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1. 发明申请

WO1995023885A1 PROCESS FOR PURIFYING AQUEOUS SOLUTIONS OF TERTIARY AMINO OXIDES 审中-公开
标题翻译：清理方法水溶液中氧化叔胺
公开(公告)号：WO1995023885A1
公开(公告)日：1995-09-08
申请号：PCT/AT1995000022
申请日：1995-02-01
申请人： LENZING AKTIENGESELLSCHAFT , MÜLLEDER, Eduard , FIRGO, Heinrich
发明人： LENZING AKTIENGESELLSCHAFT
IPC分类号： D01F13/02
CPC分类号： C07C291/04 , C08B1/003 , C08J3/096 , C08J2301/00 , C08L1/02 , D01F2/00
摘要： The invention relates to a process for producing cellulose shaped bodies, said process comprising the following steps: (A) dissolving cellulose in an aqueous solution of a tertiary amino oxide to form a cellulose solution which can be shaped; (B) shaping the cellulose solution and guiding the shaped cellulose solution into an aqueous precipitation bath in which the cellulose is precipitated, whereby a shaped body and a used precipitation bath are formed; (C) purifying the used precipitation bath by bringing it into contact with an ion exchanger, a purified, aqueous amino oxide solution being formed which is possibly dephlegmated and is then used in step (A) again for dissolving cellulose. The invention is characterized in that an ion exchanger is used whose carrier is cellulose to which groups suitable for ion exchange are attached.
摘要翻译：本发明涉及一种用于生产纤维素成型体的方法，该方法包括以下步骤：（A）将纤维素溶解在氧化叔胺的水溶液，以产生一种可模塑纤维素溶液，（B）模制所述纤维素溶液和进行模制纤维素溶液成水沉淀浴其中纤维素沉淀，由此模制体和废沉淀浴，（C）纯化由沉淀浴的用过的沉淀浴被带入与一个离子交换器，其特征在于，纯化的含水氧化胺溶液形成其接触，任选地之后，在步骤（a）浓度重新用来溶解纤维素，其特征在于，离子交换剂，其载体是纤维素，其能够附接的离子交换基团。

2. 发明申请

WO1997007137A1 PROCESS FOR PRODUCING AN AQUEOUS AMINE OXIDE SOLUTION 审中-公开
标题翻译：制造方法的水性胺
公开(公告)号：WO1997007137A1
公开(公告)日：1997-02-27
申请号：PCT/AT1996000149
申请日：1996-08-16
申请人： LENZING AKTIENGESELLSCHAFT , MÄNNER, Johann , FIRGO, Heinrich , MANGENG, Bruno , MÜLLEDER, Eduard , KALT, Wolfram
发明人： LENZING AKTIENGESELLSCHAFT
IPC分类号： C08B01/00
CPC分类号： C08B1/003 , D01F13/02 , Y02P70/627
摘要： The invention relates to a process for producing an aqueous amine oxide solution used in the amine oxide process for producing a mouldable cellulose solution, in which aqueous amine oxide-containing solutions occurring in the amine oxide process especially as regenerating baths are purified and concentrated, where a microbicidal agent is added to the aqueous amine oxide-containing solutions before, during or after purification.
摘要翻译：本发明涉及一种用于制备其在胺氧化物过程用于生产可成型纤维素溶液的水性胺氧化物溶液，在该方法中水溶液aminoxidhältige溶液从氧化胺处理而导致，特别是作为沉淀浴，进行纯化和浓缩，其特征在于，所述水性胺氧化物溶液之前，期间或清洗杀菌剂之后添加。

3. 发明申请

WO1997013893A1 CELLULOSE FIBRES 审中-公开
标题翻译：纤维素纤维
公开(公告)号：WO1997013893A1
公开(公告)日：1997-04-17
申请号：PCT/AT1996000180
申请日：1996-10-03
申请人： LENZING AKTIENGESELLSCHAFT , FIRGO, Heinrich , MÜLLEDER, Eduard , SEIDL, Sigrid
发明人： LENZING AKTIENGESELLSCHAFT
IPC分类号： D01F02/00
CPC分类号： C08B15/005 , C08B15/10 , C08J5/18 , C08J2301/02 , D01F2/00
摘要： The invention concerns a method of producing a cellulose product by the amine oxide process, a suspension of cellulose in an aqueous tertiary-amine oxide being converted into a cellulose solution and the cellulose solution shaped and passed through an aqueous regenerating bath, thus giving a product which, following optional washing, is treated with a cross-linking agent. The method is characterized in that the cellulose solution which is shaped contains a substance which activates the cross-linking agent. The method proposed enables fibres to be produced with accurately controllable fibrillation characteristics.
摘要翻译：本发明涉及一种通过氧化胺，其中纤维素的悬浮液转化成水，叔胺氧化物成纤维素溶液中，形纤维素溶液制备纤维素成形体，并通过含水沉淀浴，由此得到的成型体，其通过，任选之后洗涤，用交联剂，该方法的特征在于：用于使用含有与该交联剂可以被激活的物质形成纤维素溶液处理。本发明的方法允许生产具有目标可控颤动纤维。

