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1. 发明申请

WO2003100206A1 METHOD FOR PREPARING HIGH MOLECULAR WEIGHT POLYCARBONATE 审中-公开
标题翻译：制备高分子量聚碳酸酯的方法
公开(公告)号：WO2003100206A1
公开(公告)日：2003-12-04
申请号：PCT/KR2003/001048
申请日：2003-05-28
申请人： LG CHEM, LTD. , KIM, Jong-Hun , WOO, Boo-Gon , PARK, Eun-Duck , HONG, Mi-Jeung
发明人： KIM, Jong-Hun , WOO, Boo-Gon , PARK, Eun-Duck , HONG, Mi-Jeung
IPC分类号： E21B17/042
CPC分类号： C08G64/307 , Y10T428/31504 , Y10T428/31507
摘要： The present invention relates to a process for preparing high molecular weight polycarbonate resin, particularly to a process for preparing high molecular weight polycarbonate resin, which conducts condensation polymerization of low molecular weight amorphous polycarbonate prepolymer prepared by transesterification of dialkyl(aryl)carbonate and aromatic hydroxy compound and solid state polymerization within short time to increase molecular weight. The present invention introduces condensation polymerization to lower mole fractions of arylcarbonate existing in unreacted diarylcarboante, end groups of reaction by products of polymerization degree less than 3, and polycarbonate prepolymer obtained by transesterification, and thus can maximize molecular weight increase of polycarbonate after solid state polymerization and remarkably reduce time required for preparing polycarbonate of the same molecular weight. In addition, since the present invention does not use toxic substance phosgene, it has no danger and it can prevent deterioration, and it can prepare high molecular weigh polycarbonate that can be used for injection and extrusion.
摘要翻译：本发明涉及一种制备高分子量聚碳酸酯树脂的方法，特别涉及一种制备高分子量聚碳酸酯树脂的方法，该方法进行低分子量无定形聚碳酸酯预聚物的缩聚，其通过二烷基（芳基）碳酸酯和芳族羟基化合物和固态聚合在短时间内增加分子量。本发明将存在于未反应的二芳基羧酸酯中的芳基碳酸酯的摩尔比低，聚合度小于3的产物的反应端基和通过酯交换反应得到的聚碳酸酯预聚物进行缩聚，从而可以使固态聚合后的聚碳酸酯的分子量增加最大化并且显着地减少了制备相同分子量的聚碳酸酯所需的时间。此外，由于本发明不使用有毒物质光气，因此没有危险，可以防止劣化，并且可以制备可用于注射和挤出的高分子量聚碳酸酯。

2. 发明申请

WO2004031259A1 METHOD FOR PREPARING POLYCARBONATE RESIN 审中-公开
标题翻译：制备聚碳酸酯树脂的方法
公开(公告)号：WO2004031259A1
公开(公告)日：2004-04-15
申请号：PCT/KR2003/000799
申请日：2003-04-18
申请人： LG CHEM, LTD. , PARK, Eun-Duck , WOO, Boo-Gon , HONG, Mi-Jeung , KIM, Jong-Hun
发明人： PARK, Eun-Duck , WOO, Boo-Gon , HONG, Mi-Jeung , KIM, Jong-Hun
IPC分类号： C08G64/40
CPC分类号： C08G64/30 , C08G64/307
摘要： The present invention relates to a method for preparing polycarbonate resin, and more particularly to a method for effectively preparing polycarbonate resin having a large molecular weight in a short time under a melt polymerization condition using a catalyst system comprising phosphoranylidene ammonium salts, which is stable and maintains superior reactivity during melt polymerization and solid state polymerization.
摘要翻译：本发明涉及一种制备聚碳酸酯树脂的方法，更具体地说，涉及一种在熔融聚合条件下使用包含亚正膦基铵盐的催化剂体系在短时间内有效制备聚碳酸酯树脂的方法，所述催化剂体系是稳定的，在熔融聚合和固态聚合过程中保持优异的反应性。

