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1. 发明授权

US06515174B2 Preformed multi-acid adducts useful for grafting polyolefin polymers 失效
标题翻译：可用于接枝聚烯烃聚合物的预成型多酸加合物
公开(公告)号：US06515174B2
公开(公告)日：2003-02-04
申请号：US09760545
申请日：2001-01-16
申请人： Manuel Soler Rodriguez , Charles Chiu-Hsiung Hwo , Pui Kwan Wong , Pierre Nazareth Tu{overscore (t)}unjian , Charles Lee Edwards
发明人： Manuel Soler Rodriguez , Charles Chiu-Hsiung Hwo , Pui Kwan Wong , Pierre Nazareth Tu{overscore (t)}unjian , Charles Lee Edwards
IPC分类号： C07C22904
CPC分类号： C08F255/10 , C08F255/00 , C08L51/06 , C09J151/06
摘要： The present invention relates to reaction products formed from maleic anhydride and amino carboxylic acids. The reaction products are particularly useful for grafting polyolefins to increase their polarity and therefore enhance their physical properties.
摘要翻译：本发明涉及由马来酸酐和氨基羧酸形成的反应产物。反应产物特别适用于接枝聚烯烃以增加其极性并因此提高其物理性能。

2. 发明授权

US06221967B1 Preformed multi-acid adducts useful for grafting polyolefin polymers 失效
公开(公告)号：US06221967B1
公开(公告)日：2001-04-24
申请号：US09464145
申请日：1999-12-16
申请人： Manuel Soler Rodriguez , Charles Chiu-Hsiung Hwo , Pui Kwan Wong , Pierre Nazareth Tutunjian , Charles Lee Edwards
发明人： Manuel Soler Rodriguez , Charles Chiu-Hsiung Hwo , Pui Kwan Wong , Pierre Nazareth Tutunjian , Charles Lee Edwards
IPC分类号： C08F25500
CPC分类号： C08F255/10 , C08F255/00 , C08L51/06 , C09J151/06
摘要： The present invention relates to reaction products formed from maleic anhydride and amino carboxylic acids. The reaction products are particularly useful for grafting polyolefins to increase their polarity and therefore enhance their physical properties.

3. 发明授权

US06448333B1 Polyfunctional polyolefins 失效
标题翻译：多官能聚烯烃
公开(公告)号：US06448333B1
公开(公告)日：2002-09-10
申请号：US09464150
申请日：1999-12-16
申请人： Manuel Soler Rodriguez , Pierre Nazareth Tutunjian , Charles Lee Edwards , Paul Karol Casey , Carlton Edwin Ash , Charles C. Hwo , Pui Kwan Wong
发明人： Manuel Soler Rodriguez , Pierre Nazareth Tutunjian , Charles Lee Edwards , Paul Karol Casey , Carlton Edwin Ash , Charles C. Hwo , Pui Kwan Wong
IPC分类号： C08F28900
CPC分类号： C08F8/30 , C08F255/00 , C08F222/06
摘要： A grafted polyolefin polymers having high polarity produced by grafting bi-functional N-substituted diacids to maleated or other functional group grafted polyolefin. The new polymers exhibit improved water miscibility, compatability and good adhesion to polar materials such as nylon, polyester, glass, and metal substrates.
摘要翻译：通过将双功能N-取代的二酸接枝到马来酸化或其它官能团接枝的聚烯烃上产生的具有高极性的接枝聚烯烃聚合物。新型聚合物具有改善的水混溶性，相容性和对极性材料如尼龙，聚酯，玻璃和金属基材的良好粘附性。

4. 发明授权

US07425658B2 Process for producing 1-octene from butadiene 有权
标题翻译：从丁二烯生产1-辛烯的方法
公开(公告)号：US07425658B2
公开(公告)日：2008-09-16
申请号：US10887697
申请日：2004-07-09
申请人： Charles Lee Edwards
发明人： Charles Lee Edwards
IPC分类号： C07C2/04 , C07C1/207
CPC分类号： C07C11/02 , C07C1/20 , C07C1/24 , C07C41/06 , C07C2521/04 , C07C2523/06 , C07C2527/224 , C07C2531/24 , C07C43/15
摘要： Method for producing 1-octene from butadiene by dimerizing and alkoxylating butadiene in the presence of one or more alkoxy substituted phosphine ligands under alkoxydimerization conditions with an alkoxydimerization catalyst, the alkoxydimerization conditions being effective to produce an alkoxydimerization product with one or more alkoxy substituted octadienes comprising primarily 1-alkoxy substituted octadiene; hydrogenating the alkoxydimerization product under hydrogenation conditions effective to produce a hydrogenation product which is primarily 1-alkoxy substituted octane; eliminating the alkoxy group from the hydrogenation product under elimination conditions effective to produce an elimination product which is primarily 1-octene and a first alkanol having from about 1 to about 3 carbon atoms; and separating the 1-octene from said elimination product.
摘要翻译：通过在烷氧基二聚化条件下用烷氧基二聚催化剂在一个或多个烷氧基取代的膦配体存在下使丁二烯进行二聚和烷氧基化来制备丁烯的1-辛烯的方法，所述烷氧基二聚化条件有效地与一个或多个烷氧基取代的八面体产生烷氧基二聚产物，主要是1-烷氧基取代的辛二烯; 在有效产生主要为1-烷氧基取代的辛烷的氢化产物的氢化条件下氢化烷氧基二聚产物; 在有效产生主要是1-辛烯的消除产物和具有约1至约3个碳原子的第一链烷醇的消除条件下从氢化产物中除去烷氧基; 并从所述消除产物中分离出1-辛烯。

