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1. 发明申请

US20080132735A1 Process for the Preparation of Phenol 失效
标题翻译：苯酚的制备方法
公开(公告)号：US20080132735A1
公开(公告)日：2008-06-05
申请号：US11813874
申请日：2006-01-10
申请人： Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni , Fausto Genoni , Guido Spano , Franco Rivetti
发明人： Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni , Fausto Genoni , Guido Spano , Franco Rivetti
IPC分类号： C07C37/64
CPC分类号： B01J23/002 , B01J23/31 , B01J23/8885 , B01J2523/00 , C07C37/00 , C07C37/58 , Y02P20/52 , B01J2523/17 , B01J2523/27 , B01J2523/69 , B01J2523/54 , B01J2523/55 , B01J2523/68 , B01J2523/842 , B01J2523/3712 , B01J2523/56 , C07C39/04
摘要： A process is described for the preparation of phenol by the hydrodeoxygenation of polyhydroxylated benzene derivatives or by the selective hydroxylation of benzene under depletive conditions, characterized in that the above-mentioned reactions are carried out in the presence of a catalyst based on multi component metal oxides comprising at least one metal selected from the groups VB, VIB, VIII, IB, IIB, IVA, VA.
摘要翻译：描述了通过多羟基化苯衍生物的加氢脱氧或通过在脱碱条件下苯的选择性羟基化制备苯酚的方法，其特征在于上述反应在基于多组分金属氧化物的催化剂存在下进行包括选自组VB，VIB，VIII，IB，IIB，IVA，VA中的至少一种金属。

2. 发明授权

US07868210B2 Process for the preparation of phenol 失效
标题翻译：苯酚的制备方法
公开(公告)号：US07868210B2
公开(公告)日：2011-01-11
申请号：US11813874
申请日：2006-01-10
申请人： Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni , Fausto Genoni , Guido Spano′ , Franco Rivetti
发明人： Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni , Fausto Genoni , Guido Spano′ , Franco Rivetti
IPC分类号： C07C37/06 , C07C39/00
CPC分类号： B01J23/002 , B01J23/31 , B01J23/8885 , B01J2523/00 , C07C37/00 , C07C37/58 , Y02P20/52 , B01J2523/17 , B01J2523/27 , B01J2523/69 , B01J2523/54 , B01J2523/55 , B01J2523/68 , B01J2523/842 , B01J2523/3712 , B01J2523/56 , C07C39/04
摘要： A process is described for the preparation of phenol by the hydrodeoxygenation of polyhydroxylated benzene derivatives or by the selective hydroxylation of benzene under depletive conditions, characterized in that the above-mentioned reactions are carried out in the presence of a catalyst based on multi component metal oxides comprising at least one metal selected from the groups VB, VIB, VIII, IB, IIB, IVA, VA.
摘要翻译：描述了通过多羟基化苯衍生物的加氢脱氧或通过在脱碱条件下苯的选择性羟基化制备苯酚的方法，其特征在于上述反应在基于多组分金属氧化物的催化剂存在下进行包括选自组VB，VIB，VIII，IB，IIB，IVA，VA中的至少一种金属。

3. 发明授权

US08247622B2 Process for the preparation of phenol 失效
标题翻译：苯酚的制备方法
公开(公告)号：US08247622B2
公开(公告)日：2012-08-21
申请号：US12908583
申请日：2010-10-20
申请人： Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni , Fausto Genoni , Guido Spano , Franco Rivetti
发明人： Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni , Fausto Genoni , Guido Spano , Franco Rivetti
IPC分类号： C07C37/00
CPC分类号： B01J23/002 , B01J23/31 , B01J23/8885 , B01J2523/00 , C07C37/00 , C07C37/58 , Y02P20/52 , B01J2523/17 , B01J2523/27 , B01J2523/69 , B01J2523/54 , B01J2523/55 , B01J2523/68 , B01J2523/842 , B01J2523/3712 , B01J2523/56 , C07C39/04
摘要： A process is described for the preparation of phenol by the hydrodeoxygenation of polyhydroxylated benzene derivatives or by the selective hydroxylation of benzene under depletive conditions, characterized in that the above-mentioned reactions are carried out in the presence of a catalyst based on multi component metal oxides comprising at least one metal selected from the groups VB, VIB, VIII, IB, IIB, IVA, VA.
摘要翻译：描述了通过多羟基化苯衍生物的加氢脱氧或通过在脱碱条件下苯的选择性羟基化制备苯酚的方法，其特征在于上述反应在基于多组分金属氧化物的催化剂存在下进行包括选自组VB，VIB，VIII，IB，IIB，IVA，VA中的至少一种金属。

