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1. 发明授权

US10457597B2 Adhesion promoters and gel-modifiers for olefin metathesis compositions 有权
公开(公告)号：US10457597B2
公开(公告)日：2019-10-29
申请号：US14125837
申请日：2012-06-17
申请人： Li-Sheng Wang , Anthony R. Stephen , Paul W. Boothe , Tessa Schulze , Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Farshad J. Motamedi , Brian Edgecombe
发明人： Li-Sheng Wang , Anthony R. Stephen , Paul W. Boothe , Tessa Schulze , Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Farshad J. Motamedi , Brian Edgecombe
IPC分类号： C03C25/30 , C08K5/00 , C08K5/14 , C08K5/29 , C08F32/02 , C08G61/08
摘要： This invention relates to compositions and methods for improving the adhesion of resin compositions to substrate materials, pre-treating substrate materials to improve the adhesion of resin compositions to the substrate materials, and/or controlling gel formation of resin compositions. More particularly, the invention relates to compositions and methods for improving the adhesion of ring opening metathesis polymerization (ROMP) compositions to substrate materials using adhesion promoters containing isocyariate groups in a resin composition. The invention also relates to methods for improving the adhesion of resin compositions to substrate materials by pre-treating substrate materials with adhesion promoters containing isocyanate groups. The invention further relates to a method of providing a gel-modified ROMP composition, in which a hydroperoxide is added to a ROMP polymerizable resin composition in order to control gel formation of the polymerizing resin. An improved ROMP composition is further disclosed, comprising a cyclic olefin, a ROMP metathesis catalyst, an adhesion promoter, and an added hydroperoxide gel modifier. The polymer products produced via ROMP reactions of the invention may be utilized for a wide range of materials and composite applications. The invention has utility in the fields of catalysis, organic synthesis, and polymer and materials chemistry and manufacture.

2. 发明申请

US20140329017A1 ADHESION PROMOTERS AND GEL-MODIFIERS FOR OLEFIN METATHESIS COMPOSITIONS 审中-公开
标题翻译：粘合剂组合物的粘合促进剂和凝胶改性剂
公开(公告)号：US20140329017A1
公开(公告)日：2014-11-06
申请号：US14125837
申请日：2012-06-17
申请人： Li-Sheng Wang , Anthony R. Stephen , Paul W. Booth , Tessa Schulze , Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Farshad J. Motamedi , Brian Edgecombe
发明人： Li-Sheng Wang , Anthony R. Stephen , Paul W. Booth , Tessa Schulze , Michael A. Giardello , Mark S. Trimmer , Christopher J. Cruce , Farshad J. Motamedi , Brian Edgecombe
IPC分类号： C03C25/30
CPC分类号： C03C25/30 , C08F32/02 , C08G61/08 , C08G2261/3325 , C08G2261/418 , C08K5/0025 , C08K5/14 , C08K5/29 , C08K2201/014 , C08L65/00
摘要： This invention relates to compositions and methods for improving the adhesion of resin compositions to substrate materials, pre-treating substrate materials to improve the adhesion of resin compositions to the substrate materials, and/or controlling gel formation of resin compositions. More particularly, the invention relates to compositions and methods for improving the adhesion of ring opening metathesis polymerization (ROMP) compositions to substrate materials using adhesion promoters containing isocyariate groups in a resin composition. The invention also relates to methods for improving the adhesion of resin compositions to substrate materials by pre-treating substrate materials with adhesion promoters containing isocyanate groups. The invention further relates to a method of providing a gel-modified ROMP composition, in which a hydroperoxide is added to a ROMP polymerizable resin composition in order to control gel formation of the polymerizing resin. An improved ROMP composition is further disclosed, comprising a cyclic olefin, a ROMP metathesis catalyst, an adhesion promoter, and an added hydroperoxide gel modifier. The polymer products produced via ROMP reactions of the invention may be utilized for a wide range of materials and composite applications. The invention has utility in the fields of catalysis, organic synthesis, and polymer and materials chemistry and manufacture.
摘要翻译：本发明涉及用于改善树脂组合物与基材的粘合性，预处理基材以改善树脂组合物与基材的粘合性和/或控制树脂组合物凝胶形成的组合物和方法。更具体地，本发明涉及使用在树脂组合物中含有异质基团的粘合促进剂来改善开环易位聚合（ROMP）组合物与基材的粘合性的组合物和方法。本发明还涉及通过用含有异氰酸酯基团的粘合促进剂预处理底物材料来改善树脂组合物对基材的粘附性的方法。本发明还涉及一种提供凝胶改性的ROMP组合物的方法，其中将氢过氧化物加入到ROMP可聚合树脂组合物中以控制聚合树脂的凝胶形成。进一步公开了改进的ROMP组合物，其包含环烯烃，ROMP复分解催化剂，粘合促进剂和加入的氢过氧化物凝胶改性剂。通过本发明的ROMP反应生产的聚合物产品可用于广泛的材料和复合材料应用。本发明可用于催化，有机合成，聚合物和材料的化学和制造领域。

