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1. 发明申请

US20100087350A1 CAPPED POLYESTER POLYOL LUBRICANT COMPOSITION 审中-公开
标题翻译： CAPPED聚酯多元醇润滑剂组合物
公开(公告)号：US20100087350A1
公开(公告)日：2010-04-08
申请号：US12594137
申请日：2008-03-20
申请人： Mark F. Sonnenschein , Martin R. Greaves , Aaron W. Sanders , Zenon Lysenko , Gary E. Spilman , Joe D. Phillips , Alan K. Schrock , Steven J. Martin
发明人： Mark F. Sonnenschein , Martin R. Greaves , Aaron W. Sanders , Zenon Lysenko , Gary E. Spilman , Joe D. Phillips , Alan K. Schrock , Steven J. Martin
IPC分类号： C10M105/32
CPC分类号： C10M105/42 , C10M2207/301 , C10N2220/022 , C10N2220/025 , C10N2220/026 , C10N2220/10 , C10N2230/02 , C10N2230/06 , C10N2230/64 , C10N2260/02 , C10N2270/00
摘要： The present invention relates to polyester polyol lubricant compositions, some of which are capped, that include two or more chemically linked ester moieties, at least one of which derives from a seed or vegetable oil, and their preparation. The compositions have a pour point temperature of −10° centigrade or less without a pour point depressant and a viscosity at 25° centigrade within a range of 40 centipoises (0.04 pascal second) to 2000 centipoises (2 pascal seconds) when they either lack an initiator moiety or include an initiator moiety other than a dendritic initiator moiety, and a pour point temperature of −5° centigrade or less without a pour point depressant and a viscosity at 25° centigrade within a range of 40 centipoises (0.04 pascal second) to 8000 centipoises (8 pascal seconds) when they include a dendritic initiator moiety. The present invention also relates to a process for removing at least a portion of saturates from said compositions.
摘要翻译：本发明涉及聚酯多元醇润滑剂组合物，其中一些被封端，其包括两种或多种化学连接的酯部分，其中至少一种源自种子或植物油及其制备。组合物的倾点温度为-10℃或更低，没有倾点下降剂，并且在40厘泊（0.04帕斯卡秒）至2000厘泊（2帕斯卡秒）的范围内的25℃下的粘度，当它们缺乏引发剂部分或包括不同于树枝状引发剂部分的引发剂部分，并且倾点温度为-5℃或更低，而没有倾点下降剂，并且在25℃（0.04帕斯卡秒）至25℃的范围内的粘度在当它们包括树枝状引发剂部分时，为8000厘泊（8帕斯卡秒）。本发明还涉及从所述组合物中除去至少一部分饱和物的方法。

2. 发明授权

US08124812B2 Aldehyde compositions derived from seed oils 有权
标题翻译：衍生自种子油的醛组合物
公开(公告)号：US08124812B2
公开(公告)日：2012-02-28
申请号：US12565446
申请日：2009-09-23
申请人： Zenon Lysenko , Donald L. Morrison , David A. Babb , Donald L. Bunning , Christopher W. Derstine , James H. Gilchrist , H. Ray Jouett , Jeffrey S. Kanel , Kurt D. Olson , Wei-Jun Peng , Joe D. Phillips , Brian M. Roesch , Aaron W. Sanders , Alan K. Schrock , Pulikkottil J. Thomas
发明人： Zenon Lysenko , Donald L. Morrison , David A. Babb , Donald L. Bunning , Christopher W. Derstine , James H. Gilchrist , H. Ray Jouett , Jeffrey S. Kanel , Kurt D. Olson , Wei-Jun Peng , Joe D. Phillips , Brian M. Roesch , Aaron W. Sanders , Alan K. Schrock , Pulikkottil J. Thomas
IPC分类号： C07C47/02 , C07C45/50 , C07C29/14 , C07C59/147
CPC分类号： C08G18/4891 , C07C67/31 , C07C67/347 , C07C69/675 , C07C69/716 , C07C69/732 , C07C69/738 , C08G18/4072 , C08G18/4804 , C08G18/4841 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要： An aldehyde composition derived by hydroformylation of a transesterified seed oil and containing a mixture of formyl-substituted fatty acids or fatty acid esters having the following composition by weight: greater than about 10 to less than about 95 percent monoformyl, greater than about 1 to less than about 65 percent diformyl, and greater than about 0.1 to less than about 10 percent triformyl-substituted fatty acids or fatty acid esters, and having a diformyl to triformyl weight ratio of greater than about 5/1; preferably, greater than about 3 to less than about 20 percent saturates; and preferably, greater than about 1 to less than about 20 percent unsaturates.
摘要翻译：通过酯交换种子油的加氢甲酰化衍生的醛组合物，并含有具有以下重量组成的甲酰取代的脂肪酸或脂肪酸酯的混合物：大于约10至小于约95％的单甲基，大于约1至少并且具有大于约65％的二甲酰基和大于约0.1至小于约10％的三甲酰基取代的脂肪酸或脂肪酸酯，并且具有大于约5/1的二甲酰基 - 三甲酰基重量比; 优选大于约3至小于约20％的饱和物; 并且优选大于约1至小于约20％的不饱和度。

