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1. 发明申请

US20060258780A1 Method for preparing a silica suspension in a potentially crosslinkable silicone material 审中-公开
标题翻译：在可交联的有机硅材料中制备二氧化硅悬浮液的方法
公开(公告)号：US20060258780A1
公开(公告)日：2006-11-16
申请号：US10541161
申请日：2003-12-19
申请人： Marc Chaussade , Martial Deruelle , Gerard Mignani , Lucile Gambut-Garel
发明人： Marc Chaussade , Martial Deruelle , Gerard Mignani , Lucile Gambut-Garel
IPC分类号： C08K9/00 , B60C1/00
CPC分类号： C08J3/20 , C08G77/045 , C08G77/12 , C08G77/16 , C08G77/20 , C08G77/24 , C08G77/70 , C08G77/80 , C08J2383/04 , C08L83/04 , C08L83/00 , C08L2666/54
摘要： The invention concerns a method for preparing a precipitated silica in a silicone oil, said suspension being useable for producing silicones crosslinkable by polyaddition, polycondensation or condensation by dehydrogenation (elastomers). The invention aims at solving the problem of finding a compromise between cost, rheology and mechanical properties of the final elastomers. Therefor, the invention provides a method for preparing a precipitated silica suspension treated with trimethylchlorosilane, in the presence of hexamethyldisiloxane, in a crosslinkable silicone oil. HCl can be used. Grafting of hydrophobic units on the silica and incorporation of the polyorganosiloxane silicone material are carried out during one single processing sequence, without passing through the powder form for the silica. Sodium silicate promoting MQ resin can be incorporated in the reaction medium. One of the characteristics of the inventive method is that it does not at all comprise a step involving dried hydrophobic silica. The invention also concerns the preparation of crosslinkable silicone elastomer composition from said suspension, and the resulting composition.
摘要翻译：本发明涉及一种在硅油中制备沉淀二氧化硅的方法，所述悬浮液可用于生产通过加氢，缩聚或通过脱氢缩合（弹性体）可交联的硅氧烷。本发明旨在解决在成本，流变学和最终弹性体的机械性能之间找到妥协的问题。因此，本发明提供了在六甲基二硅氧烷存在下，在可交联的硅油中制备用三甲基氯硅烷处理的沉淀二氧化硅悬浮液的方法。可以使用HCl。疏水单元在二氧化硅上的接枝和聚有机硅氧烷硅氧烷材料的引入在一个单一的处理顺序中进行，而不通过二氧化硅的粉末形式。可以在反应介质中加入促进MQ树脂的硅酸钠。本发明方法的一个特征是它完全不包括干燥疏水性二氧化硅的步骤。本发明还涉及从所述悬浮液制备可交联硅氧烷弹性体组合物，以及所得组合物。

2. 发明申请

US20090035655A1 Crosslinkable composition for a battery electrolyte 有权
标题翻译：用于电池电解质的可交联组合物
公开(公告)号：US20090035655A1
公开(公告)日：2009-02-05
申请号：US10553058
申请日：2004-03-23
申请人： Lucile Gambut-Garel , Catherine George , Carroll Vergelati , Jean-Marc Pujol
发明人： Lucile Gambut-Garel , Catherine George , Carroll Vergelati , Jean-Marc Pujol
IPC分类号： H01M6/00
CPC分类号： H01M10/052 , C08G77/12 , C08G77/18 , C08G77/20 , C08G77/46 , C08G77/70 , C08L83/04 , H01M6/181 , H01M6/188 , H01M10/0525 , H01M10/0565 , H01M10/0567 , Y02T10/7011 , C08L83/00
摘要： The field of the present invention relates to the field of batteries and of polymer electrolytes for batteries and more particularly to the field of lithium batteries.The invention relates to a composition which can be polymerized and/or crosslinked by polyaddition for a battery electrolyte comprising: a) at least one polyorganosiloxane (POS) (A) exhibiting, per molecule, at least two C2-C6 alkenyl groups bonded to silicon and at least one group directly bonded to a silicon atom comprising a polyoxyalkylene (Poa) ether functional group; b) at least one polyorganosiloxane (POS) (B) exhibiting, per molecule, at least two hydrogen atoms bonded to silicon; c) a catalytically effective amount of at least one hydrosilylation catalyst (C); and a) at least one electrolyte salt (D).
摘要翻译：本发明的领域涉及用于电池的电池和聚合物电解质的领域，更具体地涉及锂电池领域。本发明涉及可通过聚合和/或交联的电池电解质的组合物，该组合物包括：a）至少一种每分子表现出至少两个与硅键合的C 2 -C 6链烯基的聚有机硅氧烷（POS）（A）和至少一个与包含聚氧化烯（Poa）醚官能团的硅原子直接键合的基团; b）至少一种每分子表现至少两个与硅结合的氢原子的聚有机硅氧烷（POS）（B） c）催化有效量的至少一种氢化硅烷化催化剂（C）; 和a）至少一种电解质盐（D）。

