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1. 发明授权

US4241166A Photopolymerizable composition comprising a monoazo dye as contrast colorant 失效
标题翻译：包含作为对比色剂的单偶氮染料的可光聚合组合物
公开(公告)号：US4241166A
公开(公告)日：1980-12-23
申请号：US015248
申请日：1979-02-26
申请人： Kurt Klupfel , Heide Sprengel , Walter Deucker , Hansjorg Vollmann
发明人： Kurt Klupfel , Heide Sprengel , Walter Deucker , Hansjorg Vollmann
IPC分类号： C08F2/00 , C08F2/44 , C08F2/48 , G03F7/105 , G03C1/68
CPC分类号： G03F7/105 , Y10S430/163
摘要： The present invention relates to a photopolymerizable mixture comprising a compound with at least two terminal ethylenically-unsaturated groups, a boiling point above 100.degree. C. and which is capable of addition polymerization, a polymeric binder, a photoinitiator, and a monoazo dye corresponding to Formula I: ##STR1## R.sub.2 and R.sub.3 are alkyl or alkenyl groups which may be substituted, and R.sub.4 and R.sub.5 are hydrogen or halogen atoms, or alkyl or alkoxy groups.
摘要翻译：本发明涉及一种可光聚合的混合物，其包含具有至少两个末端烯属不饱和基团，沸点高于100℃并能够加成聚合的化合物，聚合物粘合剂，光引发剂和对应于式I：其中R 2和R 3为可被取代的烷基或链烯基，R 4和R 5为氢或卤原子，或烷基或烷氧基。

2. 发明授权

US5047517A Laked pyrazolone azo pigment, process for its preparation and its use 失效
标题翻译：氯化吡唑啉酮偶氮颜料，其制备及其用途
公开(公告)号：US5047517A
公开(公告)日：1991-09-10
申请号：US413853
申请日：1989-09-28
申请人： Walter Deucker
发明人： Walter Deucker
IPC分类号： C08K5/42 , C09B29/01 , C09B29/50 , C09B63/00 , C09D11/02 , D06P1/62 , D21H21/28
CPC分类号： C09B29/0007 , C08K5/42 , C09B29/366 , C09B63/005 , Y10S534/04
摘要： The invention relates to a yellow monoazo pigment which is obtained by diazotization of 2-amino-4-chloro-5-methylbenzene-1-sulfonic acid, coupling of the diazonium compound with 1-(3'-sulfophenyl)-3-methyl-5-pyrazolone and subsequent laking of the coupling product to the calcium salt.The new pigment has excellent heat stability and bleeding fastness and good light stability. It is particularly suitable for the pigmenting of polymeric plastics in the mass.
摘要翻译：本发明涉及通过2-氨基-4-氯-5-甲基苯-1-磺酸的重氮化获得的黄色单偶氮颜料，重氮化合物与1-（3'-磺基苯基）-3-甲基 - 然后将偶联产物沉淀到钙盐中。新型颜料具有优异的热稳定性和耐渗色牢度以及良好的光稳定性。它特别适用于大量聚合物塑料的着色。