3. 发明授权

US07615658B2 Aldehyde and alcohol compositions derived from seed oils 有权
标题翻译：衍生自种子油的醛和醇组合物
公开(公告)号：US07615658B2
公开(公告)日：2009-11-10
申请号：US10551854
申请日：2004-04-22
申请人： Zenon Lysenko , Donald L. Morrison , David A. Babb , Donald L. Bunning , Christopher W. Derstine , James H. Gilchrist , H. Ray Jouett , Jeffrey S. Kanel , Kurt D. Olson , Wei-Jun Peng , Joe D. Phillips , Brian M. Roesch , Aaron W. Sanders , Alan K. Schrock , Pulikkottil J. Thomas
发明人： Zenon Lysenko , Donald L. Morrison , David A. Babb , Donald L. Bunning , Christopher W. Derstine , James H. Gilchrist , H. Ray Jouett , Jeffrey S. Kanel , Kurt D. Olson , Wei-Jun Peng , Joe D. Phillips , Brian M. Roesch , Aaron W. Sanders , Alan K. Schrock , Pulikkottil J. Thomas
IPC分类号： C07C51/367 , C07C27/00
CPC分类号： C08G18/4891 , C07C67/31 , C07C67/347 , C07C69/675 , C07C69/716 , C07C69/732 , C07C69/738 , C08G18/4072 , C08G18/4804 , C08G18/4841 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要： An aldehyde composition derived by hydroformylation of a transesterified seed oil and containing a mixture of formyl-substituted fatty acids or fatty acid esters having the following composition by weight: greater than about 10 to less than about 95 percent monoformyl, greater than about 1 to less than about 65 percent diformyl, and greater than about 0.1 to less than about 10 percent triformyl-substituted fatty acids or fatty acid esters, and having a diformyl to triformyl weight ratio of greater than about 5/1; preferably, greater than about 3 to less than about 20 percent saturates; and preferably, greater than about 1 to less than about 20 percent unsaturates. An alcohol composition derived by hydrogenation of the aforementioned aldehyde composition, containing a mixture of hydroxymethyl-substituted fatty acids or fatty acid esters having the following composition by weight: greater than about 10 to less than about 95 percent monoalcohol {mono(hydroxymethyl)}, greater than about 1 to less than about 65 percent diol {di(hydroxymethyl)}, greater than about 0.1 to less than about 10 percent triol, tri(hydroxymethyl)-substituted fatty acids or fatty acid esters; preferably greater than about 3 to less than about 35 percent saturates; and preferably, less than about 10 percent unsaturates. The alcohol composition can be converted into an oligomeric polyol for use in the manufacture of polyurethane slab stock flexible foam.
摘要翻译：通过酯交换种子油的加氢甲酰化衍生的醛组合物，并含有具有以下重量组成的甲酰取代的脂肪酸或脂肪酸酯的混合物：大于约10至小于约95％的单甲基，大于约1至少并且具有大于约65％的二甲酰基和大于约0.1至小于约10％的三甲酰基取代的脂肪酸或脂肪酸酯，并且具有大于约5/1的二甲酰基 - 三甲酰基重量比; 优选大于约3至小于约20％的饱和物; 并且优选大于约1至小于约20％的不饱和度。通过上述醛组合物的氢化衍生的醇组合物，其含有羟甲基取代的脂肪酸或具有以下重量组成的脂肪酸酯的混合物：大于约10至小于约95％的一元醇（单（羟甲基）}，大于约1至小于约65％的二醇{二（羟甲基）}，大于约0.1至小于约10％的三醇，三（羟甲基）取代的脂肪酸或脂肪酸酯; 优选大于约3至小于约35％的饱和物; 并且优选小于约10％的不饱和物。醇组合物可以转化为用于制造聚氨酯板坯柔性泡沫的低聚多元醇。