3. 发明申请

US20070128522A1 cross-linkable composition for a battery electrolyte 有权
标题翻译：用于电池电解质的可交联组合物
公开(公告)号：US20070128522A1
公开(公告)日：2007-06-07
申请号：US10551712
申请日：2004-03-23
申请人： Lucile Gambut-Garel , Carroll Vergelati , Jean-Yves Sanchez , Fannie Alloin
发明人： Lucile Gambut-Garel , Carroll Vergelati , Jean-Yves Sanchez , Fannie Alloin
IPC分类号： H01M10/40
CPC分类号： H01M10/052 , C08L83/06 , H01M6/166 , H01M6/181 , H01M6/188 , H01M10/0525 , H01M10/0565 , H01M10/0567 , Y02T10/7011 , C08L2666/54 , C08L2666/28
摘要： The field of the present invention relates to the field of batteries and of polymer electrolytes for batteries and more particularly to the field of lithium batteries. The invention relates to a composition which can be polymerized and/or crosslinked photochemically or under an electron beam for a battery electrolyte comprising: (a) at least one polyorganosiloxane (POS) (A) comprising, per molecule at least 2 siloxyl units carrying radicals comprising an epoxy (Epx) functional group with optionally an ether (Eth) functional group, and at least one of the siloxyl units carries a polyoxyalkylene (Poa) ether radical; (b) at least one electrolyte salt ; and (c) an effective amount of at least one cationic photoinitiator.
摘要翻译：本发明的领域涉及用于电池的电池和聚合物电解质的领域，更具体地涉及锂电池领域。本发明涉及一种可在光电化学或电子束电子束下聚合和/或交联电池电解质的组合物，包括：（a）至少一种聚有机硅氧烷（POS）（A），每分子含有至少2个带有自由基的甲硅烷氧基单元包括具有任选的醚（Eth）官能团的环氧（Epx）官能团，并且至少一个硅氧烷单元携带聚氧化烯（Poa）醚基; （b）至少一种电解质盐; 和（c）有效量的至少一种阳离子光引发剂。

4. 发明授权

US08093339B2 Cross-linkable silicone composition for the production of non-stick coatings for flexible supports and attachment promoting additive contained in this composition 有权
标题翻译：用于生产用于该组合物中所含的柔性载体和附着促进添加剂的不粘涂层的可交联硅氧烷组合物
公开(公告)号：US08093339B2
公开(公告)日：2012-01-10
申请号：US12304554
申请日：2007-06-27
申请人： John White , Michel Feder , Alain Pouchelon , Yassine Maadadi , Lucile Gambut-Garel
发明人： John White , Michel Feder , Alain Pouchelon , Yassine Maadadi , Lucile Gambut-Garel
IPC分类号： C08L83/04
CPC分类号： C08L83/04 , C08G77/12 , C08G77/14 , C08G77/18 , C08G77/20 , C08G77/70 , C08G77/80 , C09D183/04 , Y10T428/31511 , C08L83/00
摘要： Silicone composites subject to reticulation or reticulated, particularly for creating a coating or water-repellent and anti-adhesive film for flexible substrates such as paper or similar in the form of natural or synthetic polymer films. These compounds contain reticulating polyorganosiloxanes that have SiH units and unsaturated polyorganosiloxanes, preferably vinylated, suitable for reacting with the reticulating agent in an addition reaction and in the presence of platinum to form the reticulated anti-adhesive coating on the flexible substrate, plus at least one additive (D) to promote adhesion to it. A new liquid silicone compound can be applied without using a solvent, which is beneficial, that can be reticulated instantly to produce an anti-adhesive and/or water-repellent coating for the flexible substrate, giving very high quality reticulated silicone coatings, particularly in terms of sticking/adhering to the substrate, being harder to rub off and the anti-adhesion profile (sufficiently increase detaching force at high speed.
摘要翻译：经过网状或网状的硅氧烷复合材料，特别是为天然或合成聚合物膜形式的柔性基材如纸或类似物形成涂层或防水防粘膜。这些化合物含有网状聚有机硅氧烷，其具有SiH单元和不饱和聚有机硅氧烷，优选为乙烯基化，适于在加成反应中和在铂存在下与网状化合物反应，以在柔性基材上形成网状抗粘剂涂层，加上至少一种添加剂（D）以促进其粘附。可以在不使用溶剂的情况下施加新的液体硅氧烷化合物，这是有利的，其可以立即网状地制备用于柔性基材的抗粘合剂和/或防水涂料，提供非常高质量的网状硅氧烷涂料，特别是在粘附/粘附在基材上的问题，难以擦去和防粘附特性（足以高速地提高分离力）。