3. 发明申请

WO2004041906A1 PREPARATION METHOD OF HIGH MOLECULAR WEIGHT POLYCARBONATE RESIN 审中-公开
标题翻译：高分子量聚碳酸酯树脂的制备方法
公开(公告)号：WO2004041906A1
公开(公告)日：2004-05-21
申请号：PCT/KR2003/002070
申请日：2003-10-08
申请人： LG CHEM, LTD. , KIM, Jong-Hun , WOO, Boo-Gon , PARK, Eun-Duck , HONG, Mi-Jeung
发明人： KIM, Jong-Hun , WOO, Boo-Gon , PARK, Eun-Duck , HONG, Mi-Jeung
IPC分类号： C08G64/20
CPC分类号： C08G64/20 , C08G64/04 , C08G64/307 , C08G64/40
摘要： The present invention relates to a method for the preparation of a high molecular weight polycarbonate resin, and more particularly to a method for preparing a high molecular weight polycarbonate resin using a solid state polymerization method after the preparation of a crystalline polycarbonate or conducting the preparation of the crystalline polycarbonate and the solid state polymerization thereof simultaneously. According to the method for the preparation of a high molecular weight polycarbonate resin of the invention, it is possible to produce a high molecular weight polycarbonate resin having a narrow molecular weight distribution and uniform properties and that is applicable to injection and extrusion in large quantities with a low cost within a short time.
摘要翻译：制备高分子量聚碳酸酯树脂的方法技术领域本发明涉及一种制备高分子量聚碳酸酯树脂的方法，并且更具体地涉及在制备高分子量聚碳酸酯树脂之后使用固态聚合方法制备高分子量聚碳酸酯树脂的方法，结晶聚碳酸酯或同时进行结晶聚碳酸酯的制备和其固态聚合。根据本发明的高分子量聚碳酸酯树脂的制备方法，可以制备具有窄分子量分布和均匀性能的高分子量聚碳酸酯树脂，并且该聚碳酸酯树脂可适用于大量注入和挤出短时间内成本低。

4. 发明申请

WO2003066569A1 CONTINUOUS METHOD FOR PREPARING AROMATIC CARBONATE USING A HETEROGENEOUS CATALYST AND A REACTION APPARATUS FOR THE SAME 审中-公开
标题翻译：使用异构催化剂制备芳族碳酸酯的连续方法及其相应的反应装置
公开(公告)号：WO2003066569A1
公开(公告)日：2003-08-14
申请号：PCT/KR2003/000237
申请日：2003-02-03
申请人： LG CHEM, LTD. , WOO, Boo-Gon , KWAK, Ja-Hun , HONG, Moo-Ho , HONG, Mi-Jeung
发明人： WOO, Boo-Gon , KWAK, Ja-Hun , HONG, Moo-Ho , HONG, Mi-Jeung
IPC分类号： C07C68/06
CPC分类号： C07C68/06 , C07C68/08 , C07C69/96
摘要： The present invention relates to a continuous method for the preparation of an aromatic carbonate by reacting a dialkyl carbonate and an aromatic hydroxy compound in the presence of a heterogeneous catalyst, and a reaction apparatus for the same. The continuous method comprises the step of reacting dialkyl carbonate and an aromatic hydroxy compound in the presence of the heterogeneous catalyst in a loop-type, catalyst-containing reaction apparatus, wherein a reactor equipped with a filter in which the catalyst is contained is connected with a heat exchanger portion for providing necessary heat during the reaction, reaction solution is circulated between the catalyst-containing portion and heat exchanger via a circulation pump, and by-products can be eliminated via a distillation column connected with the reactor.
摘要翻译：本发明涉及在多相催化剂存在下使碳酸二烷基酯和芳族羟基化合物反应制备芳族碳酸酯的连续方法及其用途。连续方法包括在非均相催化剂存在下，在环状含催化剂的反应装置中使碳酸二烷基酯和芳族羟基化合物反应的步骤，其中装有其中含有催化剂的过滤器的反应器与用于在反应期间提供必要热量的热交换器部分，反应溶液通过循环泵在含催化剂的部分和热交换器之间循环，副产物可以通过与反应器连接的蒸馏塔除去。

