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1. 发明授权

US07880038B2 Metal catalyst and its use 失效
标题翻译：金属催化剂及其用途
公开(公告)号：US07880038B2
公开(公告)日：2011-02-01
申请号：US10552664
申请日：2004-04-14
申请人： Masaji Hirota , Koji Hagiya
发明人： Masaji Hirota , Koji Hagiya
IPC分类号： B01J27/00 , B01J21/04 , C07C45/00
CPC分类号： C07C409/04 , B01J31/1805 , B01J2231/70 , B01J2231/72 , B01J2531/64 , B01J2531/66 , C07C45/29 , C07C45/294 , C07C51/285 , C07C407/00 , C07C409/08 , C07D301/12 , C07C49/78 , C07C47/54 , C07C53/126 , C07C63/06
摘要： A metal catalyst obtained by contacting (A) at least one metal or metal compound selected from i) tungsten compounds composed of tungsten and an element of group IIIb, IVb, Vb, or VIb, ii) molybdenum compounds composed of molybdenum and an element of group IIIb, IVb, Vb, or VIb, and iii) tungsten metal and molybdenum metal; (B) at least one compound selected from tertiary amine compounds, tertiary amine oxide compounds, nitrogen-containing aromatic compounds and nitrogen-containing aromatic N-oxide compounds; (C) hydrogen peroxide; and (D) a phosphate compound, is provided.
摘要翻译：一种金属催化剂，其通过使（A）至少一种金属或金属化合物与选自i）钨化合物和IIIb族，IVb族，Vb族或VIb族元素组成的金属或化合物接触而获得，ii）由钼和钼元素组成的钼化合物 IIIb族，IVb族，Vb族或VIb族，iii）钨金属和钼金属; （B）至少一种选自叔胺化合物，叔胺氧化物，含氮芳族化合物和含氮芳族N-氧化物的化合物; （C）过氧化氢; 和（D）磷酸酯化合物。

2. 发明申请

US20080039653A1 Process for Producing Adipic Acid 失效
标题翻译：生产己二酸的方法
公开(公告)号：US20080039653A1
公开(公告)日：2008-02-14
申请号：US11596455
申请日：2004-05-18
申请人： Masaji Hirota , Koji Hagiya
发明人： Masaji Hirota , Koji Hagiya
IPC分类号： C07C55/14
CPC分类号： C07C51/313 , B01J23/30 , C07C51/487 , C07C55/14
摘要： It is provided to a process for producing adipic acid which comprises making a wastewater containing hydroxycaproic acid and discharged from the step of oxidizing cyclohexane with molecular oxygen in a liquid phase react with hydrogen peroxide in the presence of a tungsten catalyst in the pH range of 0 to 6.
摘要翻译：提供了一种生产己二酸的方法，其包括制备含有羟基己酸的废水，并且在氧化环己烷的步骤中与分子氧在液相中与在过氧化氢中反应的步骤在钨催化剂存在下在pH范围为0的条件下与过氧化氢反应到6。

3. 发明申请

US20060211891A1 Metal catalyst and its use 失效
标题翻译：金属催化剂及其用途
公开(公告)号：US20060211891A1
公开(公告)日：2006-09-21
申请号：US10552664
申请日：2004-04-14
申请人： Masaji Hirota , Koji Hagiya
发明人： Masaji Hirota , Koji Hagiya
IPC分类号： B01J31/00 , C07C45/29
CPC分类号： C07C409/04 , B01J31/1805 , B01J2231/70 , B01J2231/72 , B01J2531/64 , B01J2531/66 , C07C45/29 , C07C45/294 , C07C51/285 , C07C407/00 , C07C409/08 , C07D301/12 , C07C49/78 , C07C47/54 , C07C53/126 , C07C63/06
摘要： A metal catalyst obtained by contacting (A) at least one metal or metal compound selected from i) tungsten compounds composed of tungsten and an element of group IIIb, IVb, Vb, or VIb, ii) molybdenum compounds composed of molybdenum and an element of group IIIb, IVb, Vb, or VIb, and iii) tungsten metal and molybdenum metal; (B) at least one compound selected from tertiary amine compounds, tertiary amine oxide compounds, nitrogen-containing aromatic compounds and nitrogen-containing aromatic N-oxide compounds; (C) hydrogen peroxide; and (D) a phosphate compound, is provided.
摘要翻译：一种金属催化剂，其通过使（A）至少一种金属或金属化合物与选自i）钨化合物和IIIb族，IVb族，Vb族或VIb族元素组成的金属或化合物接触而获得，ii）由钼和钼元素组成的钼化合物 IIIb族，IVb族，Vb族或VIb族，iii）钨金属和钼金属; （B）至少一种选自叔胺化合物，叔胺氧化物，含氮芳族化合物和含氮芳族N-氧化物的化合物; （C）过氧化氢; 和（D）磷酸酯化合物。