4. 发明申请

US20100048753A1 ALDEHYDE AND ALCOHOL COMPOSITIONS DERIVED FROM SEED OILS 审中-公开
标题翻译：来自种子油的醛和醇组合物
公开(公告)号：US20100048753A1
公开(公告)日：2010-02-25
申请号：US12518432
申请日：2007-12-03
申请人： Wei-Jun Peng , David A. Babb , Aaron W. Sanders , Christopher W. Derstine , Jorge Jimenez , Zenon Lysenko , Kurt D. Olson , Joe D. Phillips , Brian M. Roesch , Alan K. Schrock
发明人： Wei-Jun Peng , David A. Babb , Aaron W. Sanders , Christopher W. Derstine , Jorge Jimenez , Zenon Lysenko , Kurt D. Olson , Joe D. Phillips , Brian M. Roesch , Alan K. Schrock
IPC分类号： C08G18/00 , C07C53/00 , C07C69/34
CPC分类号： C08G18/36 , C08G2190/00
摘要： An aldehyde composition containing a mixture of mono-formyl-, diformyl-, and triformyl-substituted fatty acids and/or fatty acid esters having a di-aldehyde/tri-aldehyde weight ratio of less than 5/1 and an average functionality number from greater than 0.96 to less than 1.26. A monomer alcohol composition containing a mixture of mono-hydroxymethyl-, dihydroxymethyl-, and trihydroxymethyl-substituted fatty acids and/or fatty acid esters having a diol/triol weight ratio of less than 5/1 and an average functionality number from greater than 0.90 to less than 1.20. The monomer alcohol can be converted into an oligomeric polyol for use in the manufacture of polyurethane flexible foams.
摘要翻译：含有单甲酰基，二甲酰基和三甲酰基取代的脂肪酸和/或二醛/三醛重量比小于5/1的平均官能度数和/或脂肪酸酯的混合物的醛组合物，大于0.96小于1.26。含有单羟甲基 - ，二羟甲基 - 和三羟甲基取代的脂肪酸和/或二醇/三醇重量比小于5/1并且平均官能度数大于0.90的脂肪酸酯的混合物的单体醇组合物小于1.20。单体醇可以转化为用于制备聚氨酯柔性泡沫的低聚多元醇。

