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1. 发明授权

US5856494A Preparation of 2, 2, 6, 6-tetramethylpiperidin-4-one (TAA) 失效
标题翻译：制备2,6-二甲基哌啶-4-酮（TAA）
公开(公告)号：US5856494A
公开(公告)日：1999-01-05
申请号：US911456
申请日：1997-08-14
申请人： Manfred Julius , Dieter Hermeling , Hardo Siegel , Wolfgang Harder
发明人： Manfred Julius , Dieter Hermeling , Hardo Siegel , Wolfgang Harder
IPC分类号： B01J31/02 , C07B61/00 , C07D211/74
CPC分类号： C07D211/74
摘要： A process for preparing 2,2,6,6-tetramethylpiperidin-4-one (TAA) is described, whereina mixture comprising acetone and/or acetone condensates and ammonia in a molar ratio of from 20:1 to 3:1at from 50.degree. to 130.degree. C.is reacted in the presence of dimethyl sulfate, the amount of dimethyl sulfate being from 0.5 to 5 mol-%, based on acetone.
摘要翻译：描述了制备2,2,6,6-四甲基哌啶-4-酮（TAA）的方法，其中包含丙酮和/或丙酮的混合物和摩尔比为20:1至3:1的氨， 50℃至130℃，在硫酸二甲酯存在下反应，硫酸二甲酯为丙酮为0.5-5mol％。

2. 发明授权

US5892121A Purification of tertiary phosphine oxides 失效
标题翻译：叔膦氧化物的纯化
公开(公告)号：US5892121A
公开(公告)日：1999-04-06
申请号：US968180
申请日：1997-11-12
申请人： Dieter Hermeling , Randolf Hugo , Hardo Siegel
发明人： Dieter Hermeling , Randolf Hugo , Hardo Siegel
IPC分类号： C07F9/02 , C07F9/53
CPC分类号： C07F9/025 , C07F9/5345
摘要： A process for the purification of tertiary phosphine oxides obtained in a Wittig synthesis as a contaminated by product resulting from the reaction of the corresponding tertiary phosphines, especially triphenylphosphine. The contaminated tertiary phosphine oxides coming from this Wittig synthesis have the formula I ##STR1## in which R.sup.1, R.sup.2, and R.sup.3 denote C.sub.1 -C.sub.12 alkyl, C.sub.5 -G.sub.8 cycloalkyl, aryl, C.sub.7 -C.sub.20 aralkyl, or C.sub.7 -C.sub.20 alkylaryl. The contaminated phosphine oxide I or phosphine oxide I-containing mixtures, optionally in an inert solvent, are first caused to react with an inorganic or organic acid at temperatures of from 0.degree. to 150.degree. C. to form a crystallized acid salt. The resulting salt crystals are then treated in a purifying step with water or an inorganic base or an organic base to again form the tertiary phosphine oxide. This reformed oxide is then extracted with an inert organic solvent from which the purified tertiary phosphine oxide is finally liberated.
摘要翻译：用于净化由Wittig合成得到的叔膦氧化物的方法，该方法被相应的叔膦特别是三苯基膦反应产生的产物污染。来自该Wittig合成的受污染的叔膦氧化物具有式I（I），其中R 1，R 2和R 3表示C 1 -C 12烷基，C 5 -C 8环烷基，芳基，C 7 -C 20芳烷基或C 7 -C 20 烷基芳基首先使受污染的氧化膦I或含氧化膦I的混合物，任选在惰性溶剂中，在0℃至150℃的温度下与无机或有机酸反应，形成结晶的酸盐。然后将所得盐晶体在纯化步骤中用水或无机碱或有机碱处理，以再次形成叔氧化膦。然后将该重整氧化物用惰性有机溶剂萃取，从其中最终释放纯化的叔氧化膦。