4. 发明授权

US07491845B2 Process for producing adipic acid 失效
标题翻译：己二酸生产方法
公开(公告)号：US07491845B2
公开(公告)日：2009-02-17
申请号：US11596455
申请日：2004-05-18
申请人： Masaji Hirota , Koji Hagiya
发明人： Masaji Hirota , Koji Hagiya
IPC分类号： C07C55/00
CPC分类号： C07C51/313 , B01J23/30 , C07C51/487 , C07C55/14
摘要： It is provided to a process for producing adipic acid which comprises making a wastewater containing hydroxycaproic acid and discharged from the step of oxidizing cyclohexane with molecular oxygen in a liquid phase react with hydrogen peroxide in the presence of a tungsten catalyst in the pH range of 0 to 6.
摘要翻译：提供了一种生产己二酸的方法，其包括制备含有羟基己酸的废水，并且在氧化环己烷的步骤中与分子氧在液相中与在过氧化氢中反应的步骤在钨催化剂存在下在pH范围为0的条件下与过氧化氢反应到6。

5. 发明授权

US07074947B2 Process for producing epoxide compound 失效
标题翻译：环氧化合物的制备方法
公开(公告)号：US07074947B2
公开(公告)日：2006-07-11
申请号：US10501956
申请日：2003-01-31
申请人： Masaji Hirota , Koji Hagiya
发明人： Masaji Hirota , Koji Hagiya
IPC分类号： C07D301/12 , B01J31/06
CPC分类号： B01J31/34 , B01J23/28 , B01J23/30 , B01J27/16 , B01J27/22 , B01J31/006 , B01J31/0237 , B01J31/0244 , B01J2231/72 , C07D301/12
摘要： A process for producing an epoxide compound, characterized by reacting an olefin compound with hydrogen peroxide in the presence of: a metal oxide catalyst obtained by reacting hydrogen peroxide with at least one member selected from the group consisting of tungsten metal, molybdenum metal, compounds of tungsten and a Group IIIb, IVb, Vb, or VIb element, tungstic acid and salts thereof, compounds of molybdenum and a Group IIIb, IVb, Vb, or VIb element, and molybodic acid and salts thereof; at least one member selected from the group consisting of tertiary amine compounds, tertiary amine oxide compounds, nitrogenous aromatic compounds, and nitrogenous aromatic N-oxide compounds; and a phosphoric acid compound.
摘要翻译：一种制备环氧化合物的方法，其特征在于使烯烃化合物与过氧化氢在以下存在下反应：金属氧化物催化剂，其通过使过氧化氢与至少一种选自钨金属，钼金属，钨和IIIb，IVb，Vb或VIb族元素，钨酸及其盐，钼和IIIb，IVb，Vb或VIb族元素的化合物，以及钼酸及其盐; 选自叔胺化合物，叔胺氧化物化合物，含氮芳族化合物和含氮芳族N-氧化物化合物中的至少一种; 和磷酸化合物。

6. 发明申请

US20050020841A1 Process for producing expoxide compound 失效
标题翻译：过氧化物生产工艺
公开(公告)号：US20050020841A1
公开(公告)日：2005-01-27
申请号：US10501956
申请日：2003-01-31
申请人： Masaji Hirota , Koji Hagiya
发明人： Masaji Hirota , Koji Hagiya
IPC分类号： B01J23/28 , B01J23/30 , B01J27/16 , B01J27/22 , B01J31/02 , B01J31/34 , C07D301/12
CPC分类号： B01J31/34 , B01J23/28 , B01J23/30 , B01J27/16 , B01J27/22 , B01J31/006 , B01J31/0237 , B01J31/0244 , B01J2231/72 , C07D301/12
摘要： A process for producing an epoxide compound, characterized by reacting an olefin compound with hydrogen peroxide in the presence of: a metal oxide catalyst obtained by reacting hydrogen peroxide with at least one member selected from the group consisting of tungsten metal, molybdenum metal, compounds of tungsten and a Group IIIb, IVb, Vb, or VIb element, tungstic acid and salts thereof, compounds of molybdenum and a Group IIIb, IVb, Vb, or VIb element, and molybodic acid and salts thereof; at least one member selected from the group consisting of tertiary amine compounds, tertiary amine oxide compounds, nitrogenous aromatic compounds, and nitrogenous aromatic N-oxide compounds; and a phosphoric acid compound.
摘要翻译：一种制备环氧化合物的方法，其特征在于使烯烃化合物与过氧化氢在以下存在下反应：金属氧化物催化剂，其通过使过氧化氢与至少一种选自钨金属，钼金属，钨和IIIb，IVb，Vb或VIb族元素，钨酸及其盐，钼和IIIb，IVb，Vb或VIb族元素的化合物，以及钼酸及其盐; 选自叔胺化合物，叔胺氧化物化合物，含氮芳族化合物和含氮芳族N-氧化物化合物中的至少一种; 和磷酸化合物。

7. 发明授权

US08604221B2 Production method of halogen-substituted phthalide 有权
标题翻译：卤素取代苯酞的制备方法
公开(公告)号：US08604221B2
公开(公告)日：2013-12-10
申请号：US13265699
申请日：2010-05-19
申请人： Koji Hagiya , Yasutaka Aoyagi
发明人： Koji Hagiya , Yasutaka Aoyagi
IPC分类号： C07D305/12
CPC分类号： C07D307/88 , C07B31/00 , C07D307/89
摘要： Disclosed is a method for producing a halogen-substituted phthalide, which includes a reaction step of reacting a halogen-substituted phthalic anhydride with sodium borohydride.
摘要翻译：公开了一种制备卤素取代的苯酞的方法，其包括使卤素取代的邻苯二甲酸酐与硼氢化钠反应的反应步骤。