3. 发明授权

US08324334B2 Telechelic olefin metathesis polymers from renewable feedstocks 有权
标题翻译：来自可再生原料的远视烯烃易位聚合物
公开(公告)号：US08324334B2
公开(公告)日：2012-12-04
申请号：US13060058
申请日：2009-08-21
申请人： Simon C. Jones , Farshad J. Motamedi , Li-Sheng Wang , Brian Edgecombe , Michael A. Giardello
发明人： Simon C. Jones , Farshad J. Motamedi , Li-Sheng Wang , Brian Edgecombe , Michael A. Giardello
IPC分类号： C08G61/08 , C08F4/80
CPC分类号： C08G61/08 , C08G2261/3322 , C08G2261/418
摘要： Olefin metathesis polymerization reactions are disclosed, and more particularly ring-opening metathesis polymerization of cyclic olefins with olefinic compounds, such as are derived from seed oils and the like, to form telechelic polymers. In one aspect, a method is provided for carrying out a catalytic ring-opening metathesis polymerization reaction, comprising contacting at least one olefinic compound with at least one cyclic olefin, in the presence of a ruthenium alkylidene olefin metathesis catalyst under conditions effective to allow ring-opening metathesis polymerization of the cyclic olefin, whereby the cyclic olefin polymer formed is terminated with the olefinic compound. The invention has utility in the fields of catalysis, organic synthesis, polymer chemistry, and industrial chemistry.
摘要翻译：公开了烯烃易位聚合反应，更具体地说，环烯烃与烯烃化合物如来自种子油等的开环易位聚合反应形成遥爪聚合物。在一个方面，提供了一种用于进行催化开环易位聚合反应的方法，包括在钌亚烷基烯烃复分解催化剂存在下使至少一种烯烃化合物与至少一种环烯烃接触，所述条件有效地允许环开环环烯烃的易位聚合，由此所形成的环烯烃聚合物用烯烃化合物终止。本发明可用于催化，有机合成，聚合物化学和工业化学领域。

4. 发明申请

US20110294971A1 Telechelic Olefin Metathesis Polymers from Renewable Feedstocks 有权
标题翻译：来自可再生原料的非线性烯烃复分解聚合物
公开(公告)号：US20110294971A1
公开(公告)日：2011-12-01
申请号：US13060058
申请日：2009-08-21
申请人： Simon C. Jones , Farshad J. Motamedi , Li-Sheng Wang , Brian Edgecombe , Michael A. Giardello
发明人： Simon C. Jones , Farshad J. Motamedi , Li-Sheng Wang , Brian Edgecombe , Michael A. Giardello
IPC分类号： C08F216/04 , C08F232/06 , C08F232/04 , C08F4/80 , C08F222/20 , C08F220/68 , C08F216/10
CPC分类号： C08G61/08 , C08G2261/3322 , C08G2261/418
摘要： Olefin metathesis polymerization reactions are disclosed, and more particularly ring-opening metathesis polymerization of cyclic olefins with olefinic compounds, such as are derived from seed oils and the like, to form telechelic polymers. In one aspect, a method is provided for carrying out a catalytic ring-opening metathesis polymerization reaction, comprising contacting at least one olefinic compound with at least one cyclic olefin, in the presence of a ruthenium alkylidene olefin metathesis catalyst under conditions effective to allow ring-opening metathesis polymerization of the cyclic olefin, whereby the cyclic olefin polymer formed is terminated with the olefinic compound. The invention has utility in the fields of catalysis, organic synthesis, polymer chemistry, and industrial chemistry.
摘要翻译：公开了烯烃易位聚合反应，更具体地说，环烯烃与烯烃化合物如来自种子油等的开环易位聚合反应形成遥爪聚合物。在一个方面，提供了一种用于进行催化开环易位聚合反应的方法，包括在钌亚烷基烯烃复分解催化剂存在下使至少一种烯烃化合物与至少一种环烯烃接触，所述条件有效地允许环开环环烯烃的易位聚合，由此所形成的环烯烃聚合物用烯烃化合物终止。本发明可用于催化，有机合成，聚合物化学和工业化学领域。

