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1. 发明授权

US06723484B1 Positive-working photosensitive resin precursor composition 有权
标题翻译：正性感光性树脂前体组合物
公开(公告)号：US06723484B1
公开(公告)日：2004-04-20
申请号：US09567106
申请日：2000-05-08
申请人： Masao Tomikawa , Naoyo Okamoto , Satoshi Yoshida , Ryoji Okuda
发明人： Masao Tomikawa , Naoyo Okamoto , Satoshi Yoshida , Ryoji Okuda
IPC分类号： G03F7023
CPC分类号： G03F7/0233 , C08G73/1025 , C08L79/08
摘要： The present invention relates to a positive-working photosensitive resin precursor composition which is characterized in that it contains (a) polymer in which the chief component comprises structural units of the kind where the bonding between structural units is represented by general formula (1) and (b) photoacid generator, and it can form a pattern by light irradiation and subsequent developing, and the total carboxyl groups contained in said polymer is from 0.02 to 2.0 mmol/g, and it provides a photosensitive resin composition of high sensitivity which can be developed by alkali. (R1 is an organic group of valency from 3 to 8 having at least 2 carbon atoms, R2 is an organic group of valency from 2 to 6 having at least 2 carbon atoms, R3 is hydrogen or an organic group with from 1 to 10 carbons. n is an integer of value from 3 to 100,000, m is 1 or 2, p and q are integers of value from 0 to 4 and p+q>0).
摘要翻译：本发明涉及一种正性感光性树脂前体组合物，其特征在于，其含有（a）主要成分包含结构单元之间的结合由通式（1）表示的结构单元和（b）光致酸发生剂，可以通过光照射和随后的显影形成图案，所述聚合物中所含的总羧基为0.02〜2.0mmol / g，提供高灵敏度的感光性树脂组合物，其可以是（R 1是具有至少2个碳原子的3至8价的有机基团，R 2是具有至少2个碳原子的2至6价的有机基团，R 3 是氢或1〜10个碳的有机基团，n为3〜100,000的整数，m为1或2，p和q为0〜4的整数，p + q> 0）。

2. 发明申请

US20120058889A1 Composition containing carbon nanotubes, catalyst for producing carbon nanotubes, and aqueous dispersion of carbon nanotubes 有权
标题翻译：含有碳纳米管的组合物，碳纳米管制造用催化剂和碳纳米管的水分散体
公开(公告)号：US20120058889A1
公开(公告)日：2012-03-08
申请号：US13138553
申请日：2010-03-04
申请人： Hidekazu Nishino , Hajime Kato , Naoyo Okamoto , Shuko Ikeuchi , Kenichi Sato , Shiho Tanaka , Kazuyoshi Higuchi
发明人： Hidekazu Nishino , Hajime Kato , Naoyo Okamoto , Shuko Ikeuchi , Kenichi Sato , Shiho Tanaka , Kazuyoshi Higuchi
IPC分类号： H01B1/04 , D01F9/12 , B01J21/10 , B82Y40/00 , B82Y30/00
CPC分类号： B01J21/10 , B01J23/40 , B01J23/74 , B01J23/745 , B01J23/78 , B01J35/02 , B01J37/0201 , B01J37/0203 , B01J37/10 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B32/168 , C01B32/174 , C01B2202/22 , C01B2202/34 , C01B2202/36 , Y10S977/742 , Y10S977/752 , Y10T428/2982
摘要： Disclosed is a composition containing carbon nanotubes which meets all of the following conditions (1) to (4). (1) When observed via transmission electron microscopy, at least 50 out of every 100 carbon nanotubes are double-walled carbon nanotubes. (2) The carbon nanotubes have an average outer diameter in the range of 1.0 to 3.0 nm. (3) During thermogravimetric analysis under atmosphere at a temperature increase rate of 10° C./minute, a high temperature combustion peak is at 700 to 850° C., and the relationship between low temperature weight loss (TG(L)) and high temperature weight loss (TG(H)) is TG(H)/(TG(L)+TG(H))≧0.75. (4) The composition containing carbon nanotubes has a volume resistance value between 1.0×10−2 Ω·cm and 1.0×10−4 Ω·cm, inclusive. The disclosed composition containing carbon nanotubes primarily has double-walled carbon nanotubes with high electrical conductivity and high heat resistance.
摘要翻译：公开了含有满足以下所有条件（1）〜（4）的碳纳米管的组合物。（1）当通过透射电子显微镜观察时，每100个碳纳米管中至少有50个是双壁碳纳米管。（2）碳纳米管的平均外径为1.0〜3.0nm。（3）温度升高速率为10℃/分钟的大气温度分析中，高温燃烧峰为700〜850℃，低温重量损失（TG（L））与高温重量损失（TG（H））为TG（H）/（TG（L）+ TG（H））≥0.75。（4）含有碳纳米管的组合物的体积电阻值为1.0×10 -2〜OHgr·cm，1.0×10 -4＆OHgr·cm，含有。所公开的含有碳纳米管的组合物主要具有导电性高，耐热性高的双壁碳纳米管。

