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1. 发明授权

US08778288B1 Separation method of zirconium and hafnium by solvent extraction process 失效
标题翻译：通过溶剂萃取法分离锆和铪的方法
公开(公告)号：US08778288B1
公开(公告)日：2014-07-15
申请号：US13852143
申请日：2013-03-28
申请人： Korea Institute of Science and Technology , Posco M-Tech
发明人： Hwa Young Lee , Byung Won Cho , Joong Kee Lee
IPC分类号： B01D11/00
CPC分类号： C22B3/0005 , Y02P10/234
摘要： A separation method of zirconium and hafnium is described which includes an extraction process of agitating an undiluted aqueous solution containing zirconium, hafnium, and sulfuric acid with a first stirring solution containing an acidic extractant to produce a first extract solution in which the hafnium is extracted by the acidic extractant; and a recovery process of agitating the first extract solution with a second stirring solution containing a citric acid solution to produce a citric acid solution after extraction in which zirconium is reverse-extracted from the first extract solution to the citric acid solution so as to recover zirconium contained in the first extract solution. The method may reduce the amount of extractant while greatly enhancing the separation effect of zirconium and hafnium, and increase zirconium recovery rate by more than 97% through an additional zirconium recovery process while reducing a hafnium content in zirconium by less than 50 ppm.
摘要翻译：描述了锆和铪的分离方法，其包括使用含有酸性萃取剂的第一搅拌溶液搅拌未稀释的含有锆，铪和硫酸的水溶液的提取方法，以产生其中铪被提取的第一提取溶液酸性提取剂; 以及回收方法，用含有柠檬酸溶液的第二搅拌溶液搅拌第一提取溶液，以在提取后产生柠檬酸溶液，其中将锆从第一提取溶液反萃取至柠檬酸溶液，以回收锆包含在第一提取物溶液中。该方法可以减少萃取剂的量，同时大大提高锆和铪的分离效果，并且通过另外的锆回收方法将锆回收率提高97％以上，同时将锆中的铪含量降低到低于50ppm。

2. 发明授权

US08801916B2 Recovery method of nickel from spent electroless nickel plating solutions by electrolysis 有权
标题翻译：通过电解从废化学镀镍溶液中回收镍的方法
公开(公告)号：US08801916B2
公开(公告)日：2014-08-12
申请号：US13670869
申请日：2012-11-07
申请人： Korea Institute of Science and Technology
发明人： Hwa Young Lee , Byung Won Cho , Joong Kee Lee
IPC分类号： C25C1/08 , C25C3/34 , C25C7/00
CPC分类号： C25C1/08 , C23C18/1617 , C23C18/32
摘要： A recovery method of nickel according to the present invention comprises pretreatment step to prepare a solution for electrolysis by adding hexanesulfonate salt to a treatment solution including nickel, and nickel recovery step to recover nickel in a metal form by electrolysis of the above solution for electrolysis. The present invention can produce nickel in high purity with simple process with low cost, and can recover and reproduce nickel in a metal form with at least 99.5% of high purity and at least 90% of recovery rate.
摘要翻译：根据本发明的镍的回收方法包括预处理步骤，通过向包含镍的处理溶液中加入己磺酸盐制备电解溶液，以及镍回收步骤，通过电解上述电解溶液来回收金属形式的镍。本发明可以以低成本的简单工艺生产高纯度的镍，并且可以以至少99.5％的高纯度和至少90％的回收率回收和再现金属形式的镍。

3. 发明授权

US09203114B2 Electrolyte for magnesium secondary battery and preparation method thereof 有权
标题翻译：镁二次电池用电解液及其制备方法
公开(公告)号：US09203114B2
公开(公告)日：2015-12-01
申请号：US13870439
申请日：2013-04-25
申请人： KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
发明人： Kyung Yoon Chung , Byung Won Cho , Joong Kee Lee , Jae Hyun Cho , Sang Hoon Lee , Won Young Chang
IPC分类号： H01M6/04 , H01M10/26 , H01M10/0567 , H01M10/054 , H01M10/0568
CPC分类号： H01M10/0567 , H01M10/054 , H01M10/0568
摘要： Provided are an electrolyte for a magnesium secondary battery having improved ion conductivity and stability, and a method for preparing the same. The electrolyte for a magnesium secondary battery shows higher ion conductivity as compared to the electrolyte according to the related art, increases the dissociation degree of a magnesium halide electrolyte salt, and provides stable electrochemical characteristics. In addition, after determining the capacity, output characteristics and cycle life of the magnesium secondary battery including the electrolyte, the battery provides significantly higher discharge capacity after 100 cycles, as compared to the electrolyte according to the related art. Therefore, the electrolyte may be useful for an electrolyte solution of a magnesium secondary battery.
摘要翻译：提供一种具有改善的离子传导性和稳定性的用于镁二次电池的电解质及其制备方法。与现有技术的电解液相比，镁二次电池用电解液的离子传导性高，卤化镁电解质盐的解离度提高，电化学性能稳定。此外，在确定包括电解质的镁二次电池的容量，输出特性和循环寿命之后，与根据现有技术的电解液相比，电池在100次循环后提供显着更高的放电容量。因此，电解质可用于镁二次电池的电解液。

