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1. 发明授权

US5571918A Method for producing 2-methylspiro(1,3-oxathiolane-5,3')quinuclidine 失效
标题翻译： 2-甲基螺（1,3-氧硫杂环戊烷-5,3'）奎宁环的制备方法
公开(公告)号：US5571918A
公开(公告)日：1996-11-05
申请号：US439576
申请日：1995-05-11
申请人： Koji Hayashi , Sho Tokumoto , Hiroshi Yoshizawa , Tatsuo Isogai , Masaru Kimura , Masahiko Sawaki , Takayoshi Ando , Isamu Katsuyama , Hayato Ariyoshi , Tadashi Nakamura
发明人： Koji Hayashi , Sho Tokumoto , Hiroshi Yoshizawa , Tatsuo Isogai , Masaru Kimura , Masahiko Sawaki , Takayoshi Ando , Isamu Katsuyama , Hayato Ariyoshi , Tadashi Nakamura
IPC分类号： C07D453/00 , A61K31/435 , A61P25/00 , A61P43/00 , B01J27/135 , B01J27/16 , B01J31/02 , C07B61/00 , C07D453/02 , C07D497/20
CPC分类号： C07D497/20
摘要： A method for producing 2-methylspiro(1,3-oxathiolane-5,3')quinuclidine, which comprises reacting 3-hydroxy-3-mercaptomethylquinuclidine or a salt thereof and a carbonyl compound in the presence of a catalyst made of at least one member selected from the group consisting of tin halides, oxyacids of phosphorus, phosphorus oxyhalides and organic sulfonic acids, to produce cis-form 2-methylspiro(1,3-oxathiolane-5,3')quinuclidine or a salt thereof.
摘要翻译：一种2-甲基螺（1,3-氧硫杂环戊烷-5,3'）奎宁环的制备方法，其包括使3-羟基-3-巯基乙基奎宁环或其盐与羰基化合物在催化剂存在下反应，所述催化剂由至少一种选自锡卤化物，磷酸的氧酸，磷酰卤和有机磺酸的组分，以制备顺式2-甲基螺（1,3-氧硫杂环戊烷-5,3'）奎宁环或其盐。

2. 发明申请

US20110021774A1 METHOD FOR PRODUCING PYRIMIDINE COMPOUND 有权
标题翻译：生产吡啶化合物的方法
公开(公告)号：US20110021774A1
公开(公告)日：2011-01-27
申请号：US12933980
申请日：2009-04-16
申请人： Shigeo Murai , Ryoji Koto , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takao Awazu , Hisayoshi Jonishi , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
发明人： Shigeo Murai , Ryoji Koto , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takao Awazu , Hisayoshi Jonishi , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
IPC分类号： C07D401/12 , C07D239/42
CPC分类号： C07D239/42 , C07D239/52 , C07D401/12
摘要： To provide a method for producing pyrimidine compound useful as an intermediate for agricultural chemicals or pharmaceuticals, which is simple in operation, presents high yield and produces only a small amount of by-products.The method comprises reacting a compound represented by the formula (I) with a compound represented by the formula (II) in the presence of a pyridine compound to produce a compound represented by the formula (III), a compound represented by the formula (IV) or their mixture.
摘要翻译：提供一种制造用作农药或药物中间体的嘧啶化合物的方法，其操作简单，产率高，仅产生少量副产物。该方法包括使式（I）表示的化合物与式（II）表示的化合物在吡啶化合物的存在下反应，制得由式（III）表示的化合物，式（IV）表示的化合物）或它们的混合物。

