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1. 发明申请

US20060116530A1 Optimized liquid-phase oxidation 有权
公开(公告)号：US20060116530A1
公开(公告)日：2006-06-01
申请号：US11154202
申请日：2005-06-16
申请人： Alan Wonders , Robert Lin , Lee Partin , Marcel de Vreede , Wayne Strasser
发明人： Alan Wonders , Robert Lin , Lee Partin , Marcel de Vreede , Wayne Strasser
IPC分类号： C07C51/255 , C07C51/16
CPC分类号： C07C51/16 , C07C51/21 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

2. 发明申请

US20060047163A1 Optimized liquid-phase oxidation 有权
公开(公告)号：US20060047163A1
公开(公告)日：2006-03-02
申请号：US11154504
申请日：2005-06-16
申请人： Marcel de Vreede , Alan Wonders , Robert Lin
发明人： Marcel de Vreede , Alan Wonders , Robert Lin
IPC分类号： C07C51/265
CPC分类号： B01J4/002 , B01F3/04248 , B01F3/04496 , B01F2003/04361 , B01J8/008 , B01J8/1818 , B01J8/22 , B01J8/228 , B01J2208/003 , B01J2208/00539 , B01J2208/0061 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

3. 发明申请

US20060047159A1 Optimized liquid-phase oxidation 有权
公开(公告)号：US20060047159A1
公开(公告)日：2006-03-02
申请号：US11154218
申请日：2005-06-16
申请人： Alan Wonders , Robert Lin , Marcel de Vreede , Lee Partin
发明人： Alan Wonders , Robert Lin , Marcel de Vreede , Lee Partin
IPC分类号： C07C51/265
CPC分类号： B01J8/1818 , B01J4/002 , B01J8/1872 , B01J8/22 , B01J8/226 , B01J2208/0084 , B01J2219/00006 , B01J2219/0004 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

4. 发明授权

US07692036B2 Optimized liquid-phase oxidation 有权
公开(公告)号：US07692036B2
公开(公告)日：2010-04-06
申请号：US11154202
申请日：2005-06-16
申请人： Alan George Wonders , Robert Lin , Lee Reynolds Partin , Marcel de Vreede , Wayne Scott Strasser
发明人： Alan George Wonders , Robert Lin , Lee Reynolds Partin , Marcel de Vreede , Wayne Scott Strasser
IPC分类号： C07C51/16
CPC分类号： C07C51/16 , C07C51/21 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

5. 发明申请

US20090155143A1 Optimized Liquid-Phase Oxidation 有权
公开(公告)号：US20090155143A1
公开(公告)日：2009-06-18
申请号：US12392119
申请日：2009-02-25
申请人： Alan George Wonders , Robert Lin , Marcel de Vreede , Lee Reynolds Partin
发明人： Alan George Wonders , Robert Lin , Marcel de Vreede , Lee Reynolds Partin
IPC分类号： B01J19/00
CPC分类号： B01J8/1818 , B01J4/002 , B01J8/1872 , B01J8/22 , B01J8/226 , B01J2208/0084 , B01J2219/00006 , B01J2219/0004 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

6. 发明申请

US20090136397A1 Optimized Liquid-Phase Oxidation 审中-公开
公开(公告)号：US20090136397A1
公开(公告)日：2009-05-28
申请号：US12362811
申请日：2009-01-30
申请人： Marcel De Vreede , Alan George Wonders , Robert Lin
发明人： Marcel De Vreede , Alan George Wonders , Robert Lin
IPC分类号： B01J19/00
CPC分类号： B01J4/002 , B01F3/04248 , B01F3/04496 , B01F2003/04361 , B01J8/008 , B01J8/1818 , B01J8/22 , B01J8/228 , B01J2208/003 , B01J2208/00539 , B01J2208/0061 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

