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1. 发明授权

US5420085A Methods of making composite aluminum nitride ceramic articles having embedded filler 失效
标题翻译：制备具有嵌入填料的复合氮化铝陶瓷制品的方法
公开(公告)号：US5420085A
公开(公告)日：1995-05-30
申请号：US7387
申请日：1993-01-21
申请人： Marc S. Newkirk , Harry R. Zwicker , Andrew W. Urquhart , Harold D. Lesher , Terry D. Claar , Michael K. Aghajanian , John P. Biel, Jr.
发明人： Marc S. Newkirk , Harry R. Zwicker , Andrew W. Urquhart , Harold D. Lesher , Terry D. Claar , Michael K. Aghajanian , John P. Biel, Jr.
IPC分类号： C04B35/65 , C04B35/76 , C04B35/80 , C04B41/50 , C04B41/87 , C04B35/58
CPC分类号： C04B41/5025 , C04B35/652 , C04B35/76 , C04B35/80 , C04B41/87
摘要： A method of making self-supporting ceramic composite structures having filler embedded therein includes infiltrating a permeable mass of filler with polycrystalline material comprising an oxidation reaction product obtained by oxidation of a parent metal such as aluminum and optionally, containing therein non-oxidized constituents of the parent metal. The structure is formed by placing a parent metal adjacent to a permeable filler and heating the assembly to melt the parent metal and provide a molten body of parent metal which is contacted with a suitable vapor-phase oxidant. Within a certain temperature region and optionally, aided by one or more dopants in or on the parent metal, molten parent metal will migrate through previously formed oxidation reaction product into contact with the oxidant, causing the oxidation reaction product to grow so as to embed the adjacent filler and provide the composite structure. In a preferred embodiment, a parent metal comprising aluminum is oxidized by a vapor-phase oxidant comprising nitrogen to form a ceramic matrix comprising an aluminum nitride oxidation reaction product. In a particularly preferred embodiment, one or more protective coatings are applied to the filler prior to formation of the aluminum nitride oxidation reaction product matrix.
摘要翻译：制造具有嵌入其中的填料的自支撑陶瓷复合结构的方法包括用多晶材料渗透可渗透的填料，所述多晶材料包含通过氧化母体金属如铝而获得的氧化反应产物，并且任选地含有其中的非氧化成分母金属。通过将母体金属放置在可渗透填料附近并加热该组件以熔化母体金属并提供与合适的气相氧化剂接触的母体金属的熔融体来形成结构。在一定温度范围内，任选地，由母体金属中或母体金属上的一种或多种掺杂剂辅助，熔融母体金属将迁移通过预先形成的氧化反应产物与氧化剂接触，使氧化反应产物生长，从而嵌入相邻填料并提供复合结构。在优选的实施方案中，包含铝的母体金属被包含氮的气相氧化剂氧化以形成包含氮化铝氧化反应产物的陶瓷基体。在特别优选的实施方案中，在形成氮化铝氧化反应产物基质之前，将一种或多种保护性涂料施加到填料上。

2. 发明授权

US5518061A Method of modifying the properties of a metal matrix composite body 失效
标题翻译：改性金属基复合体的性能的方法
公开(公告)号：US5518061A
公开(公告)日：1996-05-21
申请号：US199413
申请日：1994-02-22
申请人： Marc S. Newkirk , Andrew W. Urquhart , Michael K. Aghajanian , Mark G. Mortenson , Vilupanur A. Ravi , Alan S. Nagelberg
发明人： Marc S. Newkirk , Andrew W. Urquhart , Michael K. Aghajanian , Mark G. Mortenson , Vilupanur A. Ravi , Alan S. Nagelberg
IPC分类号： C04B41/52 , C04B41/89 , C22C1/10 , B22D19/14 , B22D19/00
CPC分类号： C04B41/89 , C04B41/52 , C22C1/1036 , C22C2001/1057 , C22C2001/1063
摘要： The present invention relates to modifying the properties of a metal matrix composite body by a post formation process treatment and/or a substantially contiguous modification treatment. The post formation process treatment may be applicable to a variety of metal matrix composite bodies produced by various techniques, and is particularly applicable to modifying the properties of a metal matrix composite body produced by a spontaneous infiltration technique. The substantially contiguous modification process may also be used primarily in conjunction with metal matrix composite bodies produced according to a spontaneous infiltration technique. Particularly, at least a portion of the matrix metal of the metal matrix composite body and/or the filler material of the metal matrix composite body is modified or altered during and/or after the formation process.
摘要翻译：本发明涉及通过后形成工艺处理和/或基本相邻的改性处理来改性金属基质复合体的性质。后形成处理可以适用于通过各种技术制造的各种金属基复合体，特别适用于通过自发渗透技术制造的金属基复合体的特性。基本相邻的改性方法也可以主要与根据自发渗透技术制备的金属基质复合体一起使用。特别地，金属基体复合体的基质金属和/或金属基体复合体的填充材料的至少一部分在形成过程中和/或之后被修饰或改变。