3. 发明授权

US08338612B2 Process for producing toluidine compound 有权
标题翻译：甲苯胺化合物的制备方法
公开(公告)号：US08338612B2
公开(公告)日：2012-12-25
申请号：US12671050
申请日：2008-07-29
申请人： Shigeo Murai , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
发明人： Shigeo Murai , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
IPC分类号： C07D213/74
CPC分类号： C07D213/72
摘要： Because fluazinam is excellent as an active ingredient of pesticides and highly useful, it is desired to produce it efficiently in a proper form with simple operations at low cost in an environmentally friendly manner. The desired product is obtained in good yields with simple operations by using industrially advantageous reaction systems by a process comprising (1) a step of reacting ACTF and DCDNBTF in the presence of an alkali component, a solvent selected from the group consisting of ketones, nitriles, ethers and esters and a sufficient amount of water to substantially dissolve the alkali component, (2) a step of neutralizing or acidifying the reaction mixture with an acid and (3) a step of removing the solvent by distillation from the mixture containing fluazinam as the reaction product and the reaction solvent to precipitate crystals the product.
摘要翻译：由于氟啶胺作为农药的有效成分是优异的，而且是非常有用的，因此希望能以低成本的环境友好的方式以简单的操作以适当的形式有效地生产。通过使用工业上有利的反应体系，通过使用包括（1）在碱组分，选自酮，腈的溶剂存在下使ACTF和DCDNBTF反应的步骤，以简单的操作获得所需产物，醚和酯和足够量的水以基本上溶解碱组分，（2）用酸中和或酸化反应混合物的步骤和（3）通过蒸馏从包含氟啶胺的混合物中除去溶剂的步骤为反应产物和反应溶剂使产物析出晶体。

4. 发明申请

US20100197930A1 PROCESS FOR PRODUCING TOLUIDINE COMPOUND 有权
标题翻译：生产托洛芬化合物的方法
公开(公告)号：US20100197930A1
公开(公告)日：2010-08-05
申请号：US12671050
申请日：2008-07-29
申请人： Shigeo Murai , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
发明人： Shigeo Murai , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
IPC分类号： C07D213/36
CPC分类号： C07D213/72
摘要： Because fluazinam is excellent as an active ingredient of pesticides and highly useful, it is desired to produce it efficiently in a proper form with simple operations at low cost in an environmentally friendly manner. The desired product is obtained in good yields with simple operations by using industrially advantageous reaction systems by a process comprising (1) a step of reacting ACTF and DCDNBTF in the presence of an alkali component, a solvent selected from the group consisting of ketones, nitriles, ethers and esters and a sufficient amount of water to substantially dissolve the alkali component, (2) a step of neutralizing or acidifying the reaction mixture with an acid and (3) a step of removing the solvent by distillation from the mixture containing fluazinam as the reaction product and the reaction solvent to precipitate crystals the product.
摘要翻译：由于氟啶胺作为农药的有效成分是优异的，而且是非常有用的，因此希望能以低成本的环境友好的方式以简单的操作以适当的形式有效地生产。通过使用工业上有利的反应体系，通过使用包括（1）在碱组分，选自酮，腈的溶剂存在下使ACTF和DCDNBTF反应的步骤，以简单的操作获得所需产物，醚和酯和足够量的水以基本上溶解碱组分，（2）用酸中和或酸化反应混合物的步骤和（3）通过蒸馏从包含氟啶胺的混合物中除去溶剂的步骤为反应产物和反应溶剂使产物析出晶体。

5. 发明授权

US08440824B2 Method for producing pyrimidine compound 有权
标题翻译：制备嘧啶化合物的方法
公开(公告)号：US08440824B2
公开(公告)日：2013-05-14
申请号：US12933980
申请日：2009-04-16
申请人： Shigeo Murai , Ryoji Koto , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takao Awazu , Hisayoshi Jonishi , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
发明人： Shigeo Murai , Ryoji Koto , Hiroshi Yoshizawa , Takeshi Ohshima , Katsuyoshi Murakami , Takao Awazu , Hisayoshi Jonishi , Takayoshi Ando , Tadashi Nakamura , Norio Adachi , Akihiko Isogai
IPC分类号： C07D239/02
CPC分类号： C07D239/42 , C07D239/52 , C07D401/12
摘要： To provide a method for producing pyrimidine compound useful as an intermediate for agricultural chemicals or pharmaceuticals, which is simple in operation, presents high yield and produces only a small amount of by-products.The method comprises reacting a compound represented by the formula (I) with a compound represented by the formula (II) in the presence of a pyridine compound to produce a compound represented by the formula (III), a compound represented by the formula (IV) or their mixture.
摘要翻译：提供一种制造用作农药或药物中间体的嘧啶化合物的方法，其操作简单，产率高，仅产生少量副产物。该方法包括使式（I）表示的化合物与式（II）表示的化合物在吡啶化合物的存在下反应，制得由式（III）表示的化合物，式（IV）表示的化合物）或它们的混合物。

