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1. 发明授权

US06670440B2 Production process and production system of aromatic polycarbonate 有权
标题翻译：芳香族聚碳酸酯的生产工艺和生产体系
公开(公告)号：US06670440B2
公开(公告)日：2003-12-30
申请号：US10203201
申请日：2002-08-07
申请人： Kyosuke Matsumoto , Masasi Simonaru , Toru Sawaki , Katsushi Sasaki , Keiichi Kaneko
发明人： Kyosuke Matsumoto , Masasi Simonaru , Toru Sawaki , Katsushi Sasaki , Keiichi Kaneko
IPC分类号： C08G6400
CPC分类号： C08G64/205 , C08G64/30 , C08G64/307
摘要： There is provided a technique for producing an aromatic polycarbonate which undergoes no deterioration in quality in a gear pump, has excellent hue and contains a small amount of foreign materials even when a production plant is scaled up. In producing the aromatic polycarbonate by melt-polycondensation, a molten polycondensate is fed continuously into a shaft seal portion of a self-lubricating gear pump disposed for transporting the polycondensate from a polycondensation vessel such that the following expressions: Q/S≧0.1 (cm/sec) wherein Q is a flow rate (cm3/sec) of the polycondensate, and S is a cross sectional area (cm2) of a passage provided for feeding the polycondensate to the shaft seal portion, and D≦2.9W1/3 wherein D is an internal diameter (cm) of a pipe, and W is a flow rate, are satisfied, thereby operating the gear pump. A polycondensation vessel therefor is also disclosed.
摘要翻译：提供了一种生产芳族聚碳酸酯的技术，其在齿轮泵中不会劣化，具有优异的色调并且即使在生产设备放大时也含有少量异物。通过熔融缩聚制备芳族聚碳酸酯将熔融缩聚物连续地供给到设置用于从缩聚容器输送缩聚物的自润滑齿轮泵的轴密封部分中，使得以下表达式：其中Q是流动速率（cm 3 / sec）缩聚物，S为将缩聚物供给轴封部的通路的截面积（cm 2），D为管的内径（cm），W为流量，为满意，从而操作齿轮泵。还公开了一种缩聚容器。

2. 发明授权

US06472496B2 Process for production of aromatic polycarbonate resin and molded article of aromatic polycarbonate resin 有权
标题翻译：芳香族聚碳酸酯树脂的制造方法和芳香族聚碳酸酯树脂的成型体
公开(公告)号：US06472496B2
公开(公告)日：2002-10-29
申请号：US09840144
申请日：2001-04-24
申请人： Kyosuke Matsumoto , Masasi Simonaru , Toru Sawaki , Katsushi Sasaki , Masahiro Murakami , Yoshiki Matsuoka
发明人： Kyosuke Matsumoto , Masasi Simonaru , Toru Sawaki , Katsushi Sasaki , Masahiro Murakami , Yoshiki Matsuoka
IPC分类号： C08G6400
CPC分类号： C08G64/307
摘要： An aromatic polycarbonate resin is produced under the conditions that the flow velocity of the reaction mixture in a pipe through which a molten reaction mixture passes is a specific value or over, the viscosity-average molecular weight of the reaction mixture is 1,000 or more, the sum of the average retention times of the reaction mixture is not longer than 3 hours, the wall temperature of the pipe through which a molten reaction mixture passes is set to be higher than the temperature of the reaction mixture in the pipe, the catalyst deactivation agent is added within 2 hours after the completion of the melt polycondensation reaction, the filtration is carried out by using a filter having a specific retained particle size under a specific pressure difference, specific treated amount of the aromatic polycarbonate resin per unit area of the filter and a ratio of W (flow quantity of filtered polymer)×1,000/A (maximum area of the polymer path in the filtration vessel) falling within a specific range, etc.
摘要翻译：在熔融反应混合物通过的管中的反应混合物的流速为特定值以上的条件下制造芳香族聚碳酸酯树脂，反应混合物的粘均分子量为1000以上反应混合物的平均保留时间的总和不超过3小时，熔融反应混合物通过的管的壁温设定为高于管中的反应混合物的温度，催化剂失活剂在熔融缩聚反应完成后2小时内加入，过滤通过使用具有特定保留粒径的特定压力差的过滤器，每单位面积过滤器的芳族聚碳酸酯树脂的特定处理量，过滤聚合物的流量（以过滤聚合物的流量计）×1,000 / A（过滤容器内的聚合物路径的最大面积）特点范围等

