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1. 发明公开

EP2995587A1 GRAPHENE MATERIAL AND METHOD OF PREPARING THE SAME 审中-公开
标题翻译：维多利亚州立大学DAVON
公开(公告)号：EP2995587A1
公开(公告)日：2016-03-16
申请号：EP15184220.0
申请日：2015-09-08
申请人： Liu, Jianhong
发明人： LIU, Jianhong , ZHANG, Qianling , HE, Chuanxin , XU, Jian , HU, Chao
IPC分类号： C01B31/04
CPC分类号： C01B31/0446 , C01B32/182 , C01B32/184
摘要： A method of preparing a graphene material. The method includes: (1) preparing a liquid polyacrylonitrile (LPAN) solution, stirring the LPAN solution to yield a cyclized polyacrylonitrile solution; (2) stirring the cyclized LPAN solution at between 200 and 300°C to yield a thermally-oxidized polyacrylonitrile; (3) grinding and sieving the thermally-oxidized polyacrylonitrile, and drying a resulting product at room temperature, to yield a thermally-oxidized precursor; (4) calcining the thermally-oxidized precursor in the presence of an inert gas flow of between 10 and 500 mL/min for between 1 and 24 hrs at the temperature of between 400 and 1000°C, to yield a carbonized precursor; and (5) calcining the carbonized precursor in the presence of an inert gas flow of between 10 and 500 mL/min for between 1 and 10 hrs at the temperature of between 1000 and 3000°C, to yield a graphene material.
摘要翻译：一种制备石墨烯材料的方法。该方法包括：（1）制备液态聚丙烯腈（LPAN）溶液，搅拌LPAN溶液，得到环化聚丙烯腈溶液; （2）在200-300℃之间搅拌环化的LPAN溶液，得到热氧化聚丙烯腈; （3）研磨和筛分热氧化聚丙烯腈，并在室温下干燥所得产物，得到热氧化前体; （4）在惰性气体流量为10-500mL / min的条件下，在400-1000℃的温度下煅烧热氧化的前体1至24小时，得到碳化前体; 和（5）在1000-3000℃的温度下，在10-500mL / min的惰性气体流动存在下煅烧碳化前体1至10小时，得到石墨烯材料。

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