4. 发明授权

US06645899B1 Method of the removal of the templating agent from synthetic zeolites 有权
标题翻译：从合成沸石中除去模板剂的方法
公开(公告)号：US06645899B1
公开(公告)日：2003-11-11
申请号：US09712213
申请日：2000-11-15
申请人： Stefano Palmery , Fausto Genoni , Guido Spano′ , Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni
发明人： Stefano Palmery , Fausto Genoni , Guido Spano′ , Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni
IPC分类号： B01J2906
CPC分类号： B01J29/035 , B01J29/06 , B01J29/40 , B01J29/7007 , B01J29/7034 , B01J29/89 , B01J2229/40 , C01B37/00 , C01B37/02 , C01B39/026 , C07C249/04 , C07D201/04 , C07C251/44
摘要： The present invention relates to a method for the removal of the templating agent from synthetic zeolites in general and in particular from silicalite, titanium silicalite and from composite materials containing zeolites and for their activation as catalysts. The method consists in treating the above materials with solvents in vapor phase and at a low temperature.
摘要翻译：本发明涉及通常从合成沸石中去除模板剂的方法，特别是从硅沸石，钛硅沸石以及含有沸石的复合材料中除去模板剂的方法，以及它们作为催化剂的活化。该方法包括用溶剂处理上述物质在气相和低温下。

5. 发明授权

US06949687B2 Process for the production of mesitylene and durene 失效
标题翻译：生产均三甲苯和杜烯的方法
公开(公告)号：US06949687B2
公开(公告)日：2005-09-27
申请号：US10736594
申请日：2003-12-17
申请人： Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni , Franco Rivetti , Caterina Rizzo , Virginio Arrigoni , Carlo Perego
发明人： Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni , Franco Rivetti , Caterina Rizzo , Virginio Arrigoni , Carlo Perego
IPC分类号： B01J29/08 , B01J29/18 , B01J29/70 , B01J29/90 , B01J38/02 , C07B61/00 , C07C2/70 , C07C5/27 , C07C6/12 , C07C15/02 , C07C5/22
CPC分类号： C07C6/123 , C07C5/2737 , C07C15/02
摘要： A process is described for the contemporaneous preparation of mesitylene and durene, characterized in that mesitylene and durene are obtained exclusively starting from pseudo-cumene without the use of any further chemical compound, operating in continuous, at a temperature ranging from 210 to 400° C., at a pressure ranging from 1 to 50 bar, with a weight space velocity ranging from 0.1 to 20 hours−1 and in the presence of a catalyst based on crystalline metal-silicates in acid form. After the recovery of mesitylene and durene from the reaction raw product, some of the remaining components of the raw product itself are recycled and fed to the reactor together with the pseudo-cumene.
摘要翻译：描述了同时制备均三甲苯和杜烯的方法，其特征在于，均三甲苯和杜烯仅从起始伪异丙苯开始获得，而不使用任何其它化学化合物，连续操作，温度范围为210-400℃ 在1至50巴的压力下，重量空间速度为0.1至20小时-1的范围内，并且在基于酸形式的结晶金属硅酸盐的催化剂存在下进行。在从反应原料中回收均三甲苯和杜烯后，原料的其余部分本身被再循环并与假枯烯一起进料到反应器中。