3. 发明授权

US06562936B1 Apparatus and method for producing resin 有权
标题翻译：树脂生产设备及方法
公开(公告)号：US06562936B1
公开(公告)日：2003-05-13
申请号：US09786523
申请日：2001-06-11
申请人： Kazuki Hatono , Masumi Hirata , Hiroaki Kaneko , Toru Sawaki , Wataru Funakoshi , Katsushi Sasaki , Masasi Simonaru , Kouji Kiyoshige
发明人： Kazuki Hatono , Masumi Hirata , Hiroaki Kaneko , Toru Sawaki , Wataru Funakoshi , Katsushi Sasaki , Masasi Simonaru , Kouji Kiyoshige
IPC分类号： C08G6400
CPC分类号： B29C47/767 , B29C47/0009 , B29C47/38 , B29C47/402 , C08G64/205 , C08G64/307
摘要： A method of producing a polycarbonate or the like which is excellent in hydrolysis and heat stability such as a reduction in molecular weight at the time of molding and color retention and moldability such as releasability and transferability, rarely experiences residence deterioration such as coloring, crosslinking and gel formation and has an extremely small content of foreign matter by employing a special structure for an opening in the side surface of a horizontal cylindrical vacuum resin treating apparatus, supplying a molten polycarbonate into a unidirectional rotary intermeshing double-screw extruder under specific conditions, adding a specific agent under specific conditions and cleaning the inner surface of a production apparatus by a specific method.
摘要翻译：水解和热稳定性优异的聚碳酸酯等的制造方法，例如成型时的分子量的降低和保色性以及脱模性和转印性等成型性，很少发生着色，交联等的停留劣化，凝胶形成，并且通过采用水平圆筒形真空树脂处理装置的侧表面中的开口的特殊结构，并且在特定条件下将熔融聚碳酸酯供给到单向旋转啮合双螺杆挤出机中，并且具有非常少的异物含量，在特定条件下的特定试剂，并通过具体方法清洗生产装置的内表面。

4. 发明授权

US06323302B1 Carbonic acid diester, aromatic polycarbonate and facilities, and preparation thereof 有权
标题翻译：碳酸二酯，芳族聚碳酸酯和设备及其制备
公开(公告)号：US06323302B1
公开(公告)日：2001-11-27
申请号：US09445824
申请日：1999-12-14
申请人： Katsushi Sasaki , Wataru Funakoshi , Toru Sawaki , Masumi Hirata , Hiroaki Kaneko , Masanori Abe , Masasi Simonaru , Hidemi Takemoto , Jyuhou Matsuo , Yoshiki Matsuoka
发明人： Katsushi Sasaki , Wataru Funakoshi , Toru Sawaki , Masumi Hirata , Hiroaki Kaneko , Masanori Abe , Masasi Simonaru , Hidemi Takemoto , Jyuhou Matsuo , Yoshiki Matsuoka
IPC分类号： C08G6400
CPC分类号： C08G64/307
摘要： Aromatic polycarbonate having a reduced discoloration and improved heat stability, hue, etc. is provided by keeping a pressure in a raw material melting vessel and the linear velocity of a gas in a transporting piping in a specific range, keeping the concentration of a nitrogen-containing basic compound in a specific range, recycling a byproduct containing specific amounts of impurities, suppressing the amounts of a nitrogen-containing basic compound, metallic elements and a silicic acid derivative in the carbonic acid diester at specific values or less, prescribing the material quality of the reaction facilities, and/or forming an oxide layer at the inner wall surfaces of the reaction facilities.
摘要翻译：通过将原料熔融容器中的压力和输送管道中的气体的线速度保持在特定范围来提供具有减少变色和改善的热稳定性，色相等的芳族聚碳酸酯，保持氮气浓度，含有特定范围的碱性化合物，回收含有特定量的杂质的副产物，抑制碳酸二酯中的含氮碱性化合物，金属元素和硅酸衍生物的量在特定值以下，规定材料质量的反应设备，和/或在反应设备的内壁表面形成氧化物层。