4. 发明申请

WO1997007266A1 CELLULOSE FIBRE 审中-公开
标题翻译：纤维素纤维
公开(公告)号：WO1997007266A1
公开(公告)日：1997-02-27
申请号：PCT/AT1996000137
申请日：1996-07-30
申请人： LENZING AKTIENGESELLSCHAFT , FIRGO, Heinrich , SEIDL, Sigrid , BARTSCH, Peter , KÖLL, Berndt , MÜLLEDER, Eduard
发明人： LENZING AKTIENGESELLSCHAFT
IPC分类号： D01F02/00
CPC分类号： C08J5/18 , C08J2301/02 , D01F2/00 , D01F2/02
摘要： A process is disclosed for producing a cellulose shaped body by the aminoxide process. A suspension of cellulose in an aqueous tertiary aminoxide is transformed into a spinnable solution, is extruded through a spinneret and the thus obtained shaped body passes through a spinning bath. The process has the following characteristics: (a) a suspension is used containing a substance capable of reacting with cellulose and of contributing functional groups that are more nucleophilic than the cellulose hydroxy groups; and/or (b) a cellulose is used that bears functional groups that are more nucleophilic than the cellulose hydroxy groups; and/or (c) a suspension is used containing a polymer that bears functional groups that are more nucleophilic than the cellulose hydroxy groups; and/or (d) a substance is added to the spinnable solution that can react with cellulose and contribute functional groups that are more nucleophilic than the cellulose hydroxy groups; and/or (e) a polymer is added to the spinnable solution that bears functional groups that are more nucleophilic than the cellulose hydroxy groups.
摘要翻译：本发明涉及一种通过氧化胺，其中悬浮液的纤维素转化成含水叔胺氧化物成可纺溶液通过喷丝头和得到的成型体挤出通过沉淀浴中进行，其特征在于，制造纤维素成形体（一）的悬浮液，使用通过将包含能与纤维素反应并引入这些基团比纤维素的羟基更亲核官能团的物质; 和/或（b）纤维素使用，携带其比纤维素的羟基更亲核官能团，和/或（c）中的悬浮液，使用一种新的含有携带更亲核的官能团的聚合物如纤维素的羟基基团，和/或可纺的溶液，物质被添加，其与纤维素反应并可以引入这些基团比纤维素的羟基更亲核官能团的（D）; 和可纺溶液/或（e）中，将聚合物加入携带其比纤维素的羟基更亲核官能团。

5. 发明申请

WO1995023827A1 PROCESS FOR PRODUCING CELLULOSE SHAPED BODIES 审中-公开
标题翻译：方法制备纤维素状体
公开(公告)号：WO1995023827A1
公开(公告)日：1995-09-08
申请号：PCT/AT1995000021
申请日：1995-02-01
申请人： LENZING AKTIENGESELLSCHAFT , KALT, Wolfram , FIRGO, Heinrich , MÄNNER, Johann , MÜLLEDER, Eduard , MANGENG, Bruno , NIGSCH, Arnold , SCHWENNINGER, Franz , SCHREMPF, Christoph
发明人： LENZING AKTIENGESELLSCHAFT
IPC分类号： C08L01/02
CPC分类号： C07C291/04 , C08B1/003 , C08J3/096 , C08J2301/00 , C08L1/02 , D01F2/00
摘要： The invention relates to a process for producing cellulose shaped bodies, said process comprising the following steps: (A) dissolving cellulose in an aqueous solution of a tertiary amino oxide, in particular N-methylmorpholine-N-oxide (NMMO), to form a cellulose solution which can be shaped; (B) shaping the cellulose solution and guiding the shaped cellulose solution into an aqueous precipitation bath in which the cellulose is precipitated, whereby a shaped body and a used precipitation bath are formed; (C) regenerating the used precipitation bath, a regenerated, aqueous amino oxide solution being formed which is used in step (A) again for dissolving cellulose. The invention is characterized in that in step (A) a regenerated, aqueous amino oxide solution is used which has a pH in a range whose upper and lower limits are defined, as a function of the tertiary amino oxide concentration, by the equation pH = - 0.0015 x A + 0.2816 x A + f, A being the tertiary amino oxide concentration in the aqueous solution, expressed in weight % of the aqueous solution, and satisfying the condition: 40 %
摘要翻译：本发明涉及一种用于生产纤维素成型体的方法，该方法包括以下步骤：（A）将纤维素溶解在氧化叔胺，特别是N-甲基吗啉-N-氧化物（NMMO）的水溶液，以形成可模制的纤维素溶液; （B）模塑所述纤维素溶液和进行模制纤维素溶液成含水沉淀浴，其中，所述纤维素沉淀，由此形成的成型体和废沉淀浴; （C）再生的用过的沉淀浴，其中这是在步骤（A）中再生的水溶液的氧化胺溶液再用于纤维素的溶解被形成，其特征在于在所述步骤（A）中再生的含水氧化胺溶液中时，一具有pH值在其上的范围内，并且其下限，这取决于叔胺氧化物的浓度，由下式pH值= - <2> + 0.2816×A + F被定义0.0015 X A，其中 A是在该水溶液中的叔胺氧化物的浓度，在该水溶液中和条件40％的质量％表示

