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1. 发明授权

US4690558A Method of laser emission spectroscopical analysis and apparatus therefor 失效
标题翻译：激光发射光谱分析方法及其设备
公开(公告)号：US4690558A
公开(公告)日：1987-09-01
申请号：US682835
申请日：1984-12-18
申请人： Kouzou Tsunoyama , Yoshiharu Ohashi , Yasuko Furunushi , Motoyuki Konishi
发明人： Kouzou Tsunoyama , Yoshiharu Ohashi , Yasuko Furunushi , Motoyuki Konishi
IPC分类号： G01N21/71 , G01N21/63
CPC分类号： G01N21/718
摘要： In a method of laser emission spectroscopical analysis, wherein a light emitted from the surface of a sample when a laser beam is irradiated onto the surface of the sample is spectroscopically analyzed, an emission mode of the laser beam is fixed to a gauss distribution type TEM.sub.00 mode to avoid variations in an intensity distribution due to a change in mode, and an analyzed value is obtained from an intensity of a spectral line of an element to be measured when an intensity of a preset spectral line or an intensity ratio between a pair of preset spectral lines is within a predetermined range, so that the influence of wide fluctuations in an evaporation and an excitation processes occurring on the surface of the sample can be eliminated, thereby improving the accuracy of analysis.
摘要翻译：在激光发射光谱分析的方法中，其中当激光束照射到样品的表面上时，从样品表面发射的光被光谱分析，激光束的发射模式固定为高斯分布型TEM00 模式，以避免由于模式变化引起的强度分布的变化，并且当预设的光谱线的强度或一对光束的强度比之间从待测元素的光谱线的强度获得分析值预设的光谱线在预定范围内，从而可以消除在样品表面上发生的蒸发和激发过程中的宽波动的影响，从而提高分析精度。

2. 发明授权

US4652128A Method of performing continuous on-line laser emission spectroscopic analysis on a flowing fluid sample by laser and apparatus therefor 失效
标题翻译：通过激光对流动的流体样品进行连续在线激光发射光谱分析的方法及其设备的方法
公开(公告)号：US4652128A
公开(公告)日：1987-03-24
申请号：US681436
申请日：1984-12-13
申请人： Kouzou Tsunoyama , Wataru Tanimoto , Yoshiharu Ohashi , Shigeyuki Kimura , Fumio Asakawa
发明人： Kouzou Tsunoyama , Wataru Tanimoto , Yoshiharu Ohashi , Shigeyuki Kimura , Fumio Asakawa
IPC分类号： G01N21/69 , G01N21/71 , G01N21/63
CPC分类号： G01N21/718 , G01N2021/695
摘要： A focusing lens having a focal length f is provided at a position spaced a distance L apart from a substance to be measured in the fluid state, the relationship between L and f is controlled, so that the formula:0.95f.ltoreq.L.ltoreq.1.05fis constantly satisfied, and the light emitted when a high output pulse laser irradiates the surface of the substance to be measured is analyzed spectroscopically so that the influence of variations on the surface of the substance to be measured can be avoided and a stabilized laser emission spectroscopically analysis on-line can be conducted as the substance to be measured flows.
摘要翻译：具有焦距f的聚焦透镜设置在与流体状态下的待测物质间隔开距离L的位置处，L和f之间的关系被控制，使得公式0.95f < 不断满足/=1.05f，高频输出脉冲激光照射被测定物质的表面发出的光被光谱分析，能够避免对被测定物质的表面的变化的影响，待测量物质的流动可以在线进行稳定的激光发射光谱分析。

3. 发明授权

US07279523B2 2-cyanoacrylate-based composition, method and agent for evaluating curing thereof 有权
标题翻译：基于2-氰基丙烯酸酯的组合物，用于评价其固化的方法和试剂
公开(公告)号：US07279523B2
公开(公告)日：2007-10-09
申请号：US10494329
申请日：2003-11-04
申请人： Yushi Ando , Yoshiharu Ohashi
发明人： Yushi Ando , Yoshiharu Ohashi
IPC分类号： C08F8/30 , C08F36/18 , C08K5/23 , C09B67/00
CPC分类号： C09D4/00 , C08F2/00 , C08F22/32 , C09J4/00 , C08F222/32
摘要： A 2-cyanoacrylate-based composition comprises a coloring material that changes color with curing of 2-cyanoacrylate. The composition has good visibility and excellent workability as it is colored before curing, and changes color with curing as it becomes colorless or light-colored after curing, thereby providing bonded, filled or surface treated portions with good appearance.
摘要翻译：基于2-氰基丙烯酸酯的组合物包含通过2-氰基丙烯酸酯固化改变颜色的着色材料。该组合物在固化前着色时具有良好的可见性和优异的可加工性，并且在固化后变为无色或浅色时，随着固化而变色，从而提供具有良好外观的粘合，填充或表面处理部分。