5. 发明授权

EP1507953B1 METHOD FOR PREPARING HIGH MOLECULAR WEIGHT POLYCARBONATE 有权
标题翻译：用于生产高分子聚碳酸酯
公开(公告)号：EP1507953B1
公开(公告)日：2009-07-15
申请号：EP03725848.0
申请日：2003-05-28
申请人： LG Chem, Ltd.
发明人： KIM, Jong-Hun , WOO, Boo-Gon , PARK, Eun-Duck , HONG, Mi-Jeung
IPC分类号： C08G64/30
CPC分类号： C08G64/307 , Y10T428/31504 , Y10T428/31507
摘要： The present invention relates to a process for preparing high molecular weight polycarbonate resin, particularly to a process for preparing high molecular weight polycarbonate resin, which conducts condensation polymerization of low molecular weight amorphous polycarbonate prepolymer prepared by transesterification of dialkyl(aryl)carbonate and aromatic hydroxy compound and solid state polymerization within short time to increase molecular weight. The present invention introduces condensation polymerization to lower mole fractions of arylcarbonate existing in unreacted diarylcarboante, end groups of reaction by products of polymerization degree less than 3, and polycarbonate prepolymer obtained by transesterification, and thus can maximize molecular weight increase of polycarbonate after solid state polymerization and remarkably reduce time required for preparing polycarbonate of the same molecular weight. In addition, since the present invention does not use toxic substance phosgene, it has no danger and it can prevent deterioration, and it can prepare high molecular weigh polycarbonate that can be used for injection and extrusion.

6. 发明公开

EP1507953A1 METHOD FOR PREPARING HIGH MOLECULAR WEIGHT POLYCARBONATE 有权
标题翻译：用于生产高分子聚碳酸酯
公开(公告)号：EP1507953A1
公开(公告)日：2005-02-23
申请号：EP03725848.0
申请日：2003-05-28
申请人： LG Chem, Ltd.
发明人： KIM, Jong-Hun , WOO, Boo-Gon , PARK, Eun-Duck , HONG, Mi-Jeung
IPC分类号： E21B17/042
CPC分类号： C08G64/307 , Y10T428/31504 , Y10T428/31507
摘要： The present invention relates to a process for preparing high molecular weight polycarbonate resin, particularly to a process for preparing high molecular weight polycarbonate resin, which conducts condensation polymerization of low molecular weight amorphous polycarbonate prepolymer prepared by transesterification of dialkyl(aryl)carbonate and aromatic hydroxy compound and solid state polymerization within short time to increase molecular weight. The present invention introduces condensation polymerization to lower mole fractions of arylcarbonate existing in unreacted diarylcarboante, end groups of reaction by products of polymerization degree less than 3, and polycarbonate prepolymer obtained by transesterification, and thus can maximize molecular weight increase of polycarbonate after solid state polymerization and remarkably reduce time required for preparing polycarbonate of the same molecular weight. In addition, since the present invention does not use toxic substance phosgene, it has no danger and it can prevent deterioration, and it can prepare high molecular weigh polycarbonate that can be used for injection and extrusion.