3. 发明授权

US4062642A Process for dyeing and printing synthetic fiber materials 失效
标题翻译：染色和印刷合成纤维材料的工艺
公开(公告)号：US4062642A
公开(公告)日：1977-12-13
申请号：US691846
申请日：1976-06-01
申请人： Walter Deucker , Rudolf Lowenfeld
发明人： Walter Deucker , Rudolf Lowenfeld
IPC分类号： C09B29/00 , C09B29/06 , C09B62/825 , D06P1/18 , D06P1/92 , D06P1/38 , C09B29/36
CPC分类号： C09B29/0081 , C09B29/06 , C09B62/825 , D06P1/18 , D06P1/90 , Y10S8/921 , Y10S8/922 , Y10S8/924
摘要： Process for the dyeing and printing of synthetic fibrous materials, wherein the said fibrous materials are treated with an aqueous dispersion, an aqueous padding liquor or with a solution in an organic solvent of at least one dyestuff of the formula ##STR1## in which R.sub.1 represents hydrogen, chlorine, lower alkyl or --NH--CO-lower alkyl, R.sub.2 represents hydrogen, lower alkyl or lower alkoxy, R.sub.3 represents lower alkyl, lower alkylene-OH, lower alkylene-CN, --CH.sub.2 --CBr.dbd.CH.sub.2, ##STR2## or lower alkylene-COO-lower alkyl, R.sub.4 represents hydrogen, bromine or lower alkyl, and R.sub.5 represents hydrogen, lower alkyl or phenyl, this process yielding violet to bluish-green, preferably reddish to greenish dark blue dyeings and prints of high tinctorial strength and excellent fastness properties on the said fibrous materials, such as fibers of linear polyesters, cellulose esters and polyamides.
摘要翻译：用于染色和印刷合成纤维材料的方法，其中所述纤维材料用水分散体，含水填充液或在至少一种式“IMAGE”的染料的有机溶剂中的溶液处理，其中R1代表氢，氯，低级烷基或-NH-CO-低级烷基，R2代表氢，低级烷基或低级烷氧基，R3代表低级烷基，低级亚烷基-OH，低级亚烷基-CN，-CH2-CBr = CH2，或低级亚烷基-COO-低级烷基，R 4表示氢，溴或低级烷基，R 5表示氢，低级烷基或苯基，该方法产生紫色至蓝绿色，优选为红绿色深蓝色染色和高着色强度的印花和所述纤维材料（例如线性聚酯纤维，纤维素酯和聚酰胺）的优异坚牢度性质。

4. 发明授权

US4009180A Continuous process for preparing copper phthalocyanine 失效
标题翻译：制备铜酞菁的连续工艺
公开(公告)号：US4009180A
公开(公告)日：1977-02-22
申请号：US415633
申请日：1973-11-14
申请人： Walter Deucker , Ernst Spietschka , Dieter Steidl
发明人： Walter Deucker , Ernst Spietschka , Dieter Steidl
IPC分类号： C09B47/067 , C09B67/00 , C09B47/04
CPC分类号： C09B67/0032 , C09B47/067
摘要： A continuous process for preparing copper phthalocyanines by caking a mixture of phthalodinitrile, and a copper salt which comprises carrying out the reaction in a continuously working, heatable, tubular vibration mill, which contains iron or steel bars in the grinding room.In comparison with the continuous processes hitherto known this process requires a considerably smaller amount of thermal energy from outside, since the amount of heat formed in the strongly exothermic condensation process is, to a considerable extent conducted away from the reaction zone, with the aid of heat-conducting grinding bars, and is used in order to heat up the freshly introduced starting product to room temperature.
摘要翻译：通过结合酞腈和铜盐的混合物制备铜酞菁的连续方法，其包括在连续加工的可加热的管式振动研磨机中进行反应，该研磨机在研磨室中含有铁棒或钢棒。

5. 发明授权

US3954810A Process for the preparation of 4-bromonaphthalic acid anhydride 失效
标题翻译： 4-溴苯二甲酸酐的制备方法
公开(公告)号：US3954810A
公开(公告)日：1976-05-04
申请号：US433795
申请日：1974-01-16
申请人： Walter Deucker , Helmut Troster
发明人： Walter Deucker , Helmut Troster
IPC分类号： C07D311/92 , C07C63/72 , C07D311/02
CPC分类号： C07C63/72
摘要： A process for the preparation of 4-bromo-naphthalic acid anhydride by bromination of an alkali metal salt of naphthalic acid in an aqueous medium at a pH of 6.8 to 9 by dropwise adding 0.55 to 0.65 mol of bromine per mol of naphthalic acid and oxidizing the bromine at the same pH-value with chlorine. By this process 4-bromo-naphthalic acid anhydride can be obtained in a quantitative yield whereby the formation of 4-chloro-naphthalic acid is avoided.
摘要翻译：通过在pH为6.8〜9的水性介质中，通过在每摩尔萘二甲酸中滴加0.55〜0.65摩尔溴，氧化邻苯二甲酸的碱金属盐的方法制备4-溴 - 萘二甲酸酐的方法溴在与氯相同的pH值下。通过该方法可以以定量的收率获得4-溴 - 萘二甲酸酐，从而避免形成4-氯 - 萘二甲酸。