5. 发明授权

US06613128B1 Twin screw extruder, method of making aromatic polycarbonate using a twin screw extruder, and method of removing volatiles from an aromatic polycarbonate melt 失效
标题翻译：双螺杆挤出机，使用双螺杆挤出机制备芳族聚碳酸酯的方法，以及从芳族聚碳酸酯熔体中除去挥发物的方法
公开(公告)号：US06613128B1
公开(公告)日：2003-09-02
申请号：US09509946
申请日：2000-04-04
申请人： Masasi Simonaru , Toru Sawaki , Katsushi Sasaki , Kazuki Hatono , Eiji Ito
发明人： Masasi Simonaru , Toru Sawaki , Katsushi Sasaki , Kazuki Hatono , Eiji Ito
IPC分类号： B01D1900
CPC分类号： B29C47/605 , B29C47/0009 , B29C47/0871 , B29C47/1063 , B29C47/38 , B29C47/402 , B29C47/404 , B29C47/6037 , B29C47/762 , B29C47/767 , B29C67/246 , B29K2069/00 , B29K2105/0005 , Y10S425/243
摘要： An aromatic polycarbonate extruder which is a twin screw extruder for kneading components into a molten aromatic polycarbonate, the extruder having at least one module consisting of a kneading unit, a material seal unit, a back kneading unit and full-flight unit which are arranged from an upstream side to a downstream side and a method of kneading components into an aromatic polycarbonate by using the above extruder. The present invention also provides a kneading apparatus and method for producing an aromatic polycarbonate which has an extremely small content of foreign matter and is free from residence deterioration such as coloration, crosslinking or gelation when the aromatic polycarbonate is to be kneaded with various components.
摘要翻译：一种芳族聚碳酸酯挤出机，其是将组分捏合成熔融芳族聚碳酸酯的双螺杆挤出机，该挤出机具有由捏合单元，材料密封单元，后捏合单元和全飞行单元组成的至少一个模块，通过使用上述挤出机将组分捏合成芳族聚碳酸酯的方法。本发明还提供一种用于制备芳香族聚碳酸酯的捏合装置和方法，其中当芳香族聚碳酸酯与各种组分捏合时，其具有非常少的异物含量，并且不存在着色，交联或凝胶化等停留劣化。

6. 发明授权

US06380345B1 Process for producing polycarbonates 有权
标题翻译：生产聚碳酸酯的方法
公开(公告)号：US06380345B1
公开(公告)日：2002-04-30
申请号：US09478540
申请日：2000-01-06
申请人： Kazuhiro Uenishi , Masasi Simonaru , Toru Sawaki , Katsushi Sasaki
发明人： Kazuhiro Uenishi , Masasi Simonaru , Toru Sawaki , Katsushi Sasaki
IPC分类号： C08G6400
CPC分类号： C08G64/307 , C08G64/205
摘要： Purpose To enable the reduction of the quantities of wastes and the performance of long term continuous operation in polycarbonate production. Means for solution As a method for removing the reaction byproducts in the production of a polycarbonate resin by sucking and reducing the pressure, ejectors which use the vapor of a substance comprising the condensed liquid of the reaction byproducts as the driving source are used, and the wall temperatures of piping between a polymerization reactor and the ejectors are held at a temperature equal to the boiling point of said reaction byproducts at reduced pressure or higher.
摘要翻译：目的为了减少废弃物的量和在聚碳酸酯生产中的长期连续操作的性能。解决方案作为通过吸取和降低压力来除去生产聚碳酸酯树脂中的反应副产物的方法的方法，使用蒸气的喷射器使用包含作为驱动源的反应副产物的冷凝液体的物质，聚合反应器和喷射器之间的管道的壁温保持在等于或低于所述反应副产物的沸点的温度。

7. 发明授权

US06525171B2 Process for producing a polycarbonate and method of cleaning a production unit 有权
公开(公告)号：US06525171B2
公开(公告)日：2003-02-25
申请号：US09969582
申请日：2001-10-04
申请人： Hidemi Takemoto , Toru Sawaki , Katsushi Sasaki , Keiichi Kaneko
发明人： Hidemi Takemoto , Toru Sawaki , Katsushi Sasaki , Keiichi Kaneko
IPC分类号： C08F600
CPC分类号： C08G85/008 , C08G64/205 , C08G64/307
摘要： A method of cleaning the aromatic polycarbonate production unit with a carbonic acid diaryl ester at a temperature of 200 to 350° C. in an inert gas atmosphere.