5. 发明授权

US07141539B2 Process for producing detergent molecules comprising an ether linkage from butadiene 失效
标题翻译：制备包含丁二烯醚键的洗涤剂分子的方法
公开(公告)号：US07141539B2
公开(公告)日：2006-11-28
申请号：US10887736
申请日：2004-07-09
申请人： Charles Lee Edwards
发明人： Charles Lee Edwards
IPC分类号： C11D1/722 , C07C41/06
CPC分类号： C07C43/13 , C07C41/06 , C07C41/20 , C07C41/26 , C07C43/15 , C07C43/178
摘要： Novel detergent molecules and methods for producing such detergent molecules by dimerizing and alkoxylating butadiene with one or more reactant alkanol selected from the group consisting of a primary alkanol and an α, ω-diol, hydrogenating the alkoxydimerization product to produce a hydrogenation product selected from the group consisting of primarily 1-alkoxy substituted 2-octene and primarily 1-hydroxy-alkoxyoctane, and hydroxylating the 1-alkoxy substituted 2-octene to produce primarily 1-hydroxy-9-alkoxy nonanes.
摘要翻译：新型洗涤剂分子和通过使丁二烯与一种或多种选自伯烷醇和α，ω-二醇的一种或多种反应性烷醇二聚和烷氧基化制备这种洗涤剂分子的方法，氢化烷氧基二聚化产物以产生选自主要由1-烷氧基取代的2-辛烯和主要1-羟基 - 烷氧基辛基组成的基团，并且使1-烷氧基取代的2-辛烯羟基化以主要产生1-羟基-9-烷氧基壬烷。

6. 发明授权

US07071364B2 Branched primary alcohol compositions and derivatives thereof 失效
标题翻译：支链伯醇组合物及其衍生物
公开(公告)号：US07071364B2
公开(公告)日：2006-07-04
申请号：US10679120
申请日：2003-10-03
申请人： Charles Lee Edwards , Kirk Herbert Raney , Paul Gregory Shpakoff
发明人： Charles Lee Edwards , Kirk Herbert Raney , Paul Gregory Shpakoff
IPC分类号： C07C43/20 , C11D3/20
CPC分类号： C07C43/13 , C07C43/11 , C07C305/10 , C11D1/24 , C11D1/29 , C11D1/66 , C11D1/722 , C11D3/2068 , C11D3/3409
摘要： A detergent composition having cold water solubility and exhibiting high calcium tolerance can be produced from biodegradable branched ether derivative compositions derived from a branched ether primary alcohol represented by the formula: wherein R1 represents hydrogen or a hydrocarbyl radical having from 1 to 3 carbon atoms, R2 represents a hydrocarbyl radical having from 1 to 7 carbon atoms, x is a number ranging from 0 to 16, preferably from 3 to 13, wherein the total number of carbon atoms in the alcohol ranges from 9 to 24.
摘要翻译：具有冷水溶解度和显示高耐钙性的洗涤剂组合物可以由衍生自由下式表示的支链醚伯醇的生物可降解的支链醚衍生物组合物制备：其中R 1表示氢或具有 1至3个碳原子，R 2表示具有1至7个碳原子的烃基，x为0至16，优选3至13的数，其中碳总数醇中的原子范围为9至24。