4. 发明授权

US06602970B2 2-cyanoacrylate composition 有权
公开(公告)号：US06602970B2
公开(公告)日：2003-08-05
申请号：US09878928
申请日：2001-06-13
申请人： Yushi Ando , Seitaro Tajima , Yoshiharu Ohashi , Haruhiko Takeya , Setsuko Miyanari , Toshihiro Kobori
发明人： Yushi Ando , Seitaro Tajima , Yoshiharu Ohashi , Haruhiko Takeya , Setsuko Miyanari , Toshihiro Kobori
IPC分类号： C08F22236
CPC分类号： C08F222/32 , C09J4/00
摘要： A 2-cyanoacrylate composition comprising a cyclic phenol sulfide derivative. The composition has a high curing rate and is excellent in moist-heat resistance, surface curability and clearance curability.

5. 发明授权

US07863358B2 2-cyanoacrylate composition 有权
标题翻译： 2-氰基丙烯酸酯组合物
公开(公告)号：US07863358B2
公开(公告)日：2011-01-04
申请号：US11918167
申请日：2006-05-29
申请人： Muneaki Kanou , Yoshiharu Ohashi
发明人： Muneaki Kanou , Yoshiharu Ohashi
IPC分类号： C08K5/06 , C08K5/13 , C08K5/159
CPC分类号： C09J4/00
摘要： There is provided a 2-cyanoacrylate composition useful as cyanoacrylate adhesives that maintain a high speed of adhesion to poorly adherent materials and porous materials and have an improved light stability. The 2-cyanoacrylate composition contains a 2-cyanoacrylate, (1) a hindered phenol compound having a specific structure and (2) a compound having a clathrating ability.
摘要翻译：提供了用作氰基丙烯酸酯粘合剂的2-氰基丙烯酸酯组合物，其保持对不良粘附材料和多孔材料的高粘合速度并具有改进的光稳定性。 2-氰基丙烯酸酯组合物含有2-氰基丙烯酸酯，（1）具有特定结构的受阻酚化合物和（2）具有包合能力的化合物。

6. 发明授权

US4542077A Tin-free steel sheets having improved lacquer adhesion 失效
标题翻译：无漆钢板具有改善的漆附着力
公开(公告)号：US4542077A
公开(公告)日：1985-09-17
申请号：US641943
申请日：1984-08-02
申请人： Hajime Ogata , Yoshiharu Ohashi , Shunichi Tsugawa , Toshio Ichida , Toshio Irie
发明人： Hajime Ogata , Yoshiharu Ohashi , Shunichi Tsugawa , Toshio Ichida , Toshio Irie
IPC分类号： C25D5/26 , C25D11/38 , C25D3/04
CPC分类号： C25D11/38 , Y10S428/935 , Y10T428/1259 , Y10T428/12611
摘要： This invention provides a tin-free steel sheet, having superior lacquer adhesion, comprising metallic chromium and chromium oxide coatings on a steel sheet, characterized in that the chromium oxide coating is controlled such that I.sub.Cr.sup.580 /(I.sub.Cr.sup.580 +I.sub.Cr.sup.660) has a value of 0.5 or more provided that I.sub.Cr.sup.580 is the percent transmission corresponding to ol linkage and I.sub.Cr.sup.660 is the percent transmission corresponding to oxo linkage in the infrared absorption spectrum of said chromium oxide coating as measured by Fourier transform infra-red spectroscopy.
摘要翻译： PCT No.PCT / JP84 / 00021 Sec。 371日期1984年8月2日 102（e）日期1984年8月2日PCT提交1984年1月27日PCT公布。公开号WO84 / 02931 日本1984年8月2日。本发明提供了一种具有优异的漆附着性的无锡钢板，在钢板上包含金属铬和氧化铬涂层，其特征在于控制氧化铬涂层，使ICr580 /（ICr580 + ICr660）的值为0.5以上，只要ICr580是对应于醇键的百分比传输，并且ICr660是通过傅里叶变换红外光谱法测量的，所述氧化铬涂层的红外吸收光谱中的氧键的百分比透射率。

7. 发明授权

US07709676B2 Method for producing purified 2-cyanoacrylate 有权
标题翻译：纯化2-氰基丙烯酸酯的制备方法
公开(公告)号：US07709676B2
公开(公告)日：2010-05-04
申请号：US10558382
申请日：2004-05-27
申请人： Muneaki Kanou , Yoshiharu Ohashi
发明人： Muneaki Kanou , Yoshiharu Ohashi
IPC分类号： C07C255/11
CPC分类号： C07C253/34 , C07C255/23
摘要： A method for producing a purified 2-cyanoacrylate is characterized in that distillation is conducted in the presence of a polymerization inhibitor whose boiling point is within ±12° C. of the boiling point of the 2-cyanoacrylate. With this method, polymerization of 2-cyanoacrylate can be continuously prevented in the distillate system during distillation of a crude 2-cyanoacrylate, so that a purified 2-cyanoacrylate can be obtained.
摘要翻译：一种纯化的2-氰基丙烯酸酯的制备方法的特征在于，在聚合抑制剂的沸点为2-氰基丙烯酸酯的沸点±12℃的范围内进行蒸馏。通过这种方法，可以在蒸馏2-氰基丙烯酸酯粗品时在馏出物体系中连续地防止2-氰基丙烯酸酯的聚合，从而可以获得纯化的2-氰基丙烯酸酯。