3. 发明授权

US5527966A Preparation of triphenylphosphine 失效
标题翻译：三苯膦的制备
公开(公告)号：US5527966A
公开(公告)日：1996-06-18
申请号：US285204
申请日：1994-08-03
申请人： Dieter Hermeling , Peter Bassler , Peter Hammes , Randolf Hugo , Peter Lechtken , Hardo Siegel
发明人： Dieter Hermeling , Peter Bassler , Peter Hammes , Randolf Hugo , Peter Lechtken , Hardo Siegel
IPC分类号： F16B7/18 , B01J31/02 , C07F9/50 , E04B1/19 , E04B1/342 , E04B1/58 , F16B9/02 , C07F9/02
CPC分类号： B01J31/0247 , C07F9/509
摘要： Triphenylphosphine (TPP) is prepared by reacting triphenylphosphine dichloride (TPPCl.sub.2) with magnesium, aluminum and/or iron in the presence of an inert solvent, employing a TPPCl.sub.2 solution whose content of phosgene, chlorine, diphosgene, hydrogen chloride, thionyl chloride, sulfuryl chloride, phosphorus trichloride, phosphorus oxychloride and/or aliphatic halogen compounds (active chlorine compounds) totals less than 1000 ppm Cl.
摘要翻译：三苯基膦（TPP）是通过使三氯化磷（TPPCl 2）与镁，铝和/或铁在惰性溶剂存在下反应制备的，该TPPCl 2溶液含有光气，氯气，二极光，氯化氢，亚硫酰氯，磺酰氯，三氯化磷，三氯氧化磷和/或脂肪族卤素化合物（活性氯化合物）总计小于1000ppm Cl。

4. 发明申请

US20110224379A1 Mixture of Surface Postcrosslinked Superabsorbers with Different Surface Postcrosslinking 失效
标题翻译：具有不同表面后交联的表面后交联超吸收剂的混合物
公开(公告)号：US20110224379A1
公开(公告)日：2011-09-15
申请号：US13128558
申请日：2009-11-12
申请人： Stefan Bruhns , Thomas Daniel , Dieter Hermeling , Ulrich Riegel
发明人： Stefan Bruhns , Thomas Daniel , Dieter Hermeling , Ulrich Riegel
IPC分类号： B01J20/26 , C08F20/06
CPC分类号： C08J3/245 , A61L15/60 , C08J2300/14
摘要： A mixture of superabsorbents having differing surface postcrosslinking, more particularly a mixture of differingly surface-postcrosslinked sieve cuts of a base polymer, exhibits improved absorption and retention over a unitarily surface-postcrosslinked superabsorbent.
摘要翻译：具有不同表面后交联的超吸收剂的混合物，更特别是基础聚合物的表面后交联筛分的混合物在整体表面后交联的超吸收剂上表现出改进的吸收和保留。

5. 发明申请

US20110178251A1 Water Absorbing Material 失效
标题翻译：吸水材料
公开(公告)号：US20110178251A1
公开(公告)日：2011-07-21
申请号：US13060347
申请日：2009-09-08
申请人： Veit Stegmann , Klemens Massonne , Franz Niklaus Windlin , Reinhold Schwalm , Dieter Hermeling , Thomas Daniel , Stefan Bruhns
发明人： Veit Stegmann , Klemens Massonne , Franz Niklaus Windlin , Reinhold Schwalm , Dieter Hermeling , Thomas Daniel , Stefan Bruhns
IPC分类号： C08F8/42
CPC分类号： A61L15/60 , C08J3/28 , C08J2300/14
摘要： The present invention relates to a water-absorbing material obtainable by a process comprising the steps of A) treating a particulate, non-surface-crosslinked, water-absorbing polymer with a mixture comprising an aqueous solvent and at least one salt of a transition metal and B) irradiating the polymer treated according to A) with UV radiation, to a process for its production and to articles comprising the water-absorbing material.
摘要翻译：本发明涉及通过包括以下步骤的方法获得的吸水材料：A）用包含水性溶剂和至少一种过渡金属盐的混合物处理颗粒状非表面交联的吸水性聚合物和B）用UV辐射将根据A）处理的聚合物照射到其生产方法和包含吸水材料的制品上。