6. 发明授权

US4490534A Process for producing 3-chloro-5-trifluoromethylpyridines 失效
标题翻译： 3-氯-5-三氟甲基吡啶的制备方法
公开(公告)号：US4490534A
公开(公告)日：1984-12-25
申请号：US434368
申请日：1982-10-14
申请人： Kanichi Fujikawa , Yasuhiro Tsujii , Itaru Shigehara , Tatsuo Isogai , Hiroshi Yoshizawa , Mikio Miyaji
发明人： Kanichi Fujikawa , Yasuhiro Tsujii , Itaru Shigehara , Tatsuo Isogai , Hiroshi Yoshizawa , Mikio Miyaji
IPC分类号： C07D213/61 , C07D211/72 , C07D211/84
CPC分类号： C07D213/61
摘要： A process for producing a 3-chloro-5-trifluoromethylpyridine derivative comprises reacting a 5-trifluoromethylpyridine derivative having a hydrogen atom at 3-position with chlorine. The process is characterized by reacting said 5-trifluoromethylpyridine derivative with chlorine in a vapor phase in the presence of a catalyst selected from the group consisting of activated carbon and a chloride of a metal element selected from the group consisting of iron, antimony, copper and zinc.
摘要翻译：制备3-氯-5-三氟甲基吡啶衍生物的方法包括使3位具有氢原子的5-三氟甲基吡啶衍生物与氯反应。该方法的特征在于使所述5-三氟甲基吡啶衍生物与气相中的氯反应，所述催化剂选自活性炭和选自铁，锑，铜的金属元素的氯化物和锌。

7. 发明授权

US08673505B2 Non-aqueous electrolyte secondary battery 失效
标题翻译：非水电解质二次电池
公开(公告)号：US08673505B2
公开(公告)日：2014-03-18
申请号：US11730304
申请日：2007-03-30
申请人： Tsutomu Ohzuku , Hiroshi Yoshizawa
发明人： Tsutomu Ohzuku , Hiroshi Yoshizawa
IPC分类号： H01M10/36 , H01M10/40 , H01M4/48
CPC分类号： H01M4/485 , H01M4/38 , H01M4/525 , H01M10/0567 , H01M10/0569 , H01M2004/021
摘要： A non-aqueous electrolyte secondary battery including a unit cell including a positive electrode, a negative electrode, a separator disposed between the positive electrode and the negative electrode, and a non-aqueous electrolyte, the positive electrode capacity being greater than the negative electrode capacity, and at least a portion of the non-aqueous electrolyte is gasified during charging.
摘要翻译：一种非水电解质二次电池，包括具有正极，负极，配置在所述正极和负极之间的隔板的非电解质电池的正极容量大于负极容量的单位电池，并且至少一部分非水电解质在充电期间气化。

8. 发明授权

US08173301B2 Positive electrode active material for non-aqueous electrolyte secondary battery and non-aqueous electrolyte secondary battery including the same 有权
标题翻译：用于非水电解质二次电池的正极活性材料和包含该非水电解质二次电池的非水电解质二次电池
公开(公告)号：US08173301B2
公开(公告)日：2012-05-08
申请号：US12265231
申请日：2008-11-05
申请人： Hidekazu Hiratsuka , Norihiro Yamamoto , Yutaka Kawatate , Hiroaki Furuta , Kensuke Nakura , Hiroshi Yoshizawa
发明人： Hidekazu Hiratsuka , Norihiro Yamamoto , Yutaka Kawatate , Hiroaki Furuta , Kensuke Nakura , Hiroshi Yoshizawa
IPC分类号： H01M4/525 , H01M4/13 , H01M4/505 , C01D15/00
CPC分类号： H01M4/505 , C01G53/50 , C01P2002/77 , C01P2004/03 , C01P2004/51 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/366 , H01M4/525 , H01M10/0525 , H01M2004/021 , Y02T10/7011
摘要： A positive electrode active material for a non-aqueous electrolyte secondary battery including a lithium-containing transition metal oxide having a closest-packed cubic structure of oxygen, the lithium-containing transition metal oxide having a composition represented by the formula (1): Li[Lip(NixMnyCoz)1-p]O2, where x, y, and z represent element contents of nickel, manganese, and cobalt, respectively, and satisfies 0.2+y≦x≦0.7, 0.15≦y, 0.05≦z, x+y+z=1, and 0≦p≦0.1.
摘要翻译： 1.一种非水电解质二次电池用正极活性物质，其特征在于，包括具有最密堆积立方结构的氧的含锂过渡金属氧化物，所述含锂过渡金属氧化物具有式（1）表示的组成：Li [Lip（NixMnyCoz）1-p] O 2，其中x，y和z分别表示镍，锰和钴的元素含量，满足0.2 + y＆nlE; x＆nlE; 0.7,0.15＆nlE; y，0.05＆，x + y + z = 1，0＆nlE; p＆nlE; 0.1。