6. 发明申请

WO1997007268A1 PROCESS FOR PURIFYING A TERTIARY AMINOXIDE AQUEOUS SOLUTION 审中-公开
标题翻译：清理方法的水溶液的氧化叔胺
公开(公告)号：WO1997007268A1
公开(公告)日：1997-02-27
申请号：PCT/AT1996000148
申请日：1996-08-16
申请人： LENZING AKTIENGESELLSCHAFT , MÜLLEDER, Eduard , MANGENG, Bruno , SCHWENNINGER, Franz , MÄNNER, Johann
发明人： LENZING AKTIENGESELLSCHAFT
IPC分类号： D01F13/02
CPC分类号： C07D295/28 , D01F2/00 , D01F13/02 , Y02P70/627
摘要： A process is disclosed for purifying a tertiary aminoxide aqueous solution that contains impurities that are in part dissolved and in part available in a non-dissolved, colloidal form. The process is characterised by the combination of the following steps: (A) the non-dissolved impurities in colloidal form are practically all removed from the aqueous solution; and (B) the aqueous solution obtained after step (A) is brought into contact with an ion exchanger.
摘要翻译：本发明涉及一种纯化的氧化叔胺，其溶液含有杂质，其中的一些是存在于溶解的形式和部分地以溶解的，胶体状的水溶液，且其特征在于中的步骤的组合：从水溶液中（A）存在于溶解，胶体状态的杂质基本上被完全除去，和（B）的（a）中获得步骤中的水溶液被带入与离子交换剂接触。

7. 发明申请

WO1997011213A1 METHOD OF MANUFACTURING A CELLULOSE PRODUCT 审中-公开
标题翻译：用于生产纤维素状体
公开(公告)号：WO1997011213A1
公开(公告)日：1997-03-27
申请号：PCT/AT1996000167
申请日：1996-09-19
申请人： LENZING AKTIENGESELLSCHAFT , MÜLLEDER, Eduard , SCHREMPF, Christoph , SCHILD, Gabriele
发明人： LENZING AKTIENGESELLSCHAFT
IPC分类号： D01F02/00
CPC分类号： C08B1/003 , C08L1/02 , D01F2/00
摘要： The invention concerns a method of manufacturing a cellulose product, in particular cellulose fibres, a cellulose-containing material being placed in an aqueous solution of a tertiary-amine oyide and brought into suspension, and water being removed from the suspension, while stirring vigorously and maintaining the suspension at an elevated temperature and reduced pressure, until a solution of cellulose is formed. The solution is then passed through a shaping device, in particular a spinneret, and into a regenerating bath to precipitate the dissolved cellulose. The method is characterized in that the cellulose-containing material in the suspension used to produce the cellulose solution is exposed to an electron beam.
摘要翻译：本发明涉及一种用于生产纤维素成型体，特别是纤维素纤维，其特征在于，含有纤维素的材料被引入到氧化叔胺的水溶液，以便从该悬浮液暂停所述含纤维素的材料与强烈混合和升高的温度下的应用和减压，只要水被抽出，直到形成纤维素的溶液，并且该溶液是用模制工具，尤其是喷丝头，形成并以沉淀溶解的纤维素引入到沉淀浴中，其特征在于，为了形成纤维素溶液中，悬浮液使用含有其暴露于电子束辐射的含纤维素的材料。