5. 发明授权

US09273190B2 Roll-up polyester film comprising, on at least one of the faces thereof, a scratch-resistant cross-linked coating, method for obtaining this polyester film 有权
标题翻译：在其至少一个表面上包含抗划伤性交联涂层的卷起聚酯膜，用于获得该聚酯膜的方法
公开(公告)号：US09273190B2
公开(公告)日：2016-03-01
申请号：US12810700
申请日：2008-12-23
申请人： Julien Faldysta , Lucile Gambut-Garel , Isabelle Juillard
发明人： Julien Faldysta , Lucile Gambut-Garel , Isabelle Juillard
IPC分类号： B32B7/02 , B32B15/09 , B32B27/30 , B32B27/36 , C09D133/04 , C09D133/06 , C09D133/08 , C09D133/10 , C09D133/14 , C09D133/24 , C09D133/26 , C09D7/12 , B05D3/06 , B05D3/10 , B05D3/14 , C08J7/04 , C08J7/18 , C08K3/36 , C08K5/04 , C08K5/132 , C08K5/07 , C08K5/5313 , C08K5/5397 , C08K5/3492 , C08L33/04 , C08L33/08 , C08L33/10 , C08L33/14 , C08F20/26 , C08F20/58 , C08F220/58 , C08F220/26 , C08L33/26 , C08L33/06 , C08L33/24 , C08K5/00 , C09D151/08 , C09D151/10 , B05D7/04
CPC分类号： C08J7/047 , B05D3/06 , B05D3/061 , B05D3/062 , B05D3/063 , B05D3/065 , B05D3/067 , B05D3/10 , B05D3/101 , B05D3/14 , B05D3/141 , B05D3/144 , B05D7/04 , B32B7/02 , B32B15/09 , B32B27/30 , B32B27/308 , B32B27/36 , B32B2255/10 , B32B2255/26 , B32B2307/584 , B32B2311/00 , B32B2367/00 , C08F20/26 , C08F20/58 , C08F220/26 , C08F220/58 , C08J7/18 , C08J2367/00 , C08J2433/00 , C08K3/36 , C08K5/0025 , C08K5/04 , C08K5/07 , C08K5/132 , C08K5/3492 , C08K5/5313 , C08K5/5397 , C08L33/04 , C08L33/062 , C08L33/066 , C08L33/08 , C08L33/10 , C08L33/14 , C08L33/24 , C08L33/26 , C09D7/40 , C09D7/63 , C09D7/65 , C09D133/04 , C09D133/06 , C09D133/062 , C09D133/066 , C09D133/08 , C09D133/10 , C09D133/14 , C09D133/24 , C09D133/26 , C09D151/08 , C09D151/10 , Y10T428/265 , Y10T428/266 , Y10T428/269 , Y10T428/31565 , Y10T428/31681 , Y10T428/31786 , Y10T428/31797
摘要： The invention relates to a polyester film comprising, on at least one of the faces thereof, a scratch-resistant crosslinked coating. The objective of the invention is to provide a polyester film coated with an abrasion-resistant layer which adheres perfectly to the polyester substrate, and is simple and economical to manufacture. To achieve this objective, the crosslinked hard coating applied to the polyester film comprises: i. 20% to 99% by weight of at least one ester and/or one amide of (meth)acrylic acid comprising a substituted protic group; ii. 20% to 99% by weight of acrylic resin(s); iii. 1% to 40% of a polyalkylene diacrylate; iv. 0 to 50% of at least one derivative of the benzophenone family; v. 0 to 5% of at least one photoinitiator. The invention also relates to the method for obtaining this polyester film coated with an abrasion-resistant hard layer. Use in the production of polyester/metal sheet (steel) colaminate.
摘要翻译：本发明涉及一种聚酯膜，其在至少一个表面上包含抗划伤性交联涂层。本发明的目的是提供一种涂覆有耐磨层的聚酯膜，该耐磨层完全粘附到聚酯基材上，制造简单而经济。为了达到这个目的，施加到聚酯薄膜上的交联硬涂层包括： 20重量％至99重量％的包含取代的质子基团的至少一种酯和/或一种（甲基）丙烯酸酰胺; ii。 20％至99％重量的丙烯酸树脂; iii。 1％至40％的聚亚烷基二丙烯酸酯; iv。 0至50％的至少一种二苯甲酮族衍生物; v。0至5％的至少一种光引发剂。本发明还涉及获得涂覆有耐磨硬质层的聚酯薄膜的方法。用于生产聚酯/金属板（钢）氯化钠。