9. 发明授权

US08067120B2 Non-aqueous electrolyte secondary battery 有权
标题翻译：非水电解质二次电池
公开(公告)号：US08067120B2
公开(公告)日：2011-11-29
申请号：US11689817
申请日：2007-03-22
申请人： Masaki Deguchi , Tooru Matsui , Hiroshi Yoshizawa
发明人： Masaki Deguchi , Tooru Matsui , Hiroshi Yoshizawa
IPC分类号： H01M6/16
CPC分类号： H01M2/16 , H01M4/485 , H01M10/0569
摘要： The non-aqueous electrolyte secondary battery of the present invention includes a positive electrode containing a lithium-containing transition metal oxide as a positive electrode active material, a negative electrode, a separator interposed between the positive electrode and the negative electrode and a non-aqueous electrolyte. The non-aqueous electrolyte includes a non-aqueous solvent and a solute dissolved therein, and the non-aqueous solvent includes a solvent having an electron-withdrawing substituent. The solvent having an electron-withdrawing substituent includes at least one selected from the group consisting of a sulfonic solvent, a nitrile solvent, a ketonic solvent, a fluorine-containing solvent, a chlorine-containing solvent and a carboxylic acid ester solvent. The separator includes a material containing an electron-withdrawing substituent or an atom having an unshared electron pair.
摘要翻译：本发明的非水电解质二次电池包括含有含锂过渡金属氧化物作为正极活性物质的正极，负极，夹在正极和负极之间的隔膜和非水电解质二次电池电解液非水电解质包括非水溶剂和溶解于其中的溶质，非水溶剂包括具有吸电子取代基的溶剂。具有吸电子取代基的溶剂包括选自磺酸溶剂，腈溶剂，酮溶剂，含氟溶剂，含氯溶剂和羧酸酯溶剂中的至少一种。分离器包括含有吸电子取代基或具有非共享电子对的原子的材料。

10. 发明授权

US07935443B2 Lithium nickel-manganese-cobalt oxide positive electrode active material 有权
标题翻译：锂镍锰钴氧化物正极活性物质
公开(公告)号：US07935443B2
公开(公告)日：2011-05-03
申请号：US10362944
申请日：2002-04-15
申请人： Tsutomu Ohzuku , Hiroshi Yoshizawa , Masatoshi Nagayama
发明人： Tsutomu Ohzuku , Hiroshi Yoshizawa , Masatoshi Nagayama
IPC分类号： H01M4/50 , H01M4/52
CPC分类号： H01M4/485 , H01M4/40 , H01M4/505 , H01M4/525 , H01M4/587
摘要： A nonaqueous electrolytic secondary cell produced at low cost and having a large capacity comprises a negative electrode having an active material mainly composed of a material that at least absorbs and releases lithium ions or metallic lithium, a positive electrode, and an electrolyte. The active material of the positive electrode is an oxide containing nickel, manganese, and cobalt, and the contents of the elements are substantial the same.
摘要翻译：以低成本生产并具有大容量的非水电解质二次电池包括具有主要由至少吸收和释放锂离子或金属锂的材料的活性材料的负极，正极和电解质。正极的活性物质是含有镍，锰，钴的氧化物，元素的含量基本相同。

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