8. 发明申请

US20130137897A1 PROCESS FOR PREPARING SULFUR-CONTAINING 2-KETOCARBOXYLATE COMPOUND 审中-公开
标题翻译：制备含硫酸2-羧基甲酸酯化合物的方法
公开(公告)号：US20130137897A1
公开(公告)日：2013-05-30
申请号：US13816123
申请日：2011-08-26
申请人： Kazuyasu Tani , Taro Hirose , Koji Hagiya
发明人： Kazuyasu Tani , Taro Hirose , Koji Hagiya
IPC分类号： C07C319/20
CPC分类号： C07C319/20 , B01J31/2243 , B01J2231/70 , B01J2531/0241 , B01J2531/0252 , B01J2531/56 , C07C323/52
摘要： The present invention provides a novel process for preparing a sulfur-containing 2-ketocarboxylate compound without using any enzyme. The process comprises a step of oxidizing a hydroxyacetate compound having an optionally-substituted sulfur-containing hydrocarbon group at 2-position in the presence of a vanadium compound. Preferably, the step is carried out further in the presence of oxygen, and more preferably, in the presence of an organic solvent.
摘要翻译：本发明提供了一种不使用任何酶制备含硫的2-酮羧酸盐化合物的新方法。该方法包括在钒化合物的存在下，在2-位氧化具有任选取代的含硫烃基的羟基乙酸酯化合物的步骤。优选地，该步骤在氧的存在下进一步进行，更优选在有机溶剂的存在下进行。

9. 发明授权

US08399710B2 Alkali metal fluoride dispersion and process for producing fluorine-containing organic compound using the same 失效
标题翻译：碱金属氟化物分散体及使用其的含氟有机化合物的制造方法
公开(公告)号：US08399710B2
公开(公告)日：2013-03-19
申请号：US12675042
申请日：2008-08-27
申请人： Koji Hagiya
发明人： Koji Hagiya
IPC分类号： C07C45/90
CPC分类号： C07B39/00 , C01D3/02 , C07C17/208 , C07C51/00 , C07C51/58 , C07C51/60 , C07C67/14 , C07C201/12 , C07C63/30 , C07C69/76 , C07C205/12
摘要： An alkali metal fluoride dispersion of an alkali metal fluoride and an aprotic organic solvent is obtainable by (A) separating a liquid phase from an alkali metal fluoride dispersion comprising an alcohol solvent and an alkali metal fluoride, and mixing the separated liquid phase with an aprotic organic solvent having a boiling point of 85° C. or higher at normal pressure; (B) obtaining a mixture containing the alkali metal fluoride by (b1) concentrating the mixture containing the alkali metal fluoride to obtain a concentrated fraction and a concentrated residue; (b2) mixing a residue of the alkali metal fluoride dispersion with the concentrated fraction obtained in (b1); and (b3) separating a liquid phase from the mixture containing an alkali metal fluoride obtained in (b2) and mixing the separated liquid phase with the concentrated residue; and (C) removing the alcohol solvent from the mixture containing the alkali metal fluoride.
摘要翻译：碱金属氟化物和非质子性有机溶剂的碱金属氟化物分散体可以通过（A）从包含醇溶剂和碱金属氟化物的碱金属氟化物分散液中分离液相，并将分离的液相与非质子常压下沸点为85℃以上的有机溶剂; （B）通过（b1）浓缩含有碱金属氟化物的混合物得到含有碱金属氟化物的混合物，得到浓缩馏分和浓缩残渣; （b2）将碱金属氟化物分散体的残渣与（b1）中得到的浓缩馏分混合; 和（b3）从含有（b2）中得到的碱金属氟化物的混合物中分离液相并将分离的液相与浓缩残余物混合; 和（C）从含有碱金属氟化物的混合物中除去醇溶剂。

10. 发明申请

US20130023696A1 PROCESS FOR PRODUCING SULFUR-CONTAINING AMINO ACIDS 审中-公开
标题翻译：生产含硫氨基酸的方法
公开(公告)号：US20130023696A1
公开(公告)日：2013-01-24
申请号：US13639210
申请日：2011-04-05
申请人： Koji Hagiya
发明人： Koji Hagiya
IPC分类号： C07C51/305
CPC分类号： C07C319/20 , C07C323/58
摘要： The present invention relates to a process for producing a sulfur-containing amino acid, comprising a step of oxidizing a 2-aminoethanol compound having, at position 2, a sulfur-containing hydrocarbon group having 1 to 24 carbon atoms in the presence of copper and water.
摘要翻译：本发明涉及一种生产含硫氨基酸的方法，包括在铜的存在下氧化在2位具有1至24个碳原子的含硫烃基的2-氨基乙醇化合物的步骤，和水。

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