6. 发明授权

US08293403B2 Crosslinkable composition for a battery electrolyte 有权
标题翻译：用于电池电解质的可交联组合物
公开(公告)号：US08293403B2
公开(公告)日：2012-10-23
申请号：US10553058
申请日：2004-03-23
申请人： Lucile Gambut-Garel , Catherine George , Carroll Vergelati , Jean-Marc Pujol
发明人： Lucile Gambut-Garel , Catherine George , Carroll Vergelati , Jean-Marc Pujol
IPC分类号： H01M6/00 , H01M6/04 , H01M6/14
CPC分类号： H01M10/052 , C08G77/12 , C08G77/18 , C08G77/20 , C08G77/46 , C08G77/70 , C08L83/04 , H01M6/181 , H01M6/188 , H01M10/0525 , H01M10/0565 , H01M10/0567 , Y02T10/7011 , C08L83/00
摘要： The field of the present invention relates to the field of batteries and of polymer electrolytes for batteries and more particularly to the field of lithium batteries.The invention relates to a composition which can be polymerized and/or crosslinked by polyaddition for a battery electrolyte comprising: a) at least one polyorganosiloxane (POS) (A) exhibiting, per molecule, at least two C2-C6 alkenyl groups bonded to silicon and at least one group directly bonded to a silicon atom comprising a polyoxyalkylene (Poa) ether functional group; b) at least one polyorganosiloxane (POS) (B) exhibiting, per molecule, at least two hydrogen atoms bonded to silicon; c) a catalytically effective amount of at least one hydrosilylation catalyst (C); and a) at least one electrolyte salt (D).
摘要翻译：本发明的领域涉及用于电池的电池和聚合物电解质的领域，更具体地涉及锂电池领域。本发明涉及可通过聚合和/或交联的电池电解质的组合物，该组合物包括：a）至少一种每分子表现出至少两个与硅键合的C 2 -C 6链烯基的聚有机硅氧烷（POS）（A）和至少一个与包含聚氧化烯（Poa）醚官能团的硅原子直接键合的基团; b）至少一种每分子表现至少两个与硅结合的氢原子的聚有机硅氧烷（POS）（B） c）催化有效量的至少一种氢化硅烷化催化剂（C）; 和a）至少一种电解质盐（D）。