3. 发明授权

US08038908B2 Carbon nanotube assembly and process for producing the same 有权
标题翻译：碳纳米管组件及其制造方法
公开(公告)号：US08038908B2
公开(公告)日：2011-10-18
申请号：US12734880
申请日：2008-08-19
申请人： Takayoshi Hirai , Hidekazu Nishino , Kenichi Sato , Naoyo Okamoto
发明人： Takayoshi Hirai , Hidekazu Nishino , Kenichi Sato , Naoyo Okamoto
IPC分类号： H01B1/04
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/15 , Y10S977/752 , Y10S977/842 , Y10S977/847 , Y10S977/932 , Y10T428/2918
摘要： An aggregate of carbon nanotubes satisfying all of the following requirements (1) to (3):(1) the volume resistivity is from 1×10−5 Ω·cm to 5×10−3 Ω·cm;(2) at least 50 out of 100 carbon nanotubes are double-walled carbon nanotubes in observation by a transmission electron microscope; and(3) the weight loss from 200° C. to 400° C. in thermogravimetry at a temperature rise of 10° C/min is from 5% to 20%.
摘要翻译：满足以下所有要求（1）〜（3）的碳纳米管的集合体：（1）体积电阻率为1×10-5〜OHgr·cm〜5×10-3·OHgr·cm; （2）通过透射电子显微镜观察，100个碳纳米管中的至少50个是双壁碳纳米管; 和（3）在10℃/分钟的温度升高下，在热重分析中从200℃至400℃的重量损失为5％至20％。