6. 发明授权

US07981969B2 Postcrosslinking of water-absorbing polymers 有权
标题翻译：吸水聚合物的后交联
公开(公告)号：US07981969B2
公开(公告)日：2011-07-19
申请号：US10588671
申请日：2005-02-18
申请人： Ulrich Riegel , Thomas Daniel , Matthias Weismantel , Mark Elliott , Dieter Hermeling
发明人： Ulrich Riegel , Thomas Daniel , Matthias Weismantel , Mark Elliott , Dieter Hermeling
IPC分类号： C08J3/24 , C08F20/06
CPC分类号： C08J3/245 , C08F220/06 , C08J2300/14
摘要： The invention concerns a process for producing water-absorbing polymer, which comprises a base polymer A being mixed with a first aqueous solution B of at least one surface postcrosslinker and a second aqueous solution C of at least one polyvalent cation and thermally treated, wherein said base polymer A is based on at least 50% neutralized acid-functional monomer and said solutions B and C are metered wholly or partly concurrently through separate nozzles whereby a water-absorbing polymer having a high saline flow conductivity value is obtained.
摘要翻译：本发明涉及一种生产吸水聚合物的方法，其包括将基础聚合物A与至少一个表面后交联剂的第一水溶液B和至少一种多价阳离子的第二水溶液C混合并进行热处理，其中所述基础聚合物A基于至少50％中和的酸官能单体，并且所述溶液B和C通过单独的喷嘴全部或部分同时计量，从而获得具有高盐水流动电导率值的吸水聚合物。

7. 发明授权

US07759422B2 Fine-grained water-absorbent particles with a high fluid transport and absorption capacity 有权
标题翻译：具有高流体输送和吸收能力的细颗粒吸水颗粒
公开(公告)号：US07759422B2
公开(公告)日：2010-07-20
申请号：US11665883
申请日：2005-10-14
申请人： Ulrich Riegel , Thomas Daniel , Dieter Hermeling , Mark Elliott
发明人： Ulrich Riegel , Thomas Daniel , Dieter Hermeling , Mark Elliott
IPC分类号： C08G63/60
CPC分类号： A61L15/60 , C08L33/02
摘要： The invention relates to finely divided water-absorbing polymeric particles having high fluid transportation and absorption performance, the Centrifuge Retention Capacity (CRC) being not less than 26 g/g, the absorbency under a load of 4.83 kPa (AUL0.7 psi) not less than 23 g/g and the Transportation Value (TV) not less than 15,000 cm3s, the Transportation Value (TV) being the product of Saline Flow Conductivity (SFC) and wicking absorption after 60 minutes (DA60) multiplied by 107, and wherein the wicking absorption after 60 minutes (DA60) is the weight of 0.9% by weight sodium chloride solution absorbed by 70 g of the water-absorbing polymeric particles in 60 minutes, wherein the water-absorbing polymeric particles are situated, during measurement, in a circularly round vessel which has an internal diameter of 6 cm and is sealed at its lower end by a sieve base of 36 μm mesh size, and the sieve base is in atmospheric contact with 0.9% by weight sodium chloride solution, processes for their preparation and also their use in hygiene articles and packaging materials.
摘要翻译：本发明涉及具有高流体输送和吸收性能的细分散的吸水聚合物颗粒，离心保留容量（CRC）不小于26g / g，负荷4.83kPa（AUL0.7psi）下的吸收性不是运输价值（TV）不小于15,000立方厘米，运输价值（TV）是盐水流动电导率（SFC）的乘积和60分钟后的吸液吸收（DA60）乘以107，其中 60分钟后的芯吸吸收（DA60）是在60分钟内由70g吸水性聚合物颗粒吸收的0.9重量％氯化钠溶液的重量，其中吸水聚合物颗粒在测量期间位于内径6厘米的圆形圆形容器，其下端由36微米的筛孔尺寸的筛基密封，筛基与0.9重量％氯化钠溶液大气接触，他们的准备以及在卫生用品和包装材料中的使用。