7. 发明授权

US06909020B2 Branched primary alcohol compositions and derivatives thereof 失效
公开(公告)号：US06909020B2
公开(公告)日：2005-06-21
申请号：US10679174
申请日：2003-10-03
申请人： Charles Lee Edwards , Kirk Herbert Raney , Paul Gregory Shpakoff
发明人： Charles Lee Edwards , Kirk Herbert Raney , Paul Gregory Shpakoff
IPC分类号： C11D1/14 , C07C43/11 , C07C43/13 , C07C305/10 , C07C309/10 , C11D1/24 , C11D1/29 , C11D1/66 , C11D1/722 , C11D3/20 , C11D3/34 , C07C41/00
CPC分类号： C07C43/13 , C07C43/11 , C07C305/10 , C11D1/24 , C11D1/29 , C11D1/66 , C11D1/722 , C11D3/2068 , C11D3/3409
摘要： A detergent composition having cold water solubility and exhibiting high calcium tolerance can be produced from biodegradable branched ether derivative compositions derived from a branched ether primary alcohol represented by the formula: wherein R1 represents hydrogen or a hydrocarbyl radical having from 1 to 3 carbon atoms, R2 represents a hydrocarbyl radical having from 1 to 7 carbon atoms, x is a number ranging from 0 to 16, preferably from 3 to 13, wherein the total number of carbon atoms in the alcohol ranges from 9 to 24.

8. 发明授权

US06891056B2 Branched primary alcohol compositions and derivatives thereof 失效
标题翻译：支链伯醇组合物及其衍生物
公开(公告)号：US06891056B2
公开(公告)日：2005-05-10
申请号：US10679126
申请日：2003-10-03
申请人： Charles Lee Edwards , Kirk Herbert Raney , Paul Gregory Shpakoff
发明人： Charles Lee Edwards , Kirk Herbert Raney , Paul Gregory Shpakoff
IPC分类号： C11D1/14 , C07C43/11 , C07C43/13 , C07C305/10 , C07C309/10 , C11D1/24 , C11D1/29 , C11D1/66 , C11D1/722 , C11D3/20 , C11D3/34 , C07C305/04
CPC分类号： C07C43/13 , C07C43/11 , C07C305/10 , C11D1/24 , C11D1/29 , C11D1/66 , C11D1/722 , C11D3/2068 , C11D3/3409
摘要： A detergent composition having cold water solubility and exhibiting high calcium tolerance can be produced from biodegradable branched ether derivative compositions derived from a branched ether primary alcohol represented by the formula: wherein R1 represents hydrogen or a hydrocarbyl radical having from 1 to 3 carbon atoms, R2 represents a hydrocarbyl radical having from 1 to 7 carbon atoms, x is a number ranging from 0 to 16, preferably from 3 to 13, wherein the total number of carbon atoms in the alcohol ranges from 9 to 24.
摘要翻译：具有冷水溶解度和显示高耐钙性的洗涤剂组合物可以由衍生自由下式表示的支链醚伯醇的生物可降解的支链醚衍生物组合物制备：其中R 1表示氢或具有 1至3个碳原子，R 2表示具有1至7个碳原子的烃基，x为0至16，优选3至13的数，其中碳总数醇中的原子范围为9至24。

9. 发明授权

US06953766B2 Preparation of efficient REPO and LAPO catalysts 失效
公开(公告)号：US06953766B2
公开(公告)日：2005-10-11
申请号：US10382544
申请日：2003-03-06
申请人： Charles Lee Edwards
发明人： Charles Lee Edwards
IPC分类号： B01J27/18 , B01J37/04 , B01J37/28 , C07B61/00 , C07C41/03 , C07C43/11 , C08G65/26 , B01J27/14 , B01J23/00 , B01J27/186 , B01J27/187 , B01J27/199
CPC分类号： C07C41/03 , B01J27/1804 , B01J37/28 , C08G65/266 , C07C43/11
摘要： A method of ensuring the production of efficient lanthanum phosphate catalysts (LAPO's) and rare earth phosphate catalysts (REPO's), and methods of alkoxylation using said efficient catalysts.

10. 发明授权

US06514898B2 Process of preparing a fluid rare earth alkoxylation catalyst 有权
标题翻译：制备流体稀土烷氧基化催化剂的方法
公开(公告)号：US06514898B2
公开(公告)日：2003-02-04
申请号：US09737989
申请日：2000-12-15
申请人： Charles Lee Edwards
发明人： Charles Lee Edwards
IPC分类号： B01J2714
CPC分类号： C07C41/03 , B01J27/1804 , C07C43/11
摘要： A process to prepare an improved fluid rare earth phosphate catalyst composition useful in preparing alkylene oxide adducts of organic compounds having active hydrogen atoms is provided. The catalyst is prepared by dissolving a rare earth salt in a C9-C30 active hydrogen containing organic compound and then adding phosphoric acid to the organic compound rare earth mixture.
摘要翻译：提供了制备用于制备具有活性氢原子的有机化合物的环氧烷加合物的改进的流体稀土磷酸盐催化剂组合物的方法。通过将稀土盐溶解在含C9-C30活性氢的有机化合物中，然后向有机化合物稀土混合物中加入磷酸制备催化剂。

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