6. 发明申请

US20070267324A1 Process and Catalysts for the Production of Linear Alkanes 审中-公开
标题翻译：用于生产线性烷烃的方法和催化剂
公开(公告)号：US20070267324A1
公开(公告)日：2007-11-22
申请号：US10590313
申请日：2005-02-04
申请人： Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni , Franco Rivetti
发明人： Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni , Franco Rivetti
IPC分类号： C10G35/09
CPC分类号： C10G47/20 , B01J29/088 , B01J29/126 , B01J29/146 , B01J29/166 , B01J29/86 , B01J29/87 , B01J29/88 , B01J29/89 , B01J2229/183 , B01J2229/20 , B01J2229/42 , C07C4/06 , C07C2529/10 , C07C2529/12 , C07C2529/14 , C10G47/16 , C10G47/18 , C07C9/00
摘要： The invention relates to a process for the production of linear alkanes, containing less than 6′ carbon atoms, from a mix comprising one or more hydrocarbons containing at least 6 carbon atoms. The process uses a catalytic composition comprising particular combinations of a Y-type zeolite, at least one element selected from Zn, Mo, Cu, Ga, In, W, Ta, Zr, Ti, metals of Group VIII and optionally one or more lanthanides.
摘要翻译：本发明涉及从包含一种或多种含有至少6个碳原子的烃的混合物生产包含少于6个碳原子的直链烷烃的方法。该方法使用包含Y型沸石，至少一种选自Zn，Mo，Cu，Ga，In，W，Ta，Zr，Ti，VIII族金属和任选的一种或多种镧系元素的特定组合的催化组合物。

7. 发明授权

US06936738B2 Process for the preparation of phenol by means of the hydrodeoxygenation of benzene-diols 有权
标题翻译：通过苯二醇的加氢脱氧制备苯酚的方法
公开(公告)号：US06936738B2
公开(公告)日：2005-08-30
申请号：US10683403
申请日：2003-10-14
申请人： Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni , Franco Rivetti
发明人： Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni , Franco Rivetti
IPC分类号： C07C37/88 , B01J23/28 , B01J23/30 , B01J23/42 , B01J23/60 , B01J23/75 , B01J23/88 , B01J23/881 , B01J23/882 , B01J23/888 , B01J27/188 , C07B61/00 , C07C29/60 , C07C37/00 , C07C39/04 , C07C39/06 , C07C39/00
CPC分类号： B01J23/60 , B01J23/28 , B01J23/30 , B01J23/42 , B01J23/75 , B01J23/881 , B01J23/882 , B01J23/8885 , B01J27/188 , C07C37/00 , Y02P20/52 , C07C39/04
摘要： A process is described for the preparation of phenol characterized in that the phenol is obtained by means of the hydrodeoxygenation of benzene-diols with hydrogen, operating in continuous, in an aqueous solution, at temperatures ranging from 250 to 500° C., at pressures of 1-100 bar and in the presence of a catalyst based on elements of group VIB or group VIII of the periodic table.
摘要翻译：描述了一种用于制备苯酚的方法，其特征在于通过苯二醇与氢在水溶液中在250-500℃的温度下在压力下连续操作，在氢气中进行加氢脱氧，得到苯酚。在基于元素周期表VIB族或VIII族元素的催化剂的存在下进行。

8. 发明申请

US20050032630A1 Process for the preparation of MFI-type zeolitic catalysts 有权
标题翻译：制备MFI型沸石催化剂的方法
公开(公告)号：US20050032630A1
公开(公告)日：2005-02-10
申请号：US10944802
申请日：2004-09-21
申请人： Luigi Balducci , Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni
发明人： Luigi Balducci , Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni
IPC分类号： C07D201/04 , B01J29/035 , B01J29/40 , C01B37/02 , C10G11/05 , B01J29/06
CPC分类号： B01J29/035 , B01J29/40 , B01J37/0072 , B01J37/033 , B01J2229/42
摘要： The present invention relates to a process for the preparation of zeolitic catalysts of the MFI type in spheroidal form. The process consists in emulsifying and consolidating in paraffinic hydrocarbons, in the presence of a non-ionic surface-active agent or a suitable combination of a non-ionic surface-active agent and a cationic surface-active agent, a dispersion of particles of zeolitic material of the MFI type in a silica sol.
摘要翻译：本发明涉及一种以球形形式制备MFI型沸石催化剂的方法。该方法包括在非离子表面活性剂或非离子表面活性剂和阳离子表面活性剂的合适组合的存在下在链烷烃中乳化和固结，沸石颗粒的分散体在硅溶胶中的MFI型材料。