7. 发明申请

US20100028685A1 CROSS-LINKABLE SILICONE COMPOSITION FOR THE PRODUCTION OF NON-STICK COATINGS FOR FLEXIBLE SUPPORTS AND ATTACHMENT PROMOTING ADDITIVE CONTAINED IN THIS COMPOSITION 有权
标题翻译：用于生产柔性支持物的非粘性涂料的交联硅氧烷组合物和在该组合物中包含的添加剂的附着物
公开(公告)号：US20100028685A1
公开(公告)日：2010-02-04
申请号：US12304554
申请日：2007-06-27
申请人： John White , Michel Feder , Alain Pouchelon , Yassine Maadadi , Lucile Gambut-Garel
发明人： John White , Michel Feder , Alain Pouchelon , Yassine Maadadi , Lucile Gambut-Garel
IPC分类号： B32B27/08 , C09D183/06 , C07F7/00 , B05D3/02
CPC分类号： C08L83/04 , C08G77/12 , C08G77/14 , C08G77/18 , C08G77/20 , C08G77/70 , C08G77/80 , C09D183/04 , Y10T428/31511 , C08L83/00
摘要： Silicone composites subject to reticulation or reticulated, particularly for creating a coating or water-repellent and anti-adhesive film for flexible substrates such as paper or similar in the form of natural or synthetic polymer films. These compounds contain reticulating polyorganosiloxanes that have SiH units and unsaturated polyorganosiloxanes, preferably vinylated, suitable for reacting with the reticulating agent in an addition reaction and in the presence of platinum to form the reticulated anti-adhesive coating on the flexible substrate, plus at least one additive (D) to promote adhesion to it. A new liquid silicone compound can be applied without using a solvent, which is beneficial, that can be reticulated instantly to produce an anti-adhesive and/or water-repellent coating for the flexible substrate, giving very high quality reticulated silicone coatings, particularly in terms of sticking/adhering to the substrate, being harder to rub off and the anti-adhesion profile (sufficiently increase detaching force at high speed.
摘要翻译：经过网状或网状的硅氧烷复合材料，特别是为天然或合成聚合物膜形式的柔性基材如纸或类似物形成涂层或防水防粘膜。这些化合物含有网状聚有机硅氧烷，其具有SiH单元和不饱和聚有机硅氧烷，优选为乙烯基化，适于在加成反应中和在铂存在下与网状化合物反应，以在柔性基材上形成网状抗粘剂涂层，加上至少一种添加剂（D）以促进其粘附。可以在不使用溶剂的情况下施加新的液体硅氧烷化合物，这是有利的，其可以立即网状地制备用于柔性基材的抗粘合剂和/或防水涂料，提供非常高质量的网状硅氧烷涂料，特别是在粘附/粘附在基材上的问题，难以擦去和防粘附特性（足以高速地提高分离力）。

8. 发明授权

US07750077B2 Method for the production of polymethylvinylsiloxane resins with recycling of volatile oligoorganosiloxanes 有权
标题翻译：生产具有挥发性低聚有机硅氧烷再循环的聚甲基乙烯基硅氧烷树脂的方法
公开(公告)号：US07750077B2
公开(公告)日：2010-07-06
申请号：US10544528
申请日：2004-01-26
申请人： Lucile Gambut-Garel , José-Louis Roca-Ortega , Didier Dahler , Gérard Mignani , Christian Allandrieu
发明人： Lucile Gambut-Garel , José-Louis Roca-Ortega , Didier Dahler , Gérard Mignani , Christian Allandrieu
IPC分类号： C08G77/06
CPC分类号： C08G77/02 , C08G77/06 , C08G77/20
摘要： The invention relates to the field of silicon resins, particularly polymethylvinylsiloxane resins. The invention more specifically relates to a method for the production of polymethylvinylsiloxane resins comprising at least two different types of siloxy motifs R3SiO1/2 (motif M) and SiO4/2 (motif Q, optionally QOH), said method comprising the following steps: a) producing a siloxane resin comprising motifs Q by acidic hydrolysis of a siloxane resin precursor, preferably an alkaline silicate; b) functionalizing the siloxane resin obtained in step a) with halogenosilanes in the presence of an apolar solvent, the functionalizing generating sub-products including volatile oligosiloxanes (silox); c) recovering silox produced in step b) in a solution in the apolar solvent; and d) subjecting the resin functionalized in step b) to rearrangement with the aid of a strong base in order to eliminate the silanols, wherein at least a part of the silox produced during step b) and recovered in step c) is recycled.
摘要翻译：本发明涉及硅树脂，特别是聚甲基乙烯基硅氧烷树脂领域。本发明更具体地涉及一种生产聚甲基乙烯基硅氧烷树脂的方法，其包含至少两种不同类型的甲硅烷氧基序列R3SiO1 / 2（基序M）和SiO4 / 2（基序Q，任选的QOH），所述方法包括以下步骤：）通过硅氧烷树脂前体，优选碱性硅酸盐的酸性水解产生包含图案Q的硅氧烷树脂; b）在非极性溶剂的存在下用卤代硅烷官能化步骤a）中获得的硅氧烷树脂，所述官能化产生的副产物包括挥发性低聚硅氧烷（silox）; c）将在步骤b）中生产的silox回收到非极性溶剂中的溶液中; 和d）使步骤b）中官能化的树脂在强碱的帮助下进行重排，以消除硅烷醇，其中在步骤b）中产生并在步骤c）中回收的至少部分的Silox被再循环。