7. 发明授权

EP1546233B1 METHOD FOR PREPARING POLYCARBONATE RESIN 有权
标题翻译：聚碳酸酯树脂的制备方法
公开(公告)号：EP1546233B1
公开(公告)日：2007-08-08
申请号：EP03799187.4
申请日：2003-04-18
申请人： LG Chem, Ltd.
发明人： PARK, Eun-Duck , WOO, Boo-Gon , HONG, Mi-Jeung , KIM, Jong-Hun
IPC分类号： C08G64/40 , C08G64/30 , C08G64/20
CPC分类号： C08G64/30 , C08G64/307
摘要： The present invention relates to a method for preparing polycarbonate resin, and more particularly to a method for effectively preparing polycarbonate resin having a large molecular weight in a short time under a melt polymerization condition using a catalyst system comprising phosphoranylidene ammonium salts, which is stable and maintains superior reactivity during melt polymerization and solid state polymerization.
摘要翻译：本发明涉及一种制备聚碳酸酯树脂的方法，更具体地涉及一种使用包含正膦亚基铵盐的催化剂体系在熔融聚合条件下在短时间内有效制备具有大分子量的聚碳酸酯树脂的方法，在熔融聚合和固态聚合期间保持优异的反应性。

8. 发明授权

EP1480939B1 CONTINUOUS METHOD FOR PREPARING AROMATIC CARBONATE USING A HETEROGENEOUS CATALYST AND A REACTION APPARATUS FOR THE SAME 有权
标题翻译：连续法生产芳香碳酸盐使用非均相催化剂，反应装置THEREFOR
公开(公告)号：EP1480939B1
公开(公告)日：2015-12-23
申请号：EP03703489.9
申请日：2003-02-03
申请人： LG Chem, Ltd.
发明人： WOO, Boo-Gon , KWAK, Ja-Hun , HONG, Moo-Ho , HONG, Mi-Jeung
IPC分类号： C07C68/06 , C07C69/96
CPC分类号： C07C68/06 , C07C68/08 , C07C69/96

9. 发明公开

EP1546233A1 METHOD FOR PREPARING POLYCARBONATE RESIN 有权
标题翻译：用于生产聚碳酸酯树脂
公开(公告)号：EP1546233A1
公开(公告)日：2005-06-29
申请号：EP03799187.4
申请日：2003-04-18
申请人： LG Chem, Ltd.
发明人： PARK, Eun-Duck , WOO, Boo-Gon , HONG, Mi-Jeung , KIM, Jong-Hun
IPC分类号： C08G64/40 , C08G64/30 , C08G64/20
CPC分类号： C08G64/30 , C08G64/307
摘要： The present invention relates to a method for preparing polycarbonate resin, and more particularly to a method for effectively preparing polycarbonate resin having a large molecular weight in a short time under a melt polymerization condition using a catalyst system comprising phosphoranylidene ammonium salts, which is stable and maintains superior reactivity during melt polymerization and solid state polymerization.

10. 发明公开

EP1480939A1 CONTINUOUS METHOD FOR PREPARING AROMATIC CARBONATE USING A HETEROGENEOUS CATALYST AND A REACTION APPARATUS FOR THE SAME 有权
标题翻译：连续法生产芳香碳酸盐使用非均相催化剂，反应装置THEREFOR
公开(公告)号：EP1480939A1
公开(公告)日：2004-12-01
申请号：EP03703489.9
申请日：2003-02-03
申请人： LG Chem, Ltd.
发明人： WOO, Boo-Gon , KWAK, Ja-Hun , HONG, Moo-Ho , HONG, Mi-Jeung
IPC分类号： C07C68/06 , C07C69/96
CPC分类号： C07C68/06 , C07C68/08 , C07C69/96
摘要： The present invention relates to a continuous method for the preparation of an aromatic carbonate by reacting a dialkyl carbonate and an aromatic hydroxy compound in the presence of a heterogeneous catalyst, and a reaction apparatus for the same. The continuous method comprises the step of reacting dialkyl carbonate and an aromatic hydroxy compound in the presence of the heterogeneous catalyst in a loop-type, catalyst-containing reaction apparatus, wherein a reactor equipped with a filter in which the catalyst is contained is connected with a heat exchanger portion for providing necessary heat during the reaction, reaction solution is circulated between the catalyst-containing portion and heat exchanger via a circulation pump, and by-products can be eliminated via a distillation column connected with the reactor.

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