4. 发明授权

US08992878B2 Composition containing carbon nanotubes, catalyst for producing carbon nanotubes, and aqueous dispersion of carbon nanotubes 有权
标题翻译：含有碳纳米管的组合物，碳纳米管制造用催化剂和碳纳米管的水分散体
公开(公告)号：US08992878B2
公开(公告)日：2015-03-31
申请号：US13138553
申请日：2010-03-04
申请人： Hidekazu Nishino , Hajime Kato , Naoyo Okamoto , Shuko Ikeuchi , Kenichi Sato , Shiho Tanaka , Kazuyoshi Higuchi
发明人： Hidekazu Nishino , Hajime Kato , Naoyo Okamoto , Shuko Ikeuchi , Kenichi Sato , Shiho Tanaka , Kazuyoshi Higuchi
IPC分类号： C01B31/04 , B01J21/10 , B01J23/40 , B01J23/74 , B01J23/745 , B01J23/78 , B01J37/02 , B01J37/10 , B82Y30/00 , B82Y40/00 , C01B31/02 , B01J35/02
CPC分类号： B01J21/10 , B01J23/40 , B01J23/74 , B01J23/745 , B01J23/78 , B01J35/02 , B01J37/0201 , B01J37/0203 , B01J37/10 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B32/168 , C01B32/174 , C01B2202/22 , C01B2202/34 , C01B2202/36 , Y10S977/742 , Y10S977/752 , Y10T428/2982
摘要： Disclosed is a composition containing carbon nanotubes which meets all of the following conditions (1) to (4). (1) When observed via transmission electron microscopy, at least 50 out of every 100 carbon nanotubes are double-walled carbon nanotubes. (2) The carbon nanotubes have an average outer diameter in the range of 1.0 to 3.0 nm. (3) During thermogravimetric analysis under atmosphere at a temperature increase rate of 10° C./minute, a high temperature combustion peak is at 700 to 850° C., and the relationship between low temperature weight loss (TG(L)) and high temperature weight loss (TG(H)) is TG(H)/(TG(L)+TG(H))≧0.75. (4) The composition containing carbon nanotubes has a volume resistance value between 1.0×10−2 Ω·cm and 1.0×10−4 Ω·cm, inclusive. The disclosed composition containing carbon nanotubes primarily has double-walled carbon nanotubes with high electrical conductivity and high heat resistance.
摘要翻译：公开了含有满足以下所有条件（1）〜（4）的碳纳米管的组合物。（1）当通过透射电子显微镜观察时，每100个碳纳米管中至少有50个是双壁碳纳米管。（2）碳纳米管的平均外径为1.0〜3.0nm。（3）温度升高速率为10℃/分钟的大气温度分析中，高温燃烧峰为700〜850℃，低温重量损失（TG（L））与高温重量损失（TG（H））为TG（H）/（TG（L）+ TG（H））≥0.75。（4）含有碳纳米管的组合物的体积电阻值为1.0×10 -2〜OHgr·cm，1.0×10 -4＆OHgr·cm，含有。所公开的含有碳纳米管的组合物主要具有导电性高，耐热性高的双壁碳纳米管。

5. 发明申请

US20100301278A1 CARBON NANOTUBE ASSEMBLY AND PROCESS FOR PRODUCING THE SAME 有权
标题翻译：碳纳米管组件及其制造方法
公开(公告)号：US20100301278A1
公开(公告)日：2010-12-02
申请号：US12734880
申请日：2008-08-19
申请人： Takayoshi Hirai , Hidekazu Nishino , Kenichi Sato , Naoyo Okamoto
发明人： Takayoshi Hirai , Hidekazu Nishino , Kenichi Sato , Naoyo Okamoto
IPC分类号： H01B1/04 , H01B1/12 , D02G3/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/15 , Y10S977/752 , Y10S977/842 , Y10S977/847 , Y10S977/932 , Y10T428/2918
摘要： An aggregate of carbon nanotubes satisfying all of the following requirements (1) to (3): (1) the volume resistivity is from 1×10−5 Ω·cm to 5×10−3 Ω·cm; (2) at least 50 out of 100 carbon nanotubes are double-walled carbon nanotubes in observation by a transmission electron microscope; and (3) the weight loss from 200° C. to 400° C. in thermogravimetry at a temperature rise of 10° C./min is from 5% to 20%.
摘要翻译：满足以下所有要求（1）〜（3）的碳纳米管的集合体：（1）体积电阻率为1×10-5〜OHgr·cm〜5×10-3·OHgr·cm; （2）通过透射电子显微镜观察，100个碳纳米管中的至少50个是双壁碳纳米管; 和（3）在10℃/分钟的温度升高下，在热重分析中，从200℃至400℃的重量损失为5％至20％。