5. 发明申请

US20100298610A1 ALDEHYDE COMPOSITIONS DERIVED FROM SEED OILS 有权
标题翻译：从种子油中衍生的醛类组合物
公开(公告)号：US20100298610A1
公开(公告)日：2010-11-25
申请号：US12565446
申请日：2009-09-23
申请人： Zenon Lysenko , Donald L. Morrison , David A. Babb , Donald L. Bunning , Christopher W. Derstine , James H. Gilchrist , H. Ray Jouett , Kurt D. Olson , Wei-Jun Peng , Joe D. Phillips , Brian M. Roesch , Aaron W. Sanders , Alan K. Schrock , Pulikkottil J. Thomas , Jeffrey S. Kanel
发明人： Zenon Lysenko , Donald L. Morrison , David A. Babb , Donald L. Bunning , Christopher W. Derstine , James H. Gilchrist , H. Ray Jouett , Kurt D. Olson , Wei-Jun Peng , Joe D. Phillips , Brian M. Roesch , Aaron W. Sanders , Alan K. Schrock , Pulikkottil J. Thomas , Jeffrey S. Kanel
IPC分类号： C07C47/02
CPC分类号： C08G18/4891 , C07C67/31 , C07C67/347 , C07C69/675 , C07C69/716 , C07C69/732 , C07C69/738 , C08G18/4072 , C08G18/4804 , C08G18/4841 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要： An aldehyde composition derived by hydroformylation of a transesterified seed oil and containing a mixture of formyl-substituted fatty acids or fatty acid esters having the following composition by weight: greater than about 10 to less than about 95 percent monoformyl, greater than about 1 to less than about 65 percent diformyl, and greater than about 0.1 to less than about 10 percent triformyl-substituted fatty acids or fatty acid esters, and having a diformyl to triformyl weight ratio of greater than about 5/1; preferably, greater than about 3 to less than about 20 percent saturates; and preferably, greater than about 1 to less than about 20 percent unsaturates.
摘要翻译：通过酯交换种子油的加氢甲酰化衍生的醛组合物，并含有具有以下重量组成的甲酰取代的脂肪酸或脂肪酸酯的混合物：大于约10至小于约95％的单甲基，大于约1至少并且具有大于约65％的二甲酰基和大于约0.1至小于约10％的三甲酰基取代的脂肪酸或脂肪酸酯，并且具有大于约5/1的二甲酰基 - 三甲酰基重量比; 优选大于约3至小于约20％的饱和物; 并且优选大于约1至小于约20％的不饱和度。

6. 发明申请

US20100266799A1 PREPOLYMERS AND POLYMERS FOR ELASTOMERS 审中-公开
标题翻译：弹性体的制备物和聚合物
公开(公告)号：US20100266799A1
公开(公告)日：2010-10-21
申请号：US12668500
申请日：2008-07-09
申请人： William A. Koonce , Dwight D. Latham , Randall C. Jenkines , Debkumar Bhattacharjee , Zenon Lysenko , Hongyu Chen , Mark F. Sonnenschein , Klaus Schiller , Cora Leibig , Alan K. Schrock
发明人： William A. Koonce , Dwight D. Latham , Randall C. Jenkines , Debkumar Bhattacharjee , Zenon Lysenko , Hongyu Chen , Mark F. Sonnenschein , Klaus Schiller , Cora Leibig , Alan K. Schrock
IPC分类号： C08G18/10 , C08G18/34 , B32B1/08
CPC分类号： C08G18/4288 , C08G18/0885 , C08G18/10 , C08G18/4018 , C08G18/4833 , C08G18/4841 , C08G2101/0008 , C08J9/30 , C08J2375/04 , Y10T428/139 , C08G18/3275 , C08G18/3206 , C08G18/40
摘要： A prepolymer or elastomer is the reaction product of reactants (a) at least one polyester polyol or fatty acid derived polyol which is the reaction product of at least one initiator and a mixture of fatty acids or derivatives of fatty acids comprising at least about 45 weight percent monounsaturated fatty acids or derivatives thereof, (b) optionally, at least one polyol which is different from the polyol of (a); and (c) at least one isocyanate compound (herein after isocyanate) having an average of at least about 1.8 isocyanate groups per molecule. A process comprises admixing reactants (a) at least one polyol composition comprising the fatty acid derived polyol which is the reaction product of at least one initiator and a mixture of fatty acids or derivatives of fatty acids comprising at least about any of 45 weight percent monounsaturated fatty acids or derivatives thereof; and (b) at least one isocyanate having an average functionality of at least about 1.8 under reaction conditions to form a reaction product which is an elastomer or prepolymer is formed therefrom. An article, coating or thermoplastic polyurethane comprises the elastomer is formed from the prepolymer of or using the process of the invention.
摘要翻译：预聚物或弹性体是反应物（a）至少一种聚酯多元醇或脂肪酸衍生多元醇的反应产物，其是至少一种引发剂与脂肪酸或包含至少约45重量％的脂肪酸的衍生物的混合物的反应产物百分比的单不饱和脂肪酸或其衍生物，（b）任选的至少一种不同于（a）的多元醇的多元醇; 和（c）每分子平均具有至少约1.8个异氰酸酯基团的至少一种异氰酸酯化合物（本文中为异氰酸酯）。一种方法包括混合反应物（a）至少一种多元醇组合物，其包含脂肪酸衍生的多元醇，其是至少一种引发剂的反应产物和脂肪酸或脂肪酸的混合物的混合物，其至少包含约45重量％的单不饱和物脂肪酸或其衍生物; 和（b）在反应条件下至少一种具有至少约1.8的平均官能度的异氰酸酯形成由弹性体或预聚物形成的反应产物。一种制品，涂层或热塑性聚氨酯包括弹性体由本发明的预聚物或使用本发明的方法形成。