8. 发明申请

WO1996020300A2 SPINNING DEVICE 审中-公开
标题翻译：自旋电子器件
公开(公告)号：WO1996020300A2
公开(公告)日：1996-07-04
申请号：PCT/AT1995000229
申请日：1995-11-27
申请人： LENZING AKTIENGESELLSCHAFT , SCHWENNINGER, Franz , ECKER, Friedrich , FEILMAIR, Wilhelm , SCHREMPF, Christoph , FIRGO, Heinrich
发明人： LENZING AKTIENGESELLSCHAFT
IPC分类号： D01F02/00
CPC分类号： D01D5/06 , D01F2/00
摘要： The invention relates to a spinning device for operating the wet/dry amino-oxide process with: a spinning nozzle having spinning apertures for extruding filaments; a blower device by means of which the extruded filaments can be cooled immediately after leaving the spinning apertures; a container of spinning bath liquid; a bundling unit fitted in the spinning bath liquid to bundle the extruded filaments; and an air gap defined as the distance between the spinning nozzle from the surface of the spinning bath liquid; in which: the bundling unit is at such a distance from the spinning nozzle that the angle ( alpha ) between the filaments to the perpendicular to the spinning bath liquid is 45 DEG at the most and the relation 0.1 + .0051
摘要翻译：本发明涉及一种用于通过干/湿纺丝方法进行氧化胺处理具有具有纺丝孔的喷丝头的纺丝装置具有用于挤出的长丝，淬火装置与该挤出的长丝可以被立即冷却他们已经离开纺丝孔后，与容器纺丝浴液，其在纺丝浴液提供用于捆绑的挤出长丝捆扎元件，并且被定义为喷丝板到纺丝浴液体的表面的距离的空气间隙，其特征在于，所述捆绑元件位于喷丝头这样的距离，即角（阿尔法），该长丝形成与垂直于纺丝浴液，最大45°的表面，并且该关系0.1 + 0.0051

9. 发明申请

WO1997012083A1 PROCESS FOR TRANSPORTING A CELLULOSE SOLUTION IN AN AQUEOUS TERTIARY AMINE OXIDE 审中-公开
标题翻译： METHOD FOR MOVING纤维素的溶液在水性叔胺氧化物
公开(公告)号：WO1997012083A1
公开(公告)日：1997-04-03
申请号：PCT/AT1996000171
申请日：1996-09-24
申请人： LENZING AKTIENGESELLSCHAFT , KALT, Wolfram , MÄNNER, Johann , FIRGO, Heinrich , SCHWENNINGER, Franz
发明人： LENZING AKTIENGESELLSCHAFT
IPC分类号： D01D01/06
CPC分类号： D01D1/06 , B01D29/01 , B01D29/15 , B01D29/668 , B01D29/70 , B01D29/96
摘要： The invention concerns a process for transporting a cellulose solution in an aqueous tertiary amine oxide through a component, the cellulose solution flowing in the component at a variable speed. The process is characterized in that, at a point at which the flow speed is comparatively low, the component has an aperture through which some of the cellulose solution flows out of the component.
摘要翻译：本发明涉及一种方法，用于通过一个部件，其中，在所述部件中的纤维素溶液的流速是不同的尺寸，在在该流速是比较小的，一个的位置，其特征在于在部件输送纤维素的溶液在水性叔胺氧化物开口被提供，通过该纤维素溶液的一部分从组件逸出。

10. 发明申请

WO1997007267A1 CELLULOSE FIBRE 审中-公开
标题翻译：纤维素纤维
公开(公告)号：WO1997007267A1
公开(公告)日：1997-02-27
申请号：PCT/AT1996000147
申请日：1996-08-16
申请人： LENZING AKTIENGESELLSCHAFT , SEIDL, Sigrid , FIRGO, Heinrich
发明人： LENZING AKTIENGESELLSCHAFT
IPC分类号： D01F02/00
CPC分类号： D01F2/00 , D06M13/248 , D06M13/278
摘要： The invention relates to a process for producing cellulose fibres by the amine oxide process in which a solution of cellulose is spun in an aqueous tertiary amine oxide into fibres and the fibres are brought into contact with a cross-linking agent, in which said cross-linking agent is a sulphonium compound of formula (I) in which R1 is CH2CH2Z, alkyl, aryl, substituted alkyl or a heterocycle, Z is halogen, sulphato, thiosulphato, phosphato or hydroxy and Y is an anion, and/or a sulphonium compound of formula (II) in which OW is the radical of a polybasic acid in salt or acid form and R2 is CH2CH2OW, alkyl, aryl, substituted alkyl or a heterocycle.
摘要翻译：本发明涉及一种用于生产由氧化胺处理的纤维素纤维的方法，在该方法中纺丝纤维素在水性叔胺氧化物中的溶液到纤维和纤维与交联剂接触，并且其特征在于，作为交联剂锍的式（I）其中R1 CH2CH2Z，烷基，芳基，取代的烷基或杂环，Z是卤素，硫酸根，硫代硫酸根，磷酸根或羟基，并且Y < - >是阴离子，和/或下式的锍化合物（II ）其中，是以盐或酸形式的OW多元酸的残基，和R 2 CH2CH2OW，烷基，芳基，取代的烷基或杂环装置使用。

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