5. 发明申请

US20090095635A1 MICROFLUIDIC RADIOSYNTHESIS OF A RADIOLABELED COMPOUND USING ELECTROCHEMICAL TRAPPING AND RELEASE 审中-公开
标题翻译：使用电化学捕获和释放的无定形化合物的微流体放射线
公开(公告)号：US20090095635A1
公开(公告)日：2009-04-16
申请号：US12176296
申请日：2008-07-18
申请人： Arkadij M. Elizarov , Hartmuth C. Kolb , R. Michael van Dam , James R. Heath , Brian Edgecombe , Farshad Motamedi , Anthony Stephen , Michael A. Giardello
发明人： Arkadij M. Elizarov , Hartmuth C. Kolb , R. Michael van Dam , James R. Heath , Brian Edgecombe , Farshad Motamedi , Anthony Stephen , Michael A. Giardello
IPC分类号： C25B3/08
CPC分类号： C07B59/00
摘要： Methods and apparatus enable radiosynthesis of radiolabeled compounds using electrochemical trapping and release. The trapping and release of radioactive isotopes all occur inside a microreactor, a vial or similar device, thus eliminating the need for azeotropic drying and several dead-end filling steps, as well as the necessity to move concentrated radioisotopes from one compartment of the chip to another. These and other features allow radioisotope enrichment to be carried out internally within a radiochemical synthesis chip, providing faster and more robust operation, as well as producing very high radiochemical labeling yields.
摘要翻译：方法和装置能够使用电化学捕获和释放来放射性标记化合物的放射合成。放射性同位素的捕获和释放都发生在微反应器，小瓶或类似装置内，因此不需要共沸干燥和几个死端填充步骤，以及将浓缩放射性同位素从芯片的一个室移动到另一个。这些和其他特征允许放射性同位素富集在放射化学合成芯片内部进行，提供更快和更强的操作，以及产生非常高的放射化学标记产率。

6. 发明申请

US20050154140A1 Core-shell polymers having hydrophilic shells for improved shell coverage and anti-blocking properties 有权
标题翻译：具有亲水壳的核 - 壳聚合物用于改善壳覆盖性和抗粘连性
公开(公告)号：US20050154140A1
公开(公告)日：2005-07-14
申请号：US10980720
申请日：2004-11-03
申请人： Sheng Hong , Rosangela Pirri , Brian Edgecombe
发明人： Sheng Hong , Rosangela Pirri , Brian Edgecombe
IPC分类号： C08J3/12 , C08F2/22 , C08F2/44 , C08F265/06 , C08F279/02 , C08F285/00 , C08L51/04 , C08L101/00 , C08L51/00
CPC分类号： C08L51/04 , C08F265/06 , C08F285/00 , Y10T428/2989 , C08F2/22
摘要： The present invention relates to core-shell polymers having a hydrophilic copolymer shell, and a high level of core material of from 75 to 95 weight percent. The hydrophilic shell provides better coverage of the core resulting in better powder properties such as anti-blockinig. The hydrophilic shell also allows for a thinner shell and a larger elastomeric core. Core-shell polymers of the invention are especially useful as impact modifiers for plastic materials.
摘要翻译：本发明涉及具有亲水共聚物壳的核 - 壳聚合物和75-95重量％的高含量的芯材。亲水壳提供更好的芯的覆盖，导致更好的粉末性质，如抗嵌段。亲水外壳还允许更薄的外壳和更大的弹性体芯。本发明的核 - 壳聚合物特别用作塑料材料的抗冲改性剂。

7. 发明申请

US20080262156A1 Impact Modified Acrylics Having a Bimodal Distribution of Impact Modifier Sizes 有权
标题翻译：具有冲击改性剂双峰分布的冲击改性丙烯酸酯
公开(公告)号：US20080262156A1
公开(公告)日：2008-10-23
申请号：US12091071
申请日：2006-09-28
申请人： Harold R. Banyay , Brian Edgecombe
发明人： Harold R. Banyay , Brian Edgecombe
IPC分类号： C08L53/00
CPC分类号： B32B27/08 , B32B9/045 , B32B15/082 , B32B21/04 , B32B21/08 , B32B27/308 , B32B2333/04 , C08L33/10 , C08L51/003 , C08L51/006 , C08L51/04 , C08L53/00 , C08L2666/24 , C08L2666/02 , C08L2666/14
摘要： The invention relates to an impact modified acrylic sheet composition having a bimodal distribution of impact modifier particle sizes. The composition provides an optimal balance of impact performance and appearance after melt processing.
摘要翻译：本发明涉及具有抗冲击改性剂颗粒尺寸的双峰分布的抗冲改性丙烯酸类片材组合物。组合物在熔融加工后提供冲击性能和外观的最佳平衡。