7. 发明授权

US07381386B2 Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid 有权
标题翻译：在合成羧酸时从母液中除去杂质的提取过程
公开(公告)号：US07381386B2
公开(公告)日：2008-06-03
申请号：US10455018
申请日：2003-06-05
申请人： Robert Lin , Marcel de Vreede
发明人： Robert Lin , Marcel de Vreede
IPC分类号： C07C51/00
CPC分类号： C07C51/42 , C07C51/48 , Y02P20/52 , C07C63/26
摘要： A method for removing impurities from a mother liquor comprising a carboxylic acid, a metal catalyst, impurities by (a) evaporating the mother liquor comprising a carboxylic acid, a metal catalyst, impurities and a solvent in a first evaporator zone to produce a vapor stream and a concentrated mother liquor stream; (b) evaporating the concentrated mother liquor stream in a second evaporator zone to form a solvent rich stream and a super concentrated mother liquor stream; (c) mixing in a mixing zone a water-solvent solution and optionally an extraction solvent with the super concentrated mother liquor stream to form an aqueous mixture; (d) optionally separating organic impurities from the aqueous mixture in a solid-liquid separation zone to form a purified aqueous mixture; and (e) extracting the aqueous mixture or purified aqueous mixture with an extraction solvent in an extraction zone to form an extract stream and the raffinate stream.
摘要翻译：一种通过（a）在第一蒸发区中蒸发包含羧酸，金属催化剂，杂质和溶剂的母液，从含有羧酸，金属催化剂，杂质的母液中除去杂质的方法，以产生蒸气流和浓浓的母液流; （b）在第二蒸发器区域蒸发浓缩的母液流以形成富溶剂流和超浓缩母液流; （c）在混合区中将水溶剂溶液和任选的萃取溶剂与超浓缩母液流混合以形成含水混合物; （d）任选地在固液分离区中从含水混合物中分离出有机杂质以形成纯化的含水混合物; 和（e）在提取区中用提取溶剂萃取含水混合物或纯化的含水混合物以形成提取物流和萃余液流。

8. 发明申请

US20080161598A1 Optimized Production of Aromatic Dicarboxylic Acids 审中-公开
标题翻译：优化芳香族二羧酸的生产
公开(公告)号：US20080161598A1
公开(公告)日：2008-07-03
申请号：US12050253
申请日：2008-03-18
申请人： Robert Lin , Marcel de Vreede
发明人： Robert Lin , Marcel de Vreede
IPC分类号： C07C51/16
CPC分类号： C07C51/487 , B01J2219/00006 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently producing aromatic dicarboxylic acids (e.g., terephthalic acid). In one embodiment the process/apparatus reduces costs by recovering and purifying residual terephthalic acid present in the liquid phase of an initial oxidation slurry. In another embodiment the process apparatus reduces costs associated with hydrogenation by forming a final composite product containing unhydrogenated acid particles.
摘要翻译：公开了用于更有效地制备芳族二羧酸（例如对苯二甲酸）的优化方法和装置。在一个实施方案中，方法/装置通过回收和纯化存在于初始氧化浆液的液相中的残余对苯二甲酸来降低成本。在另一个实施方案中，加工装置通过形成含有未氢化的酸性颗粒的最终复合产品来降低与氢化相关的成本。

9. 发明申请

US20080159929A1 Optimized Production of Aromatic Dicarboxylic Acids 有权
标题翻译：优化芳香族二羧酸的生产
公开(公告)号：US20080159929A1
公开(公告)日：2008-07-03
申请号：US12050251
申请日：2008-03-18
申请人： Robert Lin , Marcel de Vreede
发明人： Robert Lin , Marcel de Vreede
IPC分类号： C07C51/43
CPC分类号： C07C51/487 , B01J2219/00006 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically producing aromatic discarboxylic acids. The process reduces costs associated with hydrogenation by forming a final composite product containing unhydrogenated acid particles.
摘要翻译：公开了一种用于更有效和经济地生产芳族四羧酸的优化方法和装置。该方法通过形成含有未氢化的酸性颗粒的最终复合产物来降低与氢化相关的成本。

10. 发明授权

US07351396B2 Extraction process for removal of impurities from an aqueous mixture 有权
标题翻译：从含水混合物中除去杂质的萃取方法
公开(公告)号：US07351396B2
公开(公告)日：2008-04-01
申请号：US10455017
申请日：2003-06-05
申请人： Robert Lin , Marcel de Vreede
发明人： Robert Lin , Marcel de Vreede
IPC分类号： C07C51/43 , B01J31/00
CPC分类号： C07C51/42 , C07C51/48 , C07C63/26
摘要： A method for removing impurities from an aqueous mixture or purified aqueous by extracting the aqueous mixture or purified aqueous mixture with an extraction solvent in an extraction zone to form an extract stream and the raffinate stream; and optionally separating the extract stream and a solvent rich stream in a separation zone to form a high boiling point organic impurities stream and a recovered extraction solvent stream.
摘要翻译：一种通过在提取区提取含水混合物或纯化的含水混合物从水性混合物或纯化水中除去杂质的方法，以形成提取物流和萃余液流; 并且可选地在分离区中分离提取物流和富溶剂流以形成高沸点有机杂质流和回收的萃取溶剂流。

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