6. 发明授权

US4293306A Process for the dyeing and printing of hydrophobic synthetic organic fiber materials with water-insoluble azo dyestuffs 失效
标题翻译：用水不溶性偶氮染料染色和印刷疏水性合成有机纤维材料的方法
公开(公告)号：US4293306A
公开(公告)日：1981-10-06
申请号：US118902
申请日：1980-02-06
申请人： Ernst Hoyer , Willi Steckelberg , Walter Deucker , Rudolf Schickfluss
发明人： Ernst Hoyer , Willi Steckelberg , Walter Deucker , Rudolf Schickfluss
IPC分类号： C09B29/36 , C09B31/14 , C09B43/00 , D06P1/18 , D06P5/28
CPC分类号： D06P1/18 , C09B29/3686 , C09B31/14 , C09B43/003 , D06P5/006 , Y10S8/922
摘要： A process for the dyeing or printing of a hydrophobic organic fibrous material containing or consisting of polyester, wherein(a) the fibrous material is dyed (.alpha.) from an aqueous dispersion with a dyestuff of the formula (1) indicated below at a pH value between 2 and 9 and at a temperature above 100.degree. C. or at about 100.degree. C. in the presence of a carrier, or (.beta.) by impregnating it with an aqueous dispersion of a dyestuff of the formula (1), said dispersion having a pH value between 2 and 9, and subsequently exposing the fibrous material so treated to a short heat treatment between about 180.degree. and 210.degree. C., or(b) the fibrous material is printed with a dyestuff of the formula (1) by the transfer printing method, the dyestuff used in methods (a) and (b) being of the formula (1) ##STR1## in which X represents alkyl of 1 to 4 carbon atoms, phenyl, lower alkyl-phenyl, lower alkoxy-phenyl, nitro-phenyl, chloro-phenyl or bromo-phenyl, and D represents phenyl, lower alkyl-phenyl, lower alkoxy-phenylene, nitro-phenylene, chloro-phenylene, benzoyl-phenylene, phenyl-phenylene, phenoxy-phenylene, lower alkyl-sulfonyl-phenylene, aminocarbonyl-phenylene, aminosulfonyl-phenyl, ##STR2## chloro-nitro-phenyl, lower alkyl-nitro-phenyl, lower alkoxy-nitro-phenyl, di(cyano)-phenyl, trifluoromethyl-nitro-phenyl or hydroxyalkoxy-nitro-phenyl.
摘要翻译：用于染色或印刷含有聚酯或由聚酯组成的疏水性有机纤维材料的方法，其中（a）纤维材料用下式表示的式（1）的染料从水分散体染色（α），pH值为 2和9之间，在高于100℃的温度下或在载体存在下在约100℃，或（β）通过用式（1）的染料的水性分散体浸渍，所述分散体 pH值介于2和9之间，随后将经过处理的纤维材料暴露于约180℃至210℃之间的短热处理，或（b）用式（1）的染料印刷纤维材料，通过转印法，在方法（a）和（b）中使用的式（1）的化合物其中X表示1至4个碳原子的烷基，苯基，低级烷基 - 苯基，低级烷氧基 - 苯基，硝基 - 苯基，氯 - 苯基或溴 - 苯基，D代表苯基，低级烷基苯基，低级烷氧基 - 亚苯基，硝基亚苯基，氯 - 亚苯基，苯甲酰基 - 亚苯基，苯基 - 亚苯基，苯氧基 - 亚苯基，低级烷基 - 磺酰基亚苯基，氨基羰基 - 亚苯基，氨基磺酰基 - 苯基，苯基，低级烷基 - 硝基 - 苯基，低级烷氧基 - 硝基 - 苯基，二（氰基） - 苯基，三氟甲基 - 硝基 - 苯基或羟基烷氧基 - 硝基 - 苯基。

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