8. 发明申请

US20050266182A1 Thermoplastic article with a printable matte surface 有权
标题翻译：具有可印刷无光泽表面的热塑性制品
公开(公告)号：US20050266182A1
公开(公告)日：2005-12-01
申请号：US11123539
申请日：2005-05-06
申请人： Brian Edgecombe
发明人： Brian Edgecombe
IPC分类号： B41M5/00 , B41M5/52
CPC分类号： B41M5/5263 , B41M5/52 , B41M5/5218 , B41M5/5254 , B41M5/5272 , B41M5/529 , C08K3/22 , C08K3/26 , C08K3/36 , Y10T428/2982 , Y10T428/31721 , Y10T428/31786 , Y10T428/31855
摘要： This invention relates to thermoplastic articles having printable matte surfaces. The printable matte surface is achieved by blending inorganic particles, and especially silica particles, having a mean particle size of from 2 to 30 micron and a narrow particle size distribution into the thermoplastic at from 15 to 30 percent by weight.
摘要翻译：本发明涉及具有可印刷无光泽表面的热塑性制品。可印刷的无光泽表面是通过将平均粒径为2至30微米的无机颗粒，特别是二氧化硅颗粒与15-30重量％的热塑性混合物混合而成的。

9. 发明授权

US07195820B2 Core-shell polymers having hydrophilic shells for improved shell coverage and anti-blocking properties 有权
标题翻译：具有亲水壳的核 - 壳聚合物用于改善壳覆盖性和抗粘连性
公开(公告)号：US07195820B2
公开(公告)日：2007-03-27
申请号：US10980720
申请日：2004-11-03
申请人： Sheng Hong , Rosangela Pirri , Brian Edgecombe
发明人： Sheng Hong , Rosangela Pirri , Brian Edgecombe
IPC分类号： A61K9/50 , B01J13/03 , B32B5/16
CPC分类号： C08L51/04 , C08F265/06 , C08F285/00 , Y10T428/2989 , C08F2/22
摘要： The present invention relates to core-shell polymers having a hydrophilic copolymer shell, and a high level of core material of from 75 to 95 weight percent. The hydrophilic shell provides better coverage of the core resulting in better powder properties such as anti-blocking. The hydrophilic shell also allows for a thinner shell and a larger elastomeric core. Core-shell polymers of the invention are especially useful as impact modifiers for plastic materials.
摘要翻译：本发明涉及具有亲水共聚物壳的核 - 壳聚合物和75-95重量％的高含量的芯材。亲水壳提供更好的芯的覆盖，导致更好的粉末性质，如防粘连。亲水外壳还允许更薄的外壳和更大的弹性体芯。本发明的核 - 壳聚合物特别用作塑料材料的抗冲改性剂。

10. 发明申请

US20060211803A1 Clays pre-activated with intercalated polymerization initiation sites 审中-公开
标题翻译：粘土通过嵌入的聚合引发位点预活化
公开(公告)号：US20060211803A1
公开(公告)日：2006-09-21
申请号：US11081334
申请日：2005-03-16
申请人： Nicholas Rodak , Brian Edgecombe , Noah Macy
发明人： Nicholas Rodak , Brian Edgecombe , Noah Macy
IPC分类号： C08K9/04
CPC分类号： C08K9/04 , C01B33/44 , C01P2002/22 , C01P2002/72 , C01P2002/86 , C01P2002/88
摘要： A modified clay may be made by contacting a clay with an unsaturated cationic compound and an alkoxyamine, or an adduct thereof. The resulting pre-activated clay, which contains a cationic alkoxyamine bound to the clay, may be further treated with a monomer to provide a polymer that is bound to the clay, thereby forming a nanocomposite material. The nanocomposite material may in turn be blended with another polymer prepared from the same or a different monomer.
摘要翻译：改性粘土可以通过使粘土与不饱和阳离子化合物和烷氧基胺或其加合物接触来制备。所得到的预活化粘土含有与粘土结合的阳离子烷氧基胺，可进一步用单体处理，以提供与粘土结合的聚合物，由此形成纳米复合材料。纳米复合材料又可以与由相同或不同单体制备的另一种聚合物共混。

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