9. 发明申请

US20090297719A1 METHOD OF PREVENTING THE APPEARANCE OF MISTING WHEN COATING FLEXIBLE MEDIA WITH A CROSSLINKABLE LIQUID SILICONE COMPOSITION IN A MULTI-ROLL DEVICE 审中-公开
标题翻译：防止在多层设备中使用可交联液体硅酮组合物涂布柔性介质时出现的外观的方法
公开(公告)号：US20090297719A1
公开(公告)日：2009-12-03
申请号：US12096175
申请日：2006-12-07
申请人： Frédéric Magd , Tinia Ireland , Lucile Gambut-Garel
发明人： Frédéric Magd , Tinia Ireland , Lucile Gambut-Garel
IPC分类号： B05D1/28 , C08L83/04
CPC分类号： D21H27/001 , C08G77/12 , C08G77/20 , C08G77/42 , C08G77/70 , C08G77/80 , C08L83/04 , C09D183/04 , D06M13/144 , D06M13/288 , D06M15/643 , D06M23/10 , D21H19/32 , D21H23/56 , C08L83/00
摘要： The invention relates to the general field of coating various flexible media, such as sheets of paper or synthetic polymer (polyolefin, polyester, etc.) or else a textile, with a silicone on high-speed rolls. The invention relates to an effective method of preventing the appearance of misting when coating flexible media with a liquid silicone composition that is the precursor of crosslinked coatings, this coating operation being performed using a roll coater operating at high speed.
摘要翻译：本发明涉及在各种柔性介质（例如纸张或合成聚合物（聚烯烃，聚酯等））上涂布各种柔性介质或者在高速辊上涂覆硅树脂的纺织品的一般领域。本发明涉及一种防止在用作为交联涂层的前体的液体硅氧烷组合物涂布柔性介质时出现雾化的有效方法，该涂覆操作是使用高速操作的辊涂机进行的。

10. 发明申请

US20060241266A1 Method for the production of polymethylvinylsiloxane resins wtih recycling of volatile oligoorganosiloxanes 有权
标题翻译：用于生产聚甲基乙烯基硅氧烷树脂的方法，其是挥发性低聚有机硅氧烷的再循环
公开(公告)号：US20060241266A1
公开(公告)日：2006-10-26
申请号：US10544528
申请日：2004-01-26
申请人： Lucile Gambut-Garel , José-Louis Roca-Ortega , Didier Dahler , Gérard Mignani , Christian Allandrieu
发明人： Lucile Gambut-Garel , José-Louis Roca-Ortega , Didier Dahler , Gérard Mignani , Christian Allandrieu
IPC分类号： C08G77/00
CPC分类号： C08G77/02 , C08G77/06 , C08G77/20
摘要： The invention relates to the field of silicon resins, particularly polymethylvinylsiloxane resins. The invention more specifically relates to a method for the production of polymethylvinylsiloxane resins comprising at least two different types of siloxy motifs R3SiO1/2 (motif M) and SiO4/2 (motif Q, optionally QOH), said method comprising the following steps: a) producing a siloxane resin comprising motifs Q by acidic hydrolysis of a siloxane resin precursor, preferably an alkaline silicate; b) functionalizing the siloxane resin obtained in step a) with halogenosilanes in the presence of an apolar solvent, the functionalizing generating sub-products including volatile oligosiloxanes (silox); c) recovering silox produced in step b) in a solution in the apolar solvent; and d) subjecting the resin functionalized in step b) to rearrangement with the aid of a strong base in order to eliminate the silanols, wherein at least a part of the silox produced during step b) and recovered in step c) is recycled.
摘要翻译：本发明涉及硅树脂，特别是聚甲基乙烯基硅氧烷树脂领域。本发明更具体地涉及一种生产聚甲基乙烯基硅氧烷树脂的方法，其包含至少两种不同类型的甲硅烷氧基基团R 3 SiO 1/2（基元M）和SiO 2 所述方法包括以下步骤：a）通过酸性水解硅氧烷树脂前体制备包含图案Q的硅氧烷树脂，优选碱性硅酸盐; b）在非极性溶剂的存在下用卤代硅烷官能化步骤a）中获得的硅氧烷树脂，所述官能化产生的副产物包括挥发性低聚硅氧烷（silox）; c）将在步骤b）中生产的silox回收到非极性溶剂中的溶液中; 和d）使步骤b）中官能化的树脂在强碱的帮助下进行重排，以消除硅烷醇，其中在步骤b）中产生并在步骤c）中回收的至少部分的Silox被再循环。

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