6. 发明授权

US08834826B2 Aggregate of carbon nanotubes, dispersion thereof and conductive film using the same 有权
标题翻译：碳纳米管的集合体，其分散体和使用其的导电膜
公开(公告)号：US08834826B2
公开(公告)日：2014-09-16
申请号：US12215405
申请日：2008-06-27
申请人： Kenichi Sato , Masahito Yoshikawa , Naoyo Okamoto , Shuko Numata
发明人： Kenichi Sato , Masahito Yoshikawa , Naoyo Okamoto , Shuko Numata
IPC分类号： D01F9/12 , C08J7/06 , C09D7/12 , C08J7/04 , B82Y30/00 , H01B1/12 , C09D5/24 , B82Y40/00 , C01B31/02 , H01B1/04 , H01J1/304 , H01B1/24 , C08K3/04
CPC分类号： D01F9/12 , B82Y30/00 , B82Y40/00 , C01B32/174 , C01B2202/06 , C01B2202/28 , C08J7/047 , C08J7/06 , C08J2367/02 , C08J2400/12 , C08K3/04 , C09D5/24 , C09D7/70 , H01B1/04 , H01B1/128 , H01B1/24 , H01J1/304 , H01J2201/30469 , Y10T428/30
摘要： Provided is an aggregate of carbon nanotubes satisfying (1) there is a 2θ peak at 24°±2° by X-ray powder diffraction analysis; (2) a height ratio (G/D ratio) of G band to D band by Raman spectroscopic analysis of wavelength 532 nm is 30 or more; and (3) a combustion peak temperature is from 550° C. to 700° C. The present invention provides an aggregate of carbon nanotubes excellent in dispersibility while high quality, giving a film, molded article, membrane or the like having excellent characteristics.
摘要翻译：提供了满足（1）的碳纳米管的聚集体，其具有2＆amp; 通过X射线粉末衍射分析在24°±2°的峰值; （2）通过波长532nm的拉曼光谱分析，G波段与D波段的高度比（G / D比）为30以上; （3）燃烧峰值温度为550℃〜700℃。本发明提供了优异的分散性优异的碳纳米管骨料，得到具有优异特性的膜，成型体，膜等。

7. 发明申请

US20090001326A1 Aggregate of carbon nanotubes, dispersion thereof and conductive film using the same 有权
标题翻译：碳纳米管的集合体，其分散体和使用其的导电膜
公开(公告)号：US20090001326A1
公开(公告)日：2009-01-01
申请号：US12215405
申请日：2008-06-27
申请人： Kenichi Sato , Masahito Yoshikawa , Naoyo Okamoto , Shuko Numata
发明人： Kenichi Sato , Masahito Yoshikawa , Naoyo Okamoto , Shuko Numata
IPC分类号： H01B1/24 , B32B9/00 , D01F9/12
CPC分类号： D01F9/12 , B82Y30/00 , B82Y40/00 , C01B32/174 , C01B2202/06 , C01B2202/28 , C08J7/047 , C08J7/06 , C08J2367/02 , C08J2400/12 , C08K3/04 , C09D5/24 , C09D7/70 , H01B1/04 , H01B1/128 , H01B1/24 , H01J1/304 , H01J2201/30469 , Y10T428/30
摘要： Provided is an aggregate of carbon nanotubes satisfying (1) there is a 2θ peak at 24°±2° by X-ray powder diffraction analysis; (2) a height ratio (G/D ratio) of G band to D band by Raman spectroscopic analysis of wavelength 532 nm is 30 or more; and (3) a combustion peak temperature is 550° C. or more, and 700° C. or less. The present invention provides an aggregate of carbon nanotubes excellent in dispersibility while high quality, giving a film, molded article, membrane or the like having excellent characteristics
摘要翻译：提供满足（1）的碳纳米管的集合体，通过X射线粉末衍射分析，在24°±2°处具有2θ的峰值; （2）通过波长532nm的拉曼光谱分析，G波段与D波段的高度比（G / D比）为30以上; 和（3）燃烧峰值温度为550℃以上，700℃以下。本发明提供了一种高质量的分散性优异的碳纳米管聚集体，得到具有优异特性的膜，成型品，膜等

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