3. 发明授权

US5301738A Method of modifying the properties of a metal matrix composite body 失效
标题翻译：改性金属基复合体的性能的方法
公开(公告)号：US5301738A
公开(公告)日：1994-04-12
申请号：US841241
申请日：1992-02-24
申请人： Marc S. Newkirk , Andrew W. Urquhart , Michael K. Aghajanian , Mark G. Mortenson , Vilupanur A. Ravi , Alan S. Nagelberg
发明人： Marc S. Newkirk , Andrew W. Urquhart , Michael K. Aghajanian , Mark G. Mortenson , Vilupanur A. Ravi , Alan S. Nagelberg
IPC分类号： C04B41/52 , C04B41/89 , C22C1/10 , B22D19/14
CPC分类号： C04B41/52 , C04B41/89 , C22C1/1036
摘要： The present invention relates to modifying the properties of a metal matrix composite body by a post formation process modification treatment. The post formation process treatment may be applicable to a variety of metal matrix composite bodies produced by various techniques, and is particularly applicable to modifying the properties of a metal matrix composite body produced by a spontaneous infiltration technique. Particularly, at least a portion of the matrix metal of the metal matrix composite body and/or the filler material of the metal matrix composite body is modified or altered after the formation process. Preferably, the preform contains a second non-metal material, an infiltration enhancer of infiltration enhancer precursor, and an infiltration atmosphere.
摘要翻译：本发明涉及通过后形成工艺改性处理改性金属基复合体的性能。后形成处理可以适用于通过各种技术制造的各种金属基复合体，特别适用于通过自发渗透技术制造的金属基复合体的特性。特别地，金属基体复合体的基体金属的至少一部分和/或金属基复合体的填充材料在形成工序之后被修改或改变。优选地，预成型体包含第二非金属材料，渗透增强剂前体的渗透增强剂和渗透气氛。

4. 发明授权

US5000248A Method of modifying the properties of a metal matrix composite body 失效
标题翻译：改性金属基复合体的性能的方法
公开(公告)号：US5000248A
公开(公告)日：1991-03-19
申请号：US269309
申请日：1988-11-10
申请人： Marc S. Newkirk , Andrew W. Urquhart , Michael K. Aghajanian , Mark G. Mortenson
发明人： Marc S. Newkirk , Andrew W. Urquhart , Michael K. Aghajanian , Mark G. Mortenson
IPC分类号： B22D19/14 , B22D19/16 , C04B41/52 , C04B41/89 , C22C1/10 , C22C21/00 , C22C47/08
CPC分类号： C04B41/009 , C04B41/52 , C04B41/89 , C22C1/1036 , C04B2111/00931
摘要： The present invention relates to modifying the properties of a metal matrix composite body by a post formation process treatment and/or a substantially contiguous modification treatment. The post formation process treatment may be applicable to a variety of metal matrix composite bodies produced by various techniques, and is particularly applicable to modifying the properties of a metal matrix composite body produced by a spontaneous infiltration technique. The substantially contiguous modification process may also be used primarily in conjunction with metal matrix composite bodies produced according to a spontaneous infiltration technique. Particularly, at least a portion of the matrix metal of the metal matrix composite body and/or the filler material of the metal matrix composite body is modified or altered during and/or after the formation process.

