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    • 1. 发明授权
    • Process and apparatus for treating gaseous products of sol-gel manufacturing
    • 用于处理溶胶 - 凝胶制造气体产品的方法和设备
    • US06398849B1
    • 2002-06-04
    • US09566850
    • 2000-05-08
    • Lisa Carol GreenDavid A MixonEric M Monberg
    • Lisa Carol GreenDavid A MixonEric M Monberg
    • B01D4714
    • B01D53/1487B01D47/14
    • A process deals with gaseous by-products and tarry materials during formation of sol-gel bodies. Gaseous products from a dehydroxylation reactor pass into a gas-fluid contactor. During the early stages of heat treatment, an aqueous acid solution is recirculated through the contactor to trap basic and/or water soluble organic gaseous materials. The resultant solution and non-condensing gases pass into a reservoir. Volatile, undissolved organics exit from the reservoir with non-condensing reactor gases and are treated. Once the organics have burned out of the sol-gel body, recirculation of the aqueous acid solution is ceased, and the gas-fluid contactor is flushed. The water flow is then ceased and dry nitrogen is provided to the contactor. During the next stage of the sol-gel heat treatment, gaseous products from the dehydroxylation reactor pass through the contactor into the caustic scrubber. Once the heat treatment is complete, the contactor is flushed.
    • 一个过程在溶胶凝胶体形成期间处理气态副产物和焦油物质。 来自脱羟基化反应器的气态产物进入气液接触器。 在热处理的早期阶段,酸性水溶液通过接触器再循环以捕集碱性和/或水溶性有机气态物质。 所得溶液和非冷凝气体进入储存器。 挥发性,未溶解的有机物从具有非冷凝反应器气体的储层中排出并进行处理。 一旦有机物从溶胶 - 凝胶体中烧掉,酸性水溶液的再循环停止,并且气体 - 流体接触器被冲洗。 然后停止水流,向接触器提供干燥的氮气。 在溶胶 - 凝胶热处理的下一阶段,来自脱羟基反应器的气态产物通过接触器进入苛性碱洗涤器。 一旦热处理完成,接触器就会被冲洗掉。