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    • 1. 发明申请
    • METHOD FOR THE PRODUCTION OF ENDOHEDRAL FULLERENES
    • 用于生产富勒烯富勒烯
    • WO2004016624A3
    • 2004-05-21
    • PCT/DE0302501
    • 2003-07-21
    • LEIBNIZ INST FUER FESTKOERPERDUNSCH LOTHARGEORGI PETRAZIEGS FRANKZOELLER HEIDI
    • DUNSCH LOTHARGEORGI PETRAZIEGS FRANKZOELLER HEIDI
    • C01B31/02
    • B82Y30/00B82Y40/00C01B32/15C01B32/152
    • The invention relates to a method for the production of endohedral fullerenes in an arc reactor, by the evaporation of graphite electrodes. The aim of the invention is to achieve a method for the production of endohedral fullerenes in an arc reactor by the evaporation of graphite electrodes by means of which the yield of fullerenes may be significantly improved. Said method is characterised in that the evaporation is carried out in an atmosphere comprising a reactive gas component with at least two elements in an inert gas or an inert gas mixture. A very high fullerene yield of 50 to 95 % of endohedral M3N cluster fullerenes as main product is advantageously achieved using said method. The method may be carried out simply with little complication and gives reproducible results. Fullerenes produced as above can be applied for example as contrast agents for medical investigations.
    • 本发明涉及一种用于通过烧掉Graphitelektroden.Der发明中的电弧反应器中制备富勒烯富勒烯具有用于它的目的是通过烧掉石墨电极与它能够富勒产量显著提供一种用于在电弧反应器中制备富勒烯富勒烯的方法 erhöhen.Das本发明的方法的特征在于,燃烧是在含有一组至少两个元素反应性气体组分的气氛中进行enthält.Mit的方法中,惰性气体或惰性气体混合物中以有利的方式富勒烯的非常高的产率从50%至95% 取得的富勒烯-M 3 N簇富勒烯的主要产物。 该方法可以用很少的努力和以简单的方式来实现,并且给出了在制备可用于例如作为用于医疗检查造影剂这样的富勒烯可再现Ergebnissen.Die。