8. 发明授权

US06605686B2 Method for producing an aromatic polycarbonate and method of keeping raw materials thereof 失效
标题翻译：芳香族聚碳酸酯的制造方法及其原料的保存方法
公开(公告)号：US06605686B2
公开(公告)日：2003-08-12
申请号：US10088141
申请日：2002-03-15
申请人： Hidemi Takemoto , Toru Sawaki , Keiichi Kaneko , Katsushi Sasaki
发明人： Hidemi Takemoto , Toru Sawaki , Keiichi Kaneko , Katsushi Sasaki
IPC分类号： C08G6400
CPC分类号： C08G64/307
摘要： An aromatic polycarbonate having excellent color is obtained by keeping an aromatic dihydroxy compound and a carbonic acid diester which are raw materials for the production of an aromatic polycarbonate in consideration of the influences of storage atmosphere, temperature, temperature difference from a storage tank and residence time.
摘要翻译：考虑到储存气氛，温度，与储罐的温度差和停留时间的影响，保留作为芳香族聚碳酸酯的制造原料的芳香族二羟基化合物和碳酸二酯，得到颜色优异的芳香族聚碳酸酯。

9. 发明授权

US06448365B1 Aromatic polycarbonate composition 有权
标题翻译：芳香族聚碳酸酯组合物
公开(公告)号：US06448365B1
公开(公告)日：2002-09-10
申请号：US09959830
申请日：2001-11-08
申请人： Wataru Funakoshi , Masumi Hirata , Hiroaki Kaneko , Yuichi Kageyama , Toru Sawaki , Katsushi Sasaki
发明人： Wataru Funakoshi , Masumi Hirata , Hiroaki Kaneko , Yuichi Kageyama , Toru Sawaki , Katsushi Sasaki
IPC分类号： C08G6400
CPC分类号： G11B7/2534 , C08G64/06 , C08G64/14 , C08G64/307 , C08K5/52 , C08L69/00
摘要： An aromatic polycarbonate composition which contains 0.05 to 65 ppm of bonded phosphorus atoms to polycarbonate chains and free phosphorus compounds consisting of a tervalent phosphorus compound and a pentavalent phosphorus compound in a specific ratio. It is excellent in transparency, color stability and residence stability at the time of molding and is suitably used in disk substrates.
摘要翻译：一种芳族聚碳酸酯组合物，其含有0.05〜65ppm的键合磷原子与聚碳酸酯链，并且由特定比例的三价磷化合物和五价磷化合物组成的游离磷化合物。在成型时透明度，颜色稳定性和停留稳定性优异，适用于盘基材。

10. 发明授权

US06265524B1 Process for the preparation of aromatic polycarbonate 失效
标题翻译：芳香族聚碳酸酯的制备方法
公开(公告)号：US06265524B1
公开(公告)日：2001-07-24
申请号：US09424318
申请日：1999-11-22
申请人： Hidemi Takemoto , Toru Sawaki , Katsushi Sasaki
发明人： Hidemi Takemoto , Toru Sawaki , Katsushi Sasaki
IPC分类号： C08G6400
CPC分类号： C08G64/307 , C07C68/00 , C07C69/96
摘要： A process for producing an aromatic polycarbonate through an ester interchange reaction between an aromatic carbonic acid diester and an aromatic dihydroxy compound, wherein the aromatic carbonic acid diester is obtained through the decarbonylation reaction of an aromatic oxalic acid diester represented by the following general formula (1): wherein two Ar's are the same or different aromatic hydrocarbon groups having 6 to 14 carbon atoms, and has a hydrolyzable halogen content of 5 ppm or less. According to the present invention, an aromatic polycarbonate having a high molecular weight and excellent color can be easily produced without impairing ester interchange reactivity for the production of the aromatic polycarbonate by using an aromatic carbonic acid diester obtained through the decarbonylation of an aromatic oxalic acid diester and controlling the amount of hydrolyzable halogen contained in the aromatic carbonic acid diester to a value smaller than a predetermined value.
摘要翻译：通过芳族碳酸二酯和芳族二羟基化合物之间的酯交换反应制备芳族聚碳酸酯的方法，其中芳族碳酸二酯通过由以下通式（1）表示的芳族草酸二酯的脱羰反应获得）：其中两个Ar是相同或不同的具有6至14个碳原子的芳族烃基，并且具有5ppm或更低的可水解卤素含量。根据本发明，具有高分子量和优异颜色的芳族聚碳酸酯可以通过使用通过芳香族草酸二酯的脱羰获得的芳香族碳酸二酯和将芳香族碳酸二酯中含有的可水解卤素的量控制在较小的值，可以容易地制造而不损害用于制备芳族聚碳酸酯的酯交换反应性超过预定值。

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