8. 发明申请

US20080042057A1 Electron Spectroscopy Analysis Method and Analytical Apparatus 审中-公开
标题翻译：电子光谱分析方法及分析仪器
公开(公告)号：US20080042057A1
公开(公告)日：2008-02-21
申请号：US10595614
申请日：2004-10-27
申请人： Noriaki Sanada , Yoshiharu Ohashi , Akira Yamamoto , Retsu Oiwa
发明人： Noriaki Sanada , Yoshiharu Ohashi , Akira Yamamoto , Retsu Oiwa
IPC分类号： G01N23/227
CPC分类号： B82Y30/00 , B82Y15/00 , G01N23/2202 , G01N23/2252
摘要： [Task] The invention enables uniformly etching a surface of a sample with an improved repeatability, and etching at a low cost without requiring any large-scale equipment.[Means for Solving the Problem] In an electron spectroscopy analytical apparatus (1) for executing an analysis of a composition, a chemical state and the like of a surface of a sample (4) or in a depth direction thereof by irradiating an X-ray to the sample (4) from a high-energy particle irradiating unit (6) within a vacuum chamber (2) under a vacuum atmosphere, and detecting a kinetic energy of electrons emitted from the sample (4) by an electric energy analyzer (7) on the basis of a photoelectric effect, the surface of the sample (4) is ion-etched by irradiating a fullerene ion beam to the surface of the sample (4) from an ion gun (8) before irradiating the high-energy particle to the sample (4).
摘要翻译： [任务]本发明能够以改善的重复性均匀地蚀刻样品的表面，并且以低成本进行蚀刻，而不需要任何大型设备。解决问题的手段在电子光谱分析装置（1）中，通过照射X射线照相机，对试样（4）的表面或其深度方向的组成，化学状态等进行分析，在真空室内从真空室（2）内的高能粒子照射单元（6）向样品（4）射线，并用电能分析仪（4）检测从样品（4）发射的电子的动能（如图7所示），基于光电效应，通过在照射高能量之前从离子枪（8）照射富勒烯离子束至样品（4）的表面，对样品（4）的表面进行离子蚀刻颗粒到样品（4）。

9. 发明授权

US5703267A Process for producing 2-cyanoacrylic acid 失效
标题翻译： 2-氰基丙烯酸的制备方法
公开(公告)号：US5703267A
公开(公告)日：1997-12-30
申请号：US621612
申请日：1996-03-26
申请人： Shin Takahashi , Yoshiharu Ohashi , Yushi Ando , Toshio Okuyama
发明人： Shin Takahashi , Yoshiharu Ohashi , Yushi Ando , Toshio Okuyama
IPC分类号： C07C253/30 , C07C255/03
CPC分类号： C07C253/30
摘要： The present invention provides a process for producing 2-cyanoacrylic acid, characterized by subjecting a 2-cyanoacrylate and an organic acid to transesterification reaction. The 2-cyanoacrylic acid obtained by the process of the present invention is useful as a starting material for the preparation of polyfunctional 2-cyanoacrylates.
摘要翻译：本发明提供2-氰基丙烯酸的制备方法，其特征在于使2-氰基丙烯酸酯和有机酸进行酯交换反应。通过本发明的方法获得的2-氰基丙烯酸可用作制备多官能2-氰基丙烯酸酯的起始原料。

10. 发明申请

US20090050019A1 2-Cyanoacrylate Composition 有权
标题翻译： 2-氰基丙烯酸酯组合物
公开(公告)号：US20090050019A1
公开(公告)日：2009-02-26
申请号：US11918167
申请日：2006-05-29
申请人： Muneaki Kanou , Yoshiharu Ohashi
发明人： Muneaki Kanou , Yoshiharu Ohashi
IPC分类号： C09D4/04
CPC分类号： C09J4/00
摘要： There is provided a 2-cyanoacrylate composition useful as cyanoacrylate adhesives that maintain a high speed of adhesion to poorly adherent materials and porous materials and have an improved light stability. The 2-cyanoacrylate composition contains a 2-cyanoacrylate, (1) a hindered phenol compound having a specific structure and (2) a compound having a clathrating ability.
摘要翻译：提供了用作氰基丙烯酸酯粘合剂的2-氰基丙烯酸酯组合物，其保持对不良粘附材料和多孔材料的高粘合速度并具有改进的光稳定性。 2-氰基丙烯酸酯组合物含有2-氰基丙烯酸酯，（1）具有特定结构的受阻酚化合物和（2）具有包合能力的化合物。

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