8. 发明授权

US07553903B2 Swellable hydrogel-forming polymers having a low fraction of fines 失效
$Swellable hydrogel-forming polymers having a low fraction of fines$
标题翻译：可溶胀的水凝胶形成聚合物具有低部分的细粉
公开(公告)号：US07553903B2
公开(公告)日：2009-06-30
申请号：US10581562
申请日：2004-12-17
申请人： Ulrich Riegel , Thomas Daniel , Matthias Weismantel , Mark Elliott , Dieter Hermeling
发明人： Ulrich Riegel , Thomas Daniel , Matthias Weismantel , Mark Elliott , Dieter Hermeling
IPC分类号： C08G63/60 , C08G69/26
CPC分类号： A61L15/60 , C08G63/20 , C08G63/60 , C08K3/34 , C08L5/00 , C08L67/00 , C08L91/06 , C09D179/02 , Y10S524/916 , C08L2666/26
摘要： Swellable hydrogel-forming polymer comprising at least one hydrophilic polymer of dendritic structure, a process for preparing the swellable hydrogel-forming polymer and also its use in hygiene articles.
摘要翻译：包含至少一种树枝状结构的亲水性聚合物的可膨胀的水凝胶形成性聚合物，制备可溶胀水凝胶形成聚合物的方法以及其在卫生制品中的用途。

9. 发明申请

US20090030155A1 Absorbent Article Comprising Water-Absorbing Polymeric Particles And Method For The Production Thereof 审中-公开
标题翻译：包含吸水性聚合物颗粒的吸收性物品及其制造方法
公开(公告)号：US20090030155A1
公开(公告)日：2009-01-29
申请号：US12146530
申请日：2008-06-26
申请人： Thomas Daniel , Ulrich Riegel , Mark Elliott , Stefan Bruhns , Dieter Hermeling
发明人： Thomas Daniel , Ulrich Riegel , Mark Elliott , Stefan Bruhns , Dieter Hermeling
IPC分类号： C08F8/40
CPC分类号： A61L15/60 , A61F13/15658 , A61F13/5323 , C08J3/245
摘要： The invention refers to absorbent structures for use in an absorbent article, the absorbent structure comprising a water absorbing material. The water absorbing material is obtainable by a process comprising the steps of bringing particles of a non surface-crosslinked water-absorbing polymer in contact with at least one post-crosslinker, at least one water-insoluble metal phosphate, and at least one further ingredient. The at least one ingredient is selected from at least one Nitrogen-containing water-soluble polymer, and at least one hydrophobic polymer. The particles are heat-treated at a temperature in the range from 120° C. to 300° C.
摘要翻译：本发明涉及用于吸收制品的吸收结构，该吸收结构包括吸水材料。吸水材料可以通过以下方法获得，该方法包括以下步骤：使非表面交联的吸水聚合物的颗粒与至少一种后交联剂，至少一种水不溶性金属磷酸盐和至少一种其它成分。所述至少一种成分选自至少一种含氮水溶性聚合物和至少一种疏水性聚合物。颗粒在120℃至300℃的温度下进行热处理。

10. 发明申请

US20090029044A1 Absorbent Article Comprising Water-Absorbing Polymeric Particles And Method For The Production Thereof 审中-公开
标题翻译：包含吸水性聚合物颗粒的吸收性物品及其制造方法
公开(公告)号：US20090029044A1
公开(公告)日：2009-01-29
申请号：US12146521
申请日：2008-06-26
申请人： Thomas Daniel , Ulrich Riegel , Mark Elliott , Stefan Bruhns , Dieter Hermeling
发明人： Thomas Daniel , Ulrich Riegel , Mark Elliott , Stefan Bruhns , Dieter Hermeling
IPC分类号： B05D3/02
CPC分类号： A61L15/60
摘要： The invention refers to absorbent structures for use in an absorbent article, the absorbent structure comprising a water absorbing material. The water absorbing material is obtainable by a process comprising the steps of bringing particles of a non surface-crosslinked water-absorbing polymer in contact with at least one postcrosslinker, at least one Nitrogen-containing water-soluble polymer, and at least one hydrophobic polymer. The particles are heat-treated at a temperature in the range from 120° C. to 300° C.
摘要翻译：本发明涉及用于吸收制品的吸收结构，该吸收结构包括吸水材料。吸水材料可以通过包括以下步骤的方法获得，所述方法包括使非表面交联的吸水聚合物的颗粒与至少一种后交联剂，至少一种含氮水溶性聚合物和至少一种疏水性聚合物接触。颗粒在120℃至300℃的温度下进行热处理。

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