4. 发明授权

US08900543B2 Separation of tellurium by solvent extraction method 有权
标题翻译：通过溶剂萃取法分离碲
公开(公告)号：US08900543B2
公开(公告)日：2014-12-02
申请号：US13922380
申请日：2013-06-20
申请人： Korea Institute of Science and Technology , Recytec. Inc.
发明人： Hwa Young Lee , Joong Kee Lee , Jae Gyu Jee , Joon Chul Choi
IPC分类号： C01B19/00
CPC分类号： C01B19/001 , C01B19/00 , Y02P20/129
摘要： A method for separating tellurium includes separating and recovering tellurium (Te) from a dissolved solution containing the tellurium using a solvent extraction by an extractant, which contains one selected from a group consisting of tributyl phosphate (TBP), tris(2-ethylhexyl) phosphate (TEHP) and a combination thereof. The method may separate and recover the tellurium as a high-priced metallic element from a material, such as a Bi2Te3-based waste thermoelectric material, which contains not only the tellurium but also other metallic elements, simply and economically using a solvent extraction, whereby the tellurium with high yield and high purity can be separated, recovered and recycled.
摘要翻译：用于分离碲的方法包括使用萃取剂的溶剂萃取从含有碲的溶解溶液中分离和回收碲（Te），所述萃取剂含有选自磷酸三丁酯（TBP），磷酸三（2-乙基己基）酯（TEHP）及其组合。该方法可以从诸如基于Bi2Te3的废热电材料的材料中分离和回收作为高价金属元素的碲，其不仅包含碲而且还包含其它金属元素，简单且经济地使用溶剂萃取，由此具有高产率和高纯度的碲可以分离，回收和再循环。

5. 发明授权

US09543616B2 Electrolyte for magnesium rechargeable battery and preparation method thereof 有权
标题翻译：镁可充电电池用电解液及其制备方法
公开(公告)号：US09543616B2
公开(公告)日：2017-01-10
申请号：US14633807
申请日：2015-02-27
申请人： KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
发明人： Si Hyoung Oh , Byung Won Cho , Kyung Yoon Chung , Joong Kee Lee , Won Young Chang , Jae Hyun Cho , Junghoon Ha
IPC分类号： H01M10/54 , H01M10/0567 , H01M10/054 , H01M10/0568 , H01M10/0569
CPC分类号： H01M10/0567 , H01M10/054 , H01M10/0568 , H01M10/0569 , H01M2300/0025
摘要： Disclosed is an electrolyte solution for a magnesium rechargeable battery with a high ionic conductivity and a wide electrochemical window compared to the conventional electrolyte solution. The electrolyte solution is prepared by dissolving magnesium metal into the ethereal solution using combinations of metal chloride catalysts. The electrolyte solution can be applied to fabricate magnesium rechargeable batteries and magnesium hybrid batteries with a markedly increased reversible capacity, rate capability, and cycle life compared to those batteries employing the conventional electrolyte solution. Also disclosed is a method for preparing the electrolyte.
摘要翻译：公开了与常规电解质溶液相比，具有高离子电导率和宽电化学窗口的镁可充电电池的电解液。通过使用金属氯化物催化剂的组合将镁金属溶解在醚溶液中来制备电解质溶液。与使用常规电解质溶液的电池相比，电解质溶液可用于制造镁可充电电池和镁混合电池，其具有显着增加的可逆容量，速率能力和循环寿命。还公开了一种制备电解质的方法。

6. 发明授权

US08557202B1 Separation method of zirconium and hafnium with acidic extractants 有权
标题翻译：锆和铪与酸性萃取剂的分离方法
公开(公告)号：US08557202B1
公开(公告)日：2013-10-15
申请号：US13667404
申请日：2012-11-02
申请人： Korea Institute of Science and Technology
发明人： Hwa Young Lee , Byung Won Cho , Joong Kee Lee
IPC分类号： C22B34/00
CPC分类号： C22B3/0063 , C22B34/14 , Y02P10/234
摘要： A separation method of zirconium and hafnium according to an example of the present invention comprising, mixing step to prepare a crude liquid for extraction, by mixing a sulfuric acid solution including zirconium and hafnium, a catalyst, and an acidic extractant; and first extraction step to form a first extract solution layer comprising the acidic extractant in which the hafnium has been extracted and a sulfuric acid solution layer separated from the first extract solution layer, wherein the acidic extractant comprises any one selected from a group consisting of D2EHPA (Di-(2-ethylhexyl)phosphoric acid), PC88A (2-Ethylhexyl phosphonic acid mono-2-ethylhexyl ester), and a combination thereof. The separation method not only saves the amount of extractant used but also increases separation effect of zirconium and hafnium known to be difficult for separating each other, without using no toxic compound such as cyan.
摘要翻译：根据本发明实施例的锆和铪的分离方法，包括：混合步骤，通过混合包含锆和铪的硫酸溶液，催化剂和酸性萃取剂来制备用于萃取的粗液体; 以及第一提取步骤，形成包含其中提取了铪的酸性萃取剂和从第一提取液层分离的硫酸溶液层的第一萃取溶液层，其中酸性萃取剂包含选自D2EHPA （2-（2-乙基己基）磷酸），PC88A（2-乙基己基膦酸单-2-乙基己基酯）及其组合。分离方法不仅节省了使用的萃取剂的量，而且增加了已知难以分离的锆和铪的分离效果，而不使用无毒化合物如青色。

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