7. 发明授权

US06849666B2 Polyurethanes containing dispersed crystalline polyesters 失效
标题翻译：含有分散结晶聚酯的聚氨酯
公开(公告)号：US06849666B2
公开(公告)日：2005-02-01
申请号：US10332310
申请日：2001-05-15
申请人： Hanno R. Van der Wal , Mark F. Sonnenschein , Alan K. Schrock , Francois Casati , Christopher P. Christenson , Zenon Lysenko , Jozef Bicerano , Fabio Aguirre , Sudhakar Balijepalli
发明人： Hanno R. Van der Wal , Mark F. Sonnenschein , Alan K. Schrock , Francois Casati , Christopher P. Christenson , Zenon Lysenko , Jozef Bicerano , Fabio Aguirre , Sudhakar Balijepalli
IPC分类号： C08G18/10 , C08G18/40 , C08G18/42 , C08G18/48 , C08G101/00 , C08G18/28
CPC分类号： C08G18/4841 , C08G18/10 , C08G18/4018 , C08G18/409 , C08G18/4266 , C08G18/4277 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08G2250/00 , C08G18/48
摘要： A process is disclosed for producing resilient polyurethane foams by foaming an organic polyisocyanate, an iso-cyanate-reactive compound and a fusible polymer. The improvement in the hardness of the foams is achieved without adversely affecting the other properties of the foams, such as tensile strength and elongation.
摘要翻译：公开了通过使有机多异氰酸酯，异氰酸酯反应性化合物和易熔聚合物发泡来生产弹性聚氨酯泡沫体的方法。实现泡沫塑料的硬度的改善，而不会不利地影响泡沫的其它性能，例如拉伸强度和伸长率。

8. 发明申请

US20090312450A1 POLYURETHANES MADE FROM HYDROXYL-CONTAINING FATTY ACID AMIDES 审中-公开
标题翻译：含羟基脂肪酸的聚氨酯
公开(公告)号：US20090312450A1
公开(公告)日：2009-12-17
申请号：US11996505
申请日：2006-07-26
申请人： Charles A. Martin , Aaron W. Sanders , Jimmy D. Earls , Kurt D. Olson , John R. Briggs , Alan K. Schrock , Zenon Lysenko , David A. Babb
发明人： Charles A. Martin , Aaron W. Sanders , Jimmy D. Earls , Kurt D. Olson , John R. Briggs , Alan K. Schrock , Zenon Lysenko , David A. Babb
IPC分类号： C08G18/34 , C08G18/32 , C07C229/02
CPC分类号： C08G18/3825 , C07C235/08 , C08G18/36 , C08G2101/0025 , C08G2101/005
摘要： Polyurethanes, and rigid polyurethane foams in particular, are made using certain amides of modified fatty acids. The fatty acid groups are substituted hydroxymethyl, N-hydroxyalkyl aminoalkyl or hydroxy-substituted ester groups. The amide portion of the molecule contains hydroxyalkyl or other hydroxyl-substituted organic groups bonded to the amide nitrogen.
摘要翻译：聚氨酯和硬质聚氨酯泡沫特别是使用某些改性脂肪酸酰胺制成的。脂肪酸基团是取代的羟甲基，N-羟基烷基氨基烷基或羟基取代的酯基。分子的酰胺部分含有与酰胺氮键合的羟基烷基或其它羟基取代的有机基团。