5. 发明授权

US5303763A Directional solidification of metal matrix composites 失效
标题翻译：金属基复合材料的定向凝固
公开(公告)号：US5303763A
公开(公告)日：1994-04-19
申请号：US980418
申请日：1992-11-23
申请人： Michael K. Aghajanian , Robert C. Kantner , John P. Biel, Jr. , Kurt J. Becker
发明人： Michael K. Aghajanian , Robert C. Kantner , John P. Biel, Jr. , Kurt J. Becker
IPC分类号： C04B41/51 , C04B41/88 , C22C1/10 , B22D19/14
CPC分类号： C04B41/5155 , C04B41/009 , C04B41/88 , C22C1/1036 , B22F2003/1014 , C04B2111/00931 , C22C2001/1063
摘要： A metal matrix composite is formed by contacting a molten matrix metal with a permeable mass of filler material or preform in the presence of an infiltrating atmosphere. Under these conditions, the molten matrix metal will spontaneously infiltrate the permeable mass of filler material or preform under normal atmospheric pressures. Once a desired amount of spontaneous infiltration has been achieved, or during the spontaneous infiltration step, the matrix metal which has infiltrated the permeable mass of filler material or preform is directionally solidified. The directionally solidified metal matrix composite may be heated to a temperature in excess of the liquidus temperature of the matrix metal and quenched. This technique allows the production of spontaneously infiltrated metal matrix composites having improved microstructures and properties.
摘要翻译：金属基质复合材料是通过使熔融基体金属与可渗透的填料或预成型体在渗透气氛下接触而形成的。在这些条件下，熔融基质金属将在正常大气压力下自发渗透填料或预型体的渗透物质。一旦实现了所需量的自发渗透，或者在自发渗透步骤期间，渗透了填充材料或预型体的可渗透物质的基质金属被定向凝固。可以将定向凝固的金属基质复合材料加热到超过基质金属的液相线温度并淬火。该技术允许生产具有改进的微结构和性质的自发渗透的金属基质复合材料。

6. 发明授权

US5249621A Method of forming metal matrix composite bodies by a spontaneous infiltration process, and products produced therefrom 失效
标题翻译：通过自发渗透法形成金属基体复合体的方法及其制备的产品
公开(公告)号：US5249621A
公开(公告)日：1993-10-05
申请号：US863894
申请日：1992-04-06
申请人： Michael K. Aghajanian , Gregory E. Hannon , Russell G. Smith , John P. Biel, Jr. , John T. Burke , Christopher R. Kennedy , Michael A. Roczella , Kurt J. Becker , Thomas J. Henderson
发明人： Michael K. Aghajanian , Gregory E. Hannon , Russell G. Smith , John P. Biel, Jr. , John T. Burke , Christopher R. Kennedy , Michael A. Roczella , Kurt J. Becker , Thomas J. Henderson
IPC分类号： C04B41/51 , C04B41/88 , C22C1/10 , B22D19/14
CPC分类号： C22C1/1036 , C04B41/5155 , C04B41/88 , C22C2001/1063
摘要： The present invention relates to a novel process for forming metal matrix composite bodies. Particularly, an infiltration enhancer and/or an infiltration enhancer precursor and/or an infiltrating atmosphere are in communication with a filler material or a preform, at least at some point during the process, which permits molten matrix metal to spontaneously infiltrate the filler material or preform. Such spontaneous infiltration occurs without the requirement for the application of any pressure or vacuum.
摘要翻译：本发明涉及一种形成金属基复合体的新方法。特别地，渗透增强剂和/或渗透增强剂前体和/或渗透气氛至少在该过程中的某一点与填料或预型体连通，这允许熔融基质金属自发地渗透填料或预制件。发生这种自发性渗透，而不需要施加任何压力或真空。

7. 发明授权

US5020583A Directional solidification of metal matrix composites 失效
标题翻译：金属基复合材料的定向凝固
公开(公告)号：US5020583A
公开(公告)日：1991-06-04
申请号：US269602
申请日：1988-11-10
申请人： Michael K. Aghajanian , Robert C. Kantner , John P. Biel, Jr.
发明人： Michael K. Aghajanian , Robert C. Kantner , John P. Biel, Jr.
IPC分类号： B22D19/14 , B22D27/04 , C04B41/51 , C04B41/88 , C22C1/10 , C22C21/00 , C22C47/08
CPC分类号： C04B41/009 , C04B41/5155 , C04B41/88 , C22C1/1036 , B22F2003/1014 , C04B2111/00931 , C22C2001/1063
摘要： A metal matrix composite is formed by contacting a molten matrix alloy with a permeable mass of filler material or preform in the presence of an infiltrating atmosphere. Under these conditions, the molten matrix alloy will spontaneously infiltrate the permeable mass of filler material or preform under normal atmospheric pressures. Once a desired amount of spontaneous infiltration has been achieved, or during the spontaneous infiltration step, the matrix metal which has infiltrated the permeable mass of filler material or preform is directionally solidified. This technique allows the production of spontaneously infiltrated metal matrix composites having improved microstructures and properties.

8. 发明授权

US5482778A Method of making metal matrix composite with the use of a barrier 失效
标题翻译：使用屏障制作金属基复合材料的方法
公开(公告)号：US5482778A
公开(公告)日：1996-01-09
申请号：US179463
申请日：1994-01-10
申请人： Michael K. Aghajanian , Terry D. Claar
发明人： Michael K. Aghajanian , Terry D. Claar
IPC分类号： C04B35/65 , C04B41/51 , C04B41/88 , C22C1/10 , C04B35/00
CPC分类号： C04B35/652 , C04B41/5155 , C04B41/88 , C22C1/1036 , C22C2001/1063 , Y10T428/12007 , Y10T428/12486 , Y10T428/12576 , Y10T428/12583 , Y10T428/12736 , Y10T428/30
摘要： A net shaped ceramic-reinforced aluminum matrix composite is provided by forming a permeable mass of ceramic material with a defined surface boundary having a barrier, and contacting a molten aluminum-magnesium alloy with the permeable mass of ceramic material in the presence of a gas comprising from about 10 to 100% nitrogen, by volume, balance nonoxidizing gas, e.g. hydrogen or argon. Under these conditions, the molten alloy spontaneously infiltrates the ceramic mass under normal atmospheric pressures until it reaches the barrier. A solid body of the alloy can be placed adjacent to a permeable bedding of ceramic material having a barrier, and brought to the molten state, preferably to at least about 700.degree. C., in order to form the net shape aluminum matrix composite by spontaneous infiltration. In addition to magnesium, auxiliary alloying elements may be employed with aluminum. The resulting composite products may contain a discontinuous aluminum nitride phase in the aluminum matrix.
摘要翻译：通过形成具有限定的具有阻挡层的表面边界的陶瓷材料的可渗透物质，并且在熔融的铝 - 镁合金与可渗透的陶瓷材料的物质的存在下，在气体存在下接触，形成网状陶瓷增强的铝基复合材料，所述气体包括约10至100％的氮气（体积），平衡非氧化气体，例如氢或氩。在这些条件下，熔融合金在正常大气压力下自发渗透到陶瓷块中直至达到屏障。合金的固体可以邻近具有阻挡层的陶瓷材料的可渗透层，并且进入熔融状态，优选至少约700℃，以便通过自发形成网状铝基复合材料浸润。除了镁之外，辅助合金元素可以与铝一起使用。所得到的复合产品可能在铝基体中含有不连续的氮化铝相。