9. 发明授权

US07214637B2 Process for the preparation of MFI-type zeolitic catalysts 有权
标题翻译：制备MFI型沸石催化剂的方法
公开(公告)号：US07214637B2
公开(公告)日：2007-05-08
申请号：US10944802
申请日：2004-09-21
申请人： Luigi Balducci , Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni
发明人： Luigi Balducci , Leonardo Dalloro , Alberto Cesana , Roberto Buzzoni
IPC分类号： B01J29/06
CPC分类号： B01J29/035 , B01J29/40 , B01J37/0072 , B01J37/033 , B01J2229/42
摘要： The present invention relates to a process for the preparation of zeolitic catalysts of the MFI type in spheroidal form.The process consists in emulsifying and consolidating in paraffinic hydrocarbons, in the presence of a non-ionic surface-active agent or a suitable combination of a non-ionic surface-active agent and a cationic surface-active agent, a dispersion of particles of zeolitic material of the MFI type in a silica sol.
摘要翻译：本发明涉及一种以球形形式制备MFI型沸石催化剂的方法。该方法包括在非离子表面活性剂或非离子表面活性剂和阳离子表面活性剂的合适组合的存在下在链烷烃中乳化和固结，沸石颗粒的分散体在硅溶胶中的MFI型材料。

10. 发明授权

US07038093B2 Integrated process for the preparation of phenol from benzene with recycling of the by-products 有权
标题翻译：从苯中制备苯酚的副产物回收综合工艺
公开(公告)号：US07038093B2
公开(公告)日：2006-05-02
申请号：US10716460
申请日：2003-11-20
申请人： Daniele Bianchi , Rossella Bortolo , Roberto Buzzoni , Alberto Cesana , Leonardo Dalloro , Rino D'Aloisio
发明人： Daniele Bianchi , Rossella Bortolo , Roberto Buzzoni , Alberto Cesana , Leonardo Dalloro , Rino D'Aloisio
IPC分类号： C07C37/00
CPC分类号： C07C37/60 , B01J29/89 , B01J2229/30 , Y02P20/125 , Y02P20/52 , C07C39/04
摘要： The invention relates to a process for the preparation of phenol comprising the following phases: 1) preparation in continuous of phenol by means of the direct oxidation of benzene with hydrogen peroxide operating with an H2O2/benzene ratio ranging from 10 to 70%, in a three-phase reaction system comprising a first liquid phase consisting of benzene and an organic solvent, a second liquid phase consisting of water, a solid phase consisting of an activated catalyst based on titanium silicalite TS-1; 2) separation of the phenol and non-reacted benzene from the reaction mixture of the oxidation section (1), by means of fractionated distillation; 3) separation of the solvent and by-products from the mixture coming from the distillation tail (2), by means of basic extraction; 4) transformation of the by-products obtain in section (3) to phenol by means of hydrodeoxygenation with hydrogen operating in continuous, in aqueous solution, at a temperature ranging from 250 to 500° C., at pressures of 1-100 bar and in the presence of a catalyst based on elements of group VIB or their mixtures or group VIII of the periodic table or their mixtures; 5) recycling of the phenol obtained in section (4) to the distillation section (2).
摘要翻译：本发明涉及一种制备苯酚的方法，包括以下阶段：1）通过苯与氧化氢的直接氧化制备苯酚连续操作，所述过氧化氢用H 2 O 2 在含有由苯和有机溶剂组成的第一液相的三相反应体系中，第二液相由水组成，固相由活化的基于钛硅沸石TS-1的催化剂; 2）通过分级蒸馏从氧化段（1）的反应混合物中分离苯酚和未反应的苯; 3）通过碱性萃取法从蒸馏尾料（2）中分离出溶剂和副产物与混合物; 4）将第（3）部分获得的副产物转化为苯酚，通过加氢脱氧，氢气在连续的水溶液中，在250-500℃的温度，1-100巴的压力和在基于元素周期表VIB族元素或它们的混合物或VIII族元素或其混合物的催化剂的存在下; 5）将第（4）节中得到的酚再循环至蒸馏段（2）。

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