9. 发明申请

US20100249357A1 ROOM TEMPERATURE CURABLE POLYMERS AND PRECURSORS THEREOF 有权
公开(公告)号：US20100249357A1
公开(公告)日：2010-09-30
申请号：US12668609
申请日：2008-07-10
申请人： Paul J. Popa , Zenon Lysenko , David A. Babb , William A. Koonce , Gary E. Spilman
发明人： Paul J. Popa , Zenon Lysenko , David A. Babb , William A. Koonce , Gary E. Spilman
IPC分类号： C08G18/42 , C08G63/00
CPC分类号： C08G18/4288 , C08G18/4269 , C08G18/4277 , C08G18/718 , C08G2190/00 , C09J175/06
摘要： A polyester polyol, referred to hereinafter as a MHMS polyol comprises fatty acid based mer units wherein at least about 80 weight percent of the fatty acid based mer units are from methyl 9 (10) hydroxymethylstearate, or is prepared from an oil having fatty acids or fatty acid esters which are at least about 80 weight percent oleic acid or esters thereof and which has an average hydroxyl functionality of from 1.5 to 4. A reaction product, referred to herein after as MHMS alkoxysilane prepolymer, is produced from at least one such MHMS polyol and at least one isocyanate functional silane. The prepolymer is moisture cured to form a silylated MHMS polymer. The process of preparing a MHMS polyol comprises (A) reacting a fatty acid ester wherein at least about 80 weight percent of the fatty acid esters are methyl 9 (10) hydroxymethylstearate, or are prepared from an oil having fatty acids or fatty acid esters which are at least about 80 weight percent oleic acid or esters thereof with an initiator having at least 2 reactive groups selected from primary hydroxyl groups, amine groups, terminal isocyanate groups, terminal carbonyl groups or a combination thereof. The process of preparing at least one MHMS alkoxysilane prepolymer comprises steps of: (a) supplying at least one MHMS polyol; (b) supplying at least one isocyanate functional silane and (c) admixing the MHMS polyol and isocyanate functional silane or combination thereof, optionally in the presence of at least one catalyst to produce at least one MHMS alkoxysilane prepolymer. A process of preparing at least one silylated MHMS polymer comprises steps of: (a) supplying at least one MHMS alkoxysilane prepolymer; and (b) exposing it to moisture under conditions such that at least one silylated MHMS polymer is formed. Articles comprising the polyol, prepolymer, or polymer include elastomers, sealants, adhesives, coatings and the like.

10. 发明授权

US08178645B2 Room temperature curable polymers and precursors thereof 有权
标题翻译：室温固化聚合物及其前体
公开(公告)号：US08178645B2
公开(公告)日：2012-05-15
申请号：US12668609
申请日：2008-07-10
申请人： Paul J. Popa , Zenon Lysenko , David A. Babb , William A. Koonce , Gary E. Spilman
发明人： Paul J. Popa , Zenon Lysenko , David A. Babb , William A. Koonce , Gary E. Spilman
IPC分类号： C08G18/42 , C08G63/00 , C08G18/71
CPC分类号： C08G18/4288 , C08G18/4269 , C08G18/4277 , C08G18/718 , C08G2190/00 , C09J175/06
摘要： A polyester polyol, referred to hereinafter as a MHMS polyol comprises fatty acid based mer units wherein at least about 80 weight percent of the fatty acid based mer units are from methyl 9 (10) hydroxymethylstearate, or is prepared from an oil having fatty acids or fatty acid esters which are at least about 80 weight percent oleic acid or esters thereof and which has an average hydroxyl functionality of from 1.5 to 4. A reaction product, referred to herein after as MHMS alkoxysilane prepolymer, is produced from at least one such MHMS polyol and at least one isocyanate functional silane. This prepolymer is moisture cured to form a silylated MHMS polymer.
摘要翻译：以下称为MHMS多元醇的聚酯多元醇包括脂肪酸基mer单元，其中至少约80重量％的脂肪酸基mer单元为9（10）羟甲基硬脂酸甲酯，或由具有脂肪酸或至少约80重量％的油酸或其酯，并且其平均羟基官能度为1.5-4的脂肪酸酯。本文中称为MHMS烷氧基硅烷预聚物的反应产物由至少一种这样的MHMS 多元醇和至少一种异氰酸酯官能的硅烷。将该预聚物水分固化以形成甲硅烷基化的MHMS聚合物。

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