9. 发明授权

US5277989A Metal matrix composite which utilizes a barrier 失效
标题翻译：使用屏障的金属基复合材料
公开(公告)号：US5277989A
公开(公告)日：1994-01-11
申请号：US934823
申请日：1992-08-24
申请人： Michael K. Aghajanian , Terry D. Claar
发明人： Michael K. Aghajanian , Terry D. Claar
IPC分类号： C04B35/65 , C04B41/51 , C04B41/88 , C22C1/10 , C22C29/16
CPC分类号： C04B35/652 , C04B41/5155 , C04B41/88 , C22C1/1036 , C22C2001/1063 , Y10T428/12007 , Y10T428/12486 , Y10T428/12576 , Y10T428/12583 , Y10T428/12736 , Y10T428/30
摘要： A net shaped ceramic-reinforced aluminum matrix composite is formed by forming a permeable mass of ceramic material with a defined surface boundary having a barrier, and contacting a molten aluminum-magnesium alloy with the permeable mass of ceramic material in the presence of a gas comprising from about 10 to 100% nitrogen, by volume, balance nonoxidizing gas, e.g. hydrogen or argon. Under these conditions, the molten alloy spontaneously infiltrates the ceramic mass under normal atmospheric pressures until it reaches the barrier. A solid body of the alloy can be placed adjacent to a permeable bedding of ceramic material having a barrier, and brought to the molten state, preferably to at least about 700.degree. C., in order to form the net shape aluminum matrix composite by infiltration. In addition to magnesium, auxiliary alloying elements may be employed with aluminum. The resulting composite products may contain a discontinuous aluminum nitride phase in the aluminum matrix.
摘要翻译：网状陶瓷增强铝基复合材料通过形成具有限定的具有阻挡层的表面边界的陶瓷材料的可渗透物质形成，并且在熔融的铝 - 镁合金与可渗透物质的陶瓷材料的存在下，约10至100％的氮气（体积），平衡非氧化气体，例如氢或氩。在这些条件下，熔融合金在正常大气压力下自发渗透到陶瓷块中直至达到屏障。合金的固体可以放置在与具有阻挡层的陶瓷材料的可渗透层合物附近，并且进入熔融状态，优选至少约700℃，以便通过渗透形成网状铝基复合材料。除了镁之外，辅助合金元素可以与铝一起使用。所得到的复合产品可能在铝基体中含有不连续的氮化铝相。

10. 发明授权

US5180697A Process for preparing self-supporting bodies and products produced thereby 失效
标题翻译：制备自支撑体及其生产产品的方法
公开(公告)号：US5180697A
公开(公告)日：1993-01-19
申请号：US551306
申请日：1990-07-12
申请人： Terry D. Claar , Steven M. Mason , Kevin P. Pochopien , Danny R. White , William B. Johnson , Michael K. Aghajanian
发明人： Terry D. Claar , Steven M. Mason , Kevin P. Pochopien , Danny R. White , William B. Johnson , Michael K. Aghajanian
IPC分类号： C04B35/58 , C04B35/65 , C04B41/50 , C04B41/87 , C22C29/00
CPC分类号： C04B35/653 , C04B35/56 , C04B35/5607 , C04B35/5611 , C04B35/5622 , C04B35/5805 , C04B35/58064 , C04B35/58071 , C04B35/58078 , C04B35/652 , C04B41/5062 , C04B41/507 , C04B41/87 , C22C29/00
摘要： Self-supporting bodies are produced by reactive infiltration of a parent metal into a boron carbide material which may contain one or both of a boron donor material and a carbon donor material. The reactive infiltration typically results in a composite comprising a boron-containing compound, a carbon-containing compound and residual metal, if desired. The mass to be infiltrated may contain one or more inert filters admixed with the boron carbide material, boron-containing compound and/or carbon-containing compound. The relative amounts of reactants and process conditions may be altered or controlled to yield a body containing varying volume percents of ceramic, metal, ratios of one ceramic to another and porosity.
摘要翻译：自支撑体通过母体金属的反应性渗透到可以含有硼给体材料和碳供体材料中的一种或两种的碳化硼材料中而产生。如果需要，反应性渗透通常导致包含含硼化合物，含碳化合物和残余金属的复合材料。待渗透的物质可以含有与碳化硼材料，含硼化合物和/或含碳化合物混合的一种或多种惰性过滤器。可以改变或控制反应物和工艺条件的相对量，以产生包含不同体积百分比的陶瓷，金属，一种陶瓷与另一陶